±±¾©Ê¯ÓÍ»¯¹¤Ñ§Ôº2026ÄêÑо¿ÉúÕÐÉú½ÓÊÕµ÷¼Á¹«¸æ
²é¿´: 2123  |  »Ø¸´: 14
µ±Ç°Ö»ÏÔʾÂú×ãÖ¸¶¨Ìõ¼þµÄ»ØÌû£¬µã»÷ÕâÀï²é¿´±¾»°ÌâµÄËùÓлØÌû

335309906

½ð³æ (СÓÐÃûÆø)

[ÇóÖú] ¹ØÓÚÒ»¶ÎÓ¢Îĵķ­Òë ÒÑÓÐ5È˲ÎÓë

Ô­ÎÄÈçÏ£ºThe reaction was worked up by evaporating the ethanol solvent.  The white solid residue was mixed with 50 mL of ether.  The mixture was filtered and washed with ether (3 x 60 mL).  The white powder was mixed with hexanes and evaporated to dryness to give 44g of the hydrochloride salt of the product.  
ǰ°ë½Ø¶ùµÄÒâ˼¾ÍÊÇÒÒÃÑ´ò½¬£¬¹ýÂË£¬È»ºóÒÒÃÑϴһϣ¬ÎÒÃǰ´´Ë·½·¨×öÁË£¬×ßÁËHPLC£¬ÒÒÃÑȷʵÊǰÑÔÓÖʶ¼Ï´³öÀ´ÁË¡£
ºó°ë½Ø¶ùµÄ×ÖÃæÒâ˼£º¡°ºÍÕý¼ºÍé»ìºÏ£¬È»ºóÕô¸É¡±£¬ÄÇÓÐɶÓã¿Æñ²»Êǰ׿»îÁËô£¿£»ËùÒÔÎÒÃÇ·­ÒëΪÕý¼ºÍé´ò½¬£¬È»ºó¹ýÂË£¬Õý¼ºÍéÏ´µÓ£¬×ßÁËHPLC·¢ÏÖÕý¼ºÍéÀïɶ¶¼Ã»ÓС£

ÇóÖú£ºÕâºó°ë½Ø¶ùµ½µ×ÊÇɶ²Ù×÷£¬ÓÐɶÒâÒåÁË£¿
»Ø¸´´ËÂ¥

» ²ÂÄãϲ»¶

» ±¾Ö÷ÌâÏà¹Ø¼ÛÖµÌùÍÆ¼ö£¬¶ÔÄúͬÑùÓаïÖú:

ÐÂÉú´úÓÎ×Ê
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

genhunter

ÖÁ×ðľ³æ (ÖøÃûдÊÖ)

¡¾´ð°¸¡¿Ó¦Öú»ØÌû

¸Ðл²ÎÓ룬ӦÖúÖ¸Êý +1
Ó¦¸ÃÖ»ÊÇÓÃÕý¼ºÍéÇåÏ´½á¾§£¬µ¹µôºóÐý¸É¡£ÎÄÕµÄÓ¢Óïרҵ³Ì¶È²»ºÃ£¬±í´ï²»Çå¡£
Àë³É¹¦»¹²îÒ»µã
7Â¥2016-01-27 12:25:44
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
²é¿´È«²¿ 15 ¸ö»Ø´ð

kk1424

Ö÷¹ÜÇø³¤ (ÖøÃûдÊÖ)

ÖÐÒ©Ñо¿Õß

ÓÅÐãÇø³¤ÓÅÐãÇø³¤ÓÅÐã°æÖ÷ÓÅÐã°æÖ÷

¡¾´ð°¸¡¿Ó¦Öú»ØÌû

¸Ðл²ÎÓ룬ӦÖúÖ¸Êý +1
ËüµÄÒâ˼ÊÇÓÃÕý¼ºÍéÈܽ⣬Ȼºó¸ÉÔïµ½44gµÄʱºò¾ÍºÃÁË£¬²¢Ã»ÓÐ˵³¹µ×¸ÉÔï
Ò©Àí¶¾Àí
2Â¥2016-01-27 09:11:38
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

335309906

½ð³æ (СÓÐÃûÆø)

ÒýÓûØÌû:
2Â¥: Originally posted by kk1424 at 2016-01-27 09:11:38
ËüµÄÒâ˼ÊÇÓÃÕý¼ºÍéÈܽ⣬Ȼºó¸ÉÔïµ½44gµÄʱºò¾ÍºÃÁË£¬²¢Ã»ÓÐ˵³¹µ×¸ÉÔï

¸Ð¾õ²»¶Ô°¡¡£µÚÒ»£¬ÎªÊ²Ã´²»³¹µ×¸ÉÔïÁË£¬ÁôµãÕý¼ºÍéºÃ¹ýÄêô¡£¡£¡£µÚ¶þ£¬»¹ÊDz»ÖªµÀÕⲿ¹¤ÒÕÊÇΪÁ˸ÉÂǰһ²½Èç¹ûµÃµ½ÒºÌ壬Õý¼ºÍé¿ÉÄÜÊÇΪÁËÎö¾§·ÖÉ¢£»¿ÆÊÒǰһ²½ÊǹÌÌ壬ÔÙ¼ÓÕý¼ºÍéÖ»ÄÜÊÇ´ò½¬µÄ×÷ÓÃÁË¡£¡£¡£µ«ÊÇɶ¶¼Ã»´ò³öÀ´¡£¡£¡£
ÐÂÉú´úÓÎ×Ê
3Â¥2016-01-27 10:48:12
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

