24小时热门版块排行榜    

查看: 503  |  回复: 3

klsyt

新虫 (小有名气)

[求助] 帮我看看审稿意见

1:the quality of the structure solution and refinement seems good given that it refined to a fairly small R factor of .067, excluding weak reflexions, and the thermal motions of the atoms in Fig. 1 seem reasonable。
2:The  overall R factor reported in Table 1 of .1287, excluding weak reflections , and  .2309 for all reflections  is high by today’s standards, suggesting some problems with this refinement.  The thermal parameters of the complex seem normal , but when I display the full structure based on the CIF, thermal parameters of the single perchlorate anion in the asymmetric unit, appear very high.
具体什么意思?还有关于第二个,修完晶体后没有A类错误,不过R1值始终0.1287.晶体结构里有个高氯酸根,是它的无序引起的吗?求解。高手帮忙
回复此楼

» 猜你喜欢

» 本主题相关价值贴推荐,对您同样有帮助:

已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

stalart

木虫 (正式写手)

【答案】应助回帖

★ ★ ★ ★ ★
感谢参与,应助指数 +1
klsyt: 金币+5, ★★★很有帮助, 太谢谢了 2013-05-12 21:39:07

klsyt

新虫 (小有名气)

stalart

木虫 (正式写手)

相关版块跳转 我要订阅楼主 klsyt 的主题更新
信息提示
请填处理意见