请教 XRD中的PDF卡片的含义?
下面是一张XRD的PDF卡片的内容。
请问表头里的参数都代表什么意思?
d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
应该怎么确定其粒径。d(A)对应很多值啊。
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PDF#39-1346: QM=Star/Calculated; d=Other/Unknown; I=(Unknown)
Maghemite-C, syn
Fe2O3
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= d-Cutoff= I/Ic(RIR)=1.4
Ref= Level-1 PDF
Cubic, P4132(213) Z=10.667 mp=
Cell=8.351x8.351x8.351<90x90x90> Pearson=
Density(c)=4.90 Density(m)= Mwt= Vol=
Ref= Ibid.
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Strong Line: 2.52/X 2.95/4 1.48/3 1.61/2 2.09/2 1.70/1 1.09/1 1.27/1
d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
5.918 5.0 2.0 1 1 0 2 14.958 7.479 0.0845 1.0617
4.822 4.0 2.0 1 1 1 3 18.384 9.192 0.1037 1.3030
3.740 5.0 3.0 2 1 0 5 23.771 11.886 0.1337 1.6800
3.411 5.0 4.0 2 1 1 6 26.102 13.051 0.1466 1.8420
2.953 35.0 30.0 2 2 0 8 30.241 15.120 0.1693 2.1277
2.784 2.0 2.0 2 2 1 9 32.124 16.062 0.1796 2.2569
2.643 2.0 2.0 3 1 0 10 33.882 16.941 0.1891 2.3768
2.517 100.0 100.0 3 1 1 11 35.630 17.815 0.1986 2.4956
2.411 3.0 3.0 2 2 2 12 37.249 18.625 0.2073 2.6051
2.316 1.0 1.0 3 2 0 13 38.847 19.423 0.2159 2.7126
2.232 1.0 1.0 3 2 1 14 40.377 20.188 0.2240 2.8150
2.088 16.0 19.0 4 0 0 16 43.284 21.642 0.2394 3.0083
2.025 1.0 1.0 4 1 0 17 44.703 22.352 0.2469 3.1020
1.968 1.0 1.0 3 3 0 18 46.071 23.036 0.2540 3.1919
1.822 2.0 3.0 4 2 1 21 50.007 25.003 0.2744 3.4478
1.704 10.0 15.0 4 2 2 24 53.733 26.866 0.2933 3.6862
1.670 1.0 2.0 4 3 0 25 54.924 27.462 0.2993 3.7617
1.637 1.0 2.0 5 1 0 26 56.106 28.053 0.3053 3.8361
1.607 24.0 38.0 5 1 1 27 57.271 28.636 0.3111 3.9092
1.550 1.0 2.0 5 2 0 29 59.568 29.784 0.3224 4.0518
1.524 2.0 3.0 5 2 1 30 60.685 30.342 0.3279 4.1207
1.475 34.0 58.0 4 4 0 32 62.925 31.463 0.3388 4.2575
1.453 1.0 2.0 4 4 1 33 63.994 31.997 0.3439 4.3222
1.432 1.0 2.0 5 3 0 34 65.072 32.536 0.3491 4.3871
1.391 1.0 2.0 4 4 2 36 67.201 33.601 0.3592 4.5141
1.373 1.0 2.0 6 1 0 37 68.253 34.126 0.3642 4.5762
1.354 1.0 2.0 6 1 1 38 69.305 34.653 0.3691 4.6381
1.320 3.0 6.0 6 2 0 40 71.376 35.688 0.3787 4.7585
1.304 1.0 2.0 5 4 0 41 72.401 36.201 0.3834 4.8177
1.273 5.0 10.0 5 3 3 43 74.471 37.235 0.3928 4.9357
1.259 2.0 4.0 6 2 2 44 75.442 37.721 0.3971 4.9906
1.245 1.0 2.0 6 3 0 45 76.442 38.221 0.4016 5.0467
1.231 1.0 2.0 6 3 1 46 77.442 38.721 0.4060 5.1025
1.205 1.0 2.0 4 4 4 48 79.446 39.723 0.4148 5.2130
1.193 1.0 2.0 6 3 2 49 80.423 40.212 0.4191 5.2663
1.181 1.0 2.0 7 1 0 50 81.419 40.710 0.4234 5.3202
1.136 1.0 2.0 7 2 1 54 85.338 42.669 0.4399 5.5285
1.115 2.0 5.0 6 4 2 56 87.304 43.652 0.4481 5.6306
1.096 1.0 2.0 7 3 0 58 89.244 44.622 0.4560 5.7297
1.087 7.0 16.0 7 3 1 59 90.226 45.113 0.4599 5.7792
1.043 3.0 7.0 8 0 0 64 95.103 47.552 0.4790 6.0190
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平均粒径用Scherrer 方程估算.
好,谢谢!
D是晶面间距。粒径用Scherrer equeation 计算,在GOOGLE上搜索下就找到了,网上有很多介绍的,
请问Maghemite-C和Maghemite-Q分别代表什么意思??