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klsyt

新虫 (小有名气)

[求助] 帮我看看审稿意见

1:the quality of the structure solution and refinement seems good given that it refined to a fairly small R factor of .067, excluding weak reflexions, and the thermal motions of the atoms in Fig. 1 seem reasonable。
2:The  overall R factor reported in Table 1 of .1287, excluding weak reflections , and  .2309 for all reflections  is high by today’s standards, suggesting some problems with this refinement.  The thermal parameters of the complex seem normal , but when I display the full structure based on the CIF, thermal parameters of the single perchlorate anion in the asymmetric unit, appear very high.
具体什么意思?还有关于第二个,修完晶体后没有A类错误,不过R1值始终0.1287.晶体结构里有个高氯酸根,是它的无序引起的吗?求解。高手帮忙
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stalart

木虫 (正式写手)

【答案】应助回帖

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感谢参与,应助指数 +1
klsyt: 金币+5, ★★★很有帮助, 太谢谢了 2013-05-12 21:39:07
1没事,2是R1过高,不能接受,应该是高氯酸根无序,你没有split造成的
2楼2013-05-12 20:19:14
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klsyt

新虫 (小有名气)

引用回帖:
2楼: Originally posted by stalart at 2013-05-12 20:19:14
1没事,2是R1过高,不能接受,应该是高氯酸根无序,你没有split造成的

不太会处理高氯酸根的无序。同学,能帮个忙吗?lis文件里说是O2和O4无序,我该怎么修呢?是将四个氧全都split还是只要处理O2O4就好。怎么修呢?能指导一下吗
3楼2013-05-12 21:37:36
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stalart

木虫 (正式写手)

看xi2004老师的帖子即可
4楼2013-05-13 19:26:04
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