24小时热门版块排行榜    

查看: 374  |  回复: 0

童心111

金虫 (职业作家)

小木虫快乐精灵

[求助] 请大家帮忙分析这个审稿意见怎么回答呢?做过水样基质影响的一定进来帮忙啊!

1) Reviewer 1 placed some interesting questions regarding the filtration/spiking of the samples and the matrix effect. If I agree with the authors regarding to the filtration, that is a standard procedure. Independently of the PAHs adsortion to particulate matter, normally what is measured is the soluble phase. Another type of methodology should be employed considering particulate matter or other phase, what is not the focus of the present manuscript. However, Reviewer 1 has a point regarding matrix effect. It is very typical in new methodologies to show that there is no significant difference between an external calibration or a standard addition method. In other cases, and very usual for PAHs analysis, internal standards may also be employed to overcome this matrix effects. But this is not theory that is checked against the literature but actually measured. When the authors present a method for water analysis, it includes all type of water samples even wastewater, correct? Wastewater can be a very complex matrix.

审稿人1觉得水样分析之前不要过滤,因为过滤会滤去颗粒物,而水中污染物的分析不仅包含溶于水的,还应包含颗粒物吸附的。但是文献基本都过滤了,这应该是一个常规程序吧?所以审稿人2是这么认为的。但是他们都认为要考虑基质的影响,可是我见过的水样分析的基本不做基质影响啊!我修改的时候,是纯水和实际水样各自处理了进样,比较峰面积,大小在20%以内表示基质不受影响。有没有具体做过水样基质影响的啊?我不确定我做的对不对。请大侠们帮忙!十分感谢!!

[ Last edited by 自私的猫1988 on 2014-12-9 at 15:16 ]
回复此楼
会当凌绝顶一览众山小
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

智能机器人

Robot (super robot)

我们都爱小木虫

找到一些相关的精华帖子,希望有用哦~

科研从小木虫开始,人人为我,我为人人
相关版块跳转 我要订阅楼主 童心111 的主题更新
最具人气热帖推荐 [查看全部] 作者 回/看 最后发表
[基金申请] 能否申诉? +4 echo8914667 2026-08-30 5/250 2026-08-30 21:11 by echo8914667
[基金申请] 29号明天会评吗 +3 笨笨唐 2026-08-28 3/150 2026-08-30 09:29 by cww8181
[基金申请] 麻烦专家们看看评委们的意见(F口面上) +6 gdd2018 2026-08-28 11/550 2026-08-30 08:58 by 超级无敌华子
[基金申请] 我就是申请一个面上项目而已,这评审意见是按照杰青的条件评的吧? +6 gouxfjh 2026-08-28 11/550 2026-08-30 07:57 by gouxfjh
[基金申请] 国自然评审意见 +13 wangmingqi 2026-08-28 19/950 2026-08-29 10:22 by Poppy1104
[基金申请] 为什么资助数各大高校都创新高,自己申请怎么就这么难 +12 Kittylucky 2026-08-27 13/650 2026-08-29 00:04 by superceng
[基金申请] 系统查不到 +11 董八千 2026-08-26 11/550 2026-08-28 18:06 by Leogzhya
[基金申请] 基金系统什么内容也没有 30+4 winsaint 2026-08-27 9/450 2026-08-28 11:06 by maolC
[基金申请] 怎么查啊 +6 huang1991js 2026-08-26 6/300 2026-08-28 08:42 by winsaint
[基金申请] 哪位高人中了,把查询到的截图贴出来让我看看,让我长长见识 +5 yuleib84 2026-08-26 6/300 2026-08-28 00:02 by yudaoqian88
[基金申请] 基金未中,这种答复是模板吗? +5 zhaosm1982 2026-08-27 6/300 2026-08-27 16:00 by lfy8008
[基金申请] 看板上这么多中的,有点像50人群里49个人都是骗子的那种感觉…… +5 a089 2026-08-26 6/300 2026-08-27 14:05 by jonewore
[文学芳草园] 梦想 +3 myrtle 2026-08-26 3/150 2026-08-27 10:01 by angelyueyi
[基金申请] 出来了 +9 trojank 2026-08-26 9/450 2026-08-26 14:25 by 宝贝虫子
[基金申请] 项目信息和经费信息在系统里都可以看到了 +6 wittyboy 2026-08-26 14/700 2026-08-26 10:55 by wittyboy
[基金申请] 国合可查了 +3 paperzjh 2026-08-26 3/150 2026-08-26 10:41 by LemmonTr
[基金申请] 国合现在查不到了吗? +10 chengyan1220 2026-08-24 20/1000 2026-08-26 08:57 by peasantsprig
[基金申请] 牛来!米来!面来! +8 beefly 2026-08-26 8/400 2026-08-26 08:37 by xuzhipiao
[基金申请] 在坚冰还盖着北海的时候,我看到了怒放的梅花。 (金币+10) +6 ziyangfang 2026-08-25 9/450 2026-08-25 20:26 by huagongfeihu
[基金申请] 没有任何消息-是不是就凉了 +9 图啦图啦 2026-08-24 10/500 2026-08-25 11:59 by 南海小哥
信息提示
请填处理意见