335309906

½ð³æ (СÓÐÃûÆø)

ÒýÓûØÌû:
2Â¥: Originally posted by kk1424 at 2016-01-27 09:11:38
ËüµÄÒâ˼ÊÇÓÃÕý¼ºÍéÈܽ⣬Ȼºó¸ÉÔïµ½44gµÄʱºò¾ÍºÃÁË£¬²¢Ã»ÓÐ˵³¹µ×¸ÉÔï

´ËÍ⣬²úÆ·ÊDz»ÈܽâÓÚÕý¼ºÍéµÄ£¬
ÐÂÉú´úÓÎ×Ê
4Â¥2016-01-27 10:53:16
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
×î¾ßÈËÆøÈÈÌûÍÆ¼ö [²é¿´È«²¿] ×÷Õß »Ø/¿´ ×îºó·¢±í
[¿¼ÑÐ] Çóµ÷¼Á£¬Ò»Ö¾Ô¸ ÄϾ©º½¿Õº½Ìì´óѧ´óѧ £¬080500²ÄÁÏ¿ÆÑ§Ó빤³Ìѧ˶ +3 @taotao 2026-03-26 4/200 2026-03-27 03:50 by wxiongid
[¿¼ÑÐ] 304²ÄÁÏÇóµ÷¼Á +4 ÖÓllll 2026-03-26 4/200 2026-03-27 03:42 by wxiongid
[¿¼ÑÐ] 286Çóµ÷¼Á +5 PolarBear11 2026-03-26 5/250 2026-03-26 23:59 by ÔËÆøyunqi
[¿¼ÑÐ] 312Çóµ÷¼Á +8 Éϰ¶°ÉZJY 2026-03-22 12/600 2026-03-26 18:49 by muchong357
[¿¼ÑÐ] 274Çóµ÷¼Á +14 ¹Ë¾ÅóÏҪǫÐé 2026-03-24 20/1000 2026-03-26 18:15 by ÀֺǺǵÄ×·ÃÎÈË
[¿¼ÑÐ] 271Çóµ÷¼Á +6 ÉúÈçÏÄ»¨¡­ 2026-03-22 6/300 2026-03-26 16:48 by ÕÅ¿­Ê®°ËºÅ
[¿¼ÑÐ] Ò»Ö¾Ô¸ Î÷±±´óѧ ×Ü·Ö282 Ó¢ÓïÒ»62 Çóµ÷¼Á +7 18419759900 2026-03-25 7/350 2026-03-26 16:07 by ²»³Ôô~µÄ؈
[¿¼ÑÐ] 081700 µ÷¼Á 267·Ö +11 ÃÔÈ˵Ĺþ¹þ 2026-03-23 11/550 2026-03-26 15:41 by zzll406
[¿¼ÑÐ] ²ÄÁÏÓ뻯¹¤¿¼Ñе÷¼Á +10 ‹üÈA 2026-03-22 10/500 2026-03-26 15:40 by zzll406
[¿¼ÑÐ] 291 Çóµ÷¼Á +7 »¯¹¤2026½ì±ÏÒµÉ 2026-03-21 8/400 2026-03-26 11:25 by AlenQIN.
[¿¼ÑÐ] 332Çóµ÷¼Á +6 032500 2026-03-25 6/300 2026-03-25 22:45 by 418490947
[¿¼ÑÐ] 0703»¯Ñ§Çóµ÷¼Á +6 ÄÌÓͲÝÝ®. 2026-03-22 7/350 2026-03-25 10:00 by shangxh
[¿¼ÑÐ] 306Çó0703µ÷¼ÁÒ»Ö¾Ô¸»ªÖÐʦ·¶ +10 Ö½Óãly 2026-03-21 11/550 2026-03-24 17:22 by qingfeng258
[¿¼ÑÐ] Çóµ÷¼ÁÒ»Ö¾Ô¸Î人Àí¹¤´óѧ²ÄÁϹ¤³Ì£¨085601£© +5 WW.' 2026-03-23 7/350 2026-03-24 14:50 by sprinining
[¿¼ÑÐ] »·¾³Ñ§Ë¶288Çóµ÷¼Á +8 ƤƤƤ123456 2026-03-22 8/400 2026-03-23 23:47 by ÈÈÇéɳĮ
[¿¼ÑÐ] Ò»Ö¾Ô¸¹ú¿Æ¹ý³ÌËù081700£¬274Çóµ÷¼Á +3 ÈýË®ÑÐ0Ë®Á¢·½ 2026-03-23 3/150 2026-03-23 23:11 by MajorWen
[¿¼ÑÐ] ²ÄÁÏÓ뻯¹¤085600£¬×Ü·Ö304£¬±¾¿ÆÓÐÁ½Æªsci²ÎÓ룬Çóµ÷¼Á +4 ÐÒÔ˵Ľ´½´ 2026-03-22 5/250 2026-03-22 20:15 by edmund7
[¿¼ÑÐ] 275Çóµ÷¼Á +6 shansx 2026-03-22 8/400 2026-03-22 15:27 by barlinike
[¿¼ÑÐ] 285Çóµ÷¼Á +6 ytter 2026-03-22 6/300 2026-03-22 12:09 by ÐÇ¿ÕÐÇÔÂ
[¿¼ÑÐ] 261ÇóBÇøµ÷¼Á£¬¿ÆÑо­Àú·á¸» +3 Å£Ä̺Üæ 2026-03-20 4/200 2026-03-20 19:34 by JourneyLucky
ÐÅÏ¢Ìáʾ
ÇëÌî´¦ÀíÒâ¼û