±±¾©Ê¯ÓÍ»¯¹¤Ñ§Ôº2026ÄêÑо¿ÉúÕÐÉú½ÓÊÕµ÷¼Á¹«¸æ
²é¿´: 542  |  »Ø¸´: 3
µ±Ç°Ö»ÏÔʾÂú×ãÖ¸¶¨Ìõ¼þµÄ»ØÌû£¬µã»÷ÕâÀï²é¿´±¾»°ÌâµÄËùÓлØÌû

klsyt

гæ (СÓÐÃûÆø)

[ÇóÖú] °ïÎÒ¿´¿´Éó¸åÒâ¼û

1£ºthe quality of the structure solution and refinement seems good given that it refined to a fairly small R factor of .067, excluding weak reflexions, and the thermal motions of the atoms in Fig. 1 seem reasonable¡£
2£ºThe  overall R factor reported in Table 1 of .1287, excluding weak reflections , and  .2309 for all reflections  is high by today¡¯s standards, suggesting some problems with this refinement.  The thermal parameters of the complex seem normal , but when I display the full structure based on the CIF, thermal parameters of the single perchlorate anion in the asymmetric unit, appear very high.
¾ßÌåʲôÒâ˼£¿»¹ÓйØÓÚµÚ¶þ¸ö£¬ÐÞÍê¾§ÌåºóûÓÐAÀà´íÎ󣬲»¹ýR1ֵʼÖÕ0.1287.¾§Ìå½á¹¹ÀïÓиö¸ßÂÈËá¸ù£¬ÊÇËüµÄÎÞÐòÒýÆðµÄÂð£¿Çó½â¡£¸ßÊÖ°ïæ
»Ø¸´´ËÂ¥

» ²ÂÄãϲ»¶

» ±¾Ö÷ÌâÏà¹Ø¼ÛÖµÌùÍÆ¼ö£¬¶ÔÄúͬÑùÓаïÖú:

ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

stalart

ľ³æ (ÕýʽдÊÖ)

¿´xi2004ÀÏʦµÄÌû×Ó¼´¿É
4Â¥2013-05-13 19:26:04
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
²é¿´È«²¿ 4 ¸ö»Ø´ð

stalart

ľ³æ (ÕýʽдÊÖ)

¡¾´ð°¸¡¿Ó¦Öú»ØÌû

¡ï ¡ï ¡ï ¡ï ¡ï
¸Ðл²ÎÓ룬ӦÖúÖ¸Êý +1
klsyt: ½ð±Ò+5, ¡ï¡ï¡ïºÜÓаïÖú, ̫ллÁË 2013-05-12 21:39:07
1ûÊ£¬2ÊÇR1¹ý¸ß£¬²»ÄܽÓÊÜ£¬Ó¦¸ÃÊǸßÂÈËá¸ùÎÞÐò£¬ÄãûÓÐsplitÔì³ÉµÄ
2Â¥2013-05-12 20:19:14
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

klsyt

гæ (СÓÐÃûÆø)

ÒýÓûØÌû:
2Â¥: Originally posted by stalart at 2013-05-12 20:19:14
1ûÊ£¬2ÊÇR1¹ý¸ß£¬²»ÄܽÓÊÜ£¬Ó¦¸ÃÊǸßÂÈËá¸ùÎÞÐò£¬ÄãûÓÐsplitÔì³ÉµÄ

