可以考虑将六水三氯化铁晶体在氯化氢气体中脱水，麻烦着呢。如果是就用一点的话，最好采用纯氯在低浓度和惰性气体充斥的条件下氧化还原铁粉（反应剧烈）

学习了。好牛，什么都有人知道！！

it is very simple. It was refluxed in SOCl2 overnight, and then solvent was removed and dried under vacuum. You'd better use a vacuum line. (you can find the exact procedure in Inorganic Synthesis, sorry, I can't remember which volume.) I hope it will be helpful for you.

谢谢了，在氯气中和Fe粉反应比较麻烦吧，也不好控制把，谢谢，现在我这里有很多六水的三氯化铁，希望还有更简单一点的办法，再次辛苦大家了！

二楼的能说得详细点吗？能把文献传过来吗？谢谢！

好的，我试一下哦！谢谢！