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【有奖交流】积极回复本帖子，参与交流，就有机会分得作者 nick225 的 30 个金币

nick225

新虫 (初入文坛)

应助: 0 (幼儿园)
金币: 16.5
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在线: 24.2小时
虫号: 4164276
注册: 2015-10-22
性别: GG
专业: 碳素材料与超硬材料

[交流] 现在想利用电沉积的方法生长铜枝晶，请大神们看看如何设置工作站，谢谢！

我找了一个参考文献，但是不太会设置电化学工作站，请大神帮我看看吧！感激不尽！

[In a typical fabrication procedure, a two-electrode configuration of the electrochemical system was used. A copper gauze 140 mesh woven, wire
diameter ≈ 50 μm) substrate was used as a working electrode and a copper plate was used as a counter electrode. Here, the copper plate (counter electrode) was polished using a sandpaper to remove surface contaminants before the electrodeposition process. The Cu NPF was then grown by electrodeposition in an aqueous electrolyte containing 0.05 m CuSO4, 0.1 m NaBr (or NaCl), and 0.1 m H2SO4 at a deposition voltage of −0.2 V for 20 s, and subsequently in the voltage range of −0.9 to −1.8 V for 200–300 s. After electrodeposition of the Cu NPF, the sample was rinsed in a deionized (DI) water bath for 10 min to remove the remaining reactant ions (e.g., Cu2+, Br–, and H2SO4) on its surface.] -----10.1002/aenm.201803764
这里的沉积过程在电化学工作站上应该选择什么模式呢？