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1£ºthe quality of the structure solution and refinement seems good given that it refined to a fairly small R factor of .067, excluding weak reflexions, and the thermal motions of the atoms in Fig. 1 seem reasonable¡£
2£ºThe  overall R factor reported in Table 1 of .1287, excluding weak reflections , and  .2309 for all reflections  is high by today¡¯s standards, suggesting some problems with this refinement.  The thermal parameters of the complex seem normal , but when I display the full structure based on the CIF, thermal parameters of the single perchlorate anion in the asymmetric unit, appear very high.
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2Â¥: Originally posted by stalart at 2013-05-12 20:19:14
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