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1\ in  acetonitrile: addn. of TFMS to a slurry of MnCO3 in CH3CN, stirring (55-60.deg.C, 15 min), hot filtration from the insol. brown material through a fine-fritted funnel, concg. of the yellowish filtrate to a white waxy solid (rotary evapn.); washing (anhyd. ether), drying (vac., over drierite);
Diril, Habibe; Chang, Hsiu-Rong; Nilges, Mark J.; Zhang, Xiaohua; Potenza, Joseph A.; et al. Journal of the American Chemical Society,   1989 ,  vol. 111,  p. 5102 - 5114
2\  in  diethyl ether: MnCl2 reacted with excess anhyd. CF3SO3H; pptd. of diethyl ether, collected and dried;
Hambley, Trevor W.; Lawrance, Geoffrey A.; Sangster, David F.; Ward, Christopher B. Australian Journal of Chemistry,   1987 ,  vol. 40,  p. 883 - 894，

不好意思，我也只能找到这些，具体的文献也没能下载下来！要是能下载下来的话，上次就传上去了！