²»Ì«»á´¦Àí¸ßÂÈËá¸ùµÄÎÞÐò¡£Í¬Ñ§£¬Äܰï¸öæÂð£¿lisÎļþÀï˵ÊÇO2ºÍO4ÎÞÐò£¬ÎÒ¸ÃÔõôÐÞÄØ£¿Êǽ«ËĸöÑõÈ«¶¼split»¹ÊÇÖ»Òª´¦ÀíO2O4¾ÍºÃ¡£ÔõôÐÞÄØ£¿ÄÜÖ¸µ¼Ò»ÏÂÂð
3Â¥2013-05-12 21:37:36
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
×î¾ßÈËÆøÈÈÌûÍÆ¼ö [²é¿´È«²¿] ×÷Õß »Ø/¿´ ×îºó·¢±í
[¿¼ÑÐ] 267Çóµ÷¼Á +4 uiybh 2026-03-31 4/200 2026-03-31 19:47 by vgtyfty
[¿¼ÑÐ] 070300»¯Ñ§Çóµ÷¼Á +12 С»ÆÑ¼±¦ 2026-03-30 12/600 2026-03-31 19:15 by 253863592
[¿¼ÑÐ] »·¾³¹¤³Ì297·ÖÇóµ÷¼ÁÒ»Ö¾Ô¸º¼¸ßÔº +6 GENJIOW 2026-03-31 6/300 2026-03-31 18:01 by 544594351
[¿¼ÑÐ] 330·ÖÇóµ÷¼Á +6 qzenlc 2026-03-29 6/300 2026-03-31 16:44 by Wang200018
[¿¼ÑÐ] 334·Ö Ò»Ö¾Ô¸ÎäÀí-080500 ²ÄÁÏÇóµ÷¼Á +9 ÀîÀî²»·þÊä 2026-03-25 9/450 2026-03-31 16:25 by hypershenger
[¿¼ÑÐ] 08¹¤¿Æ£¬295£¬½ÓÊÜ¿çרҵµ÷¼Á +4 lmnlzy 2026-03-31 4/200 2026-03-31 15:25 by Î÷¾©Ñ§ÔºÕаì
[¿¼ÑÐ] ±¾¿Æ211°²È«¹¤³Ì£¬³õÊÔ290·Ö£¬Çóµ÷¼Á +3 2719846834 2026-03-28 3/150 2026-03-31 13:52 by ÈÈÇéɳĮ
[¿¼ÑÐ] 085404 22408 315·Ö +5 zhuangyan123 2026-03-31 6/300 2026-03-31 13:48 by limeifeng
[¿¼ÑÐ] Ò»Ö¾Ô¸Õã½­´óѧ¹¤¿Æ¶¯Á¦¹¤³Ì370,ÊýÒ»121,רҵ¿Î135£¬ÏÖÔÚÄÜÈ¥ÄÄÀï +3 080700µ÷¼Á 2026-03-30 4/200 2026-03-31 12:00 by KLMY666
[¿¼ÑÐ] Ò»Ö¾Ô¸´óÁ¬Àí¹¤´óѧ£¬»úе¹¤³Ìѧ˶£¬341 +3 Î÷¹ÏÌïµÄÊØÍûÕß 2026-03-30 3/150 2026-03-31 11:08 by asdfzly
[¿¼ÑÐ] 291Çóµ÷¼Á +12 Y-cap 2026-03-29 15/750 2026-03-31 09:25 by Huaxue_Wang
[¿¼ÑÐ] Ò»Ö¾Ô¸Î÷½»288»¯¹¤×¨Ë¶Çóµ÷¼Á +4 ºÃÔ˺ÃÔË½Ó½Ó 2026-03-24 4/200 2026-03-31 09:18 by Î÷¾©Ñ§ÔºÍÁľ¹¤³
[¿¼ÑÐ] 22408 359·Öµ÷¼Á +4 Qshers 2026-03-27 8/400 2026-03-31 08:53 by Qshers
[¿¼ÑÐ] Ò»Ö¾Ô¸Öк£Ñó320»¯Ñ§¹¤³ÌÓë¼¼Êõѧ˶Çóµ÷¼Á +8 ÅûÐÇºÓ 2026-03-30 8/400 2026-03-31 08:53 by lbsjt
[¿¼ÑÐ] Çóµ÷¼Á£¬Ò»Ö¾Ô¸ ÄϾ©º½¿Õº½Ìì´óѧ £¬080500²ÄÁÏ¿ÆÑ§Ó빤³Ìѧ˶£¬×Ü·Ö289·Ö +9 @taotao 2026-03-29 9/450 2026-03-30 22:29 by ÎÒÊÇС¿µ
[¿¼ÑÐ] 329Çóµ÷¼Á +8 ÐÇÒ°? 2026-03-26 8/400 2026-03-30 13:41 by chemdavid
[¿¼ÑÐ] Çóµ÷¼Á +10 ÕÅzz111 2026-03-27 11/550 2026-03-30 09:17 by Î޼ʵIJÝÔ­
[˶²©¼ÒÔ°] ÕÐÊÕÉúÎïѧ/ϸ°ûÉúÎïѧµ÷¼Á +4 IceGuo 2026-03-26 5/250 2026-03-29 01:25 by griffith2014
[¿¼ÑÐ] 085701»·¾³¹¤³Ì£¬267Çóµ÷¼Á +16 minht 2026-03-26 16/800 2026-03-28 12:16 by zllcz
[¿¼ÑÐ] ÍøÂç¿Õ¼ä°²È«0839Õе÷¼Á +4 w320357296 2026-03-25 6/300 2026-03-25 17:59 by 255671
ÐÅÏ¢Ìáʾ
ÇëÌî´¦ÀíÒâ¼û