现在想利用电沉积的方法生长铜枝晶,请大神们看看如何设置工作站,谢谢!
我找了一个参考文献,但是不太会设置电化学工作站,请大神帮我看看吧!感激不尽!
[In a typical fabrication procedure, a two-electrode configuration of the electrochemical system was used. A copper gauze 140 mesh woven, wire
diameter ≈ 50 μm) substrate was used as a working electrode and a copper plate was used as a counter electrode. Here, the copper plate (counter electrode) was polished using a sandpaper to remove surface contaminants before the electrodeposition process. The Cu NPF was then grown by electrodeposition in an aqueous electrolyte containing 0.05 m CuSO4, 0.1 m NaBr (or NaCl), and 0.1 m H2SO4 at a deposition voltage of −0.2 V for 20 s, and subsequently in the voltage range of −0.9 to −1.8 V for 200–300 s. After electrodeposition of the Cu NPF, the sample was rinsed in a deionized (DI) water bath for 10 min to remove the remaining reactant ions (e.g., Cu2+, Br–, and H2SO4) on its surface.] -----10.1002/aenm.201803764
这里的沉积过程在电化学工作站上应该选择什么模式呢?
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我看很多文献都是用CV和计时电位法,或计时电流法
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我也刚开始接触电沉积,很多迷茫的地方,求分享