24小时热门版块排行榜    

查看: 383  |  回复: 0

童心111

金虫 (职业作家)

小木虫快乐精灵

[求助] 请大家帮忙分析这个审稿意见怎么回答呢?做过水样基质影响的一定进来帮忙啊!

1) Reviewer 1 placed some interesting questions regarding the filtration/spiking of the samples and the matrix effect. If I agree with the authors regarding to the filtration, that is a standard procedure. Independently of the PAHs adsortion to particulate matter, normally what is measured is the soluble phase. Another type of methodology should be employed considering particulate matter or other phase, what is not the focus of the present manuscript. However, Reviewer 1 has a point regarding matrix effect. It is very typical in new methodologies to show that there is no significant difference between an external calibration or a standard addition method. In other cases, and very usual for PAHs analysis, internal standards may also be employed to overcome this matrix effects. But this is not theory that is checked against the literature but actually measured. When the authors present a method for water analysis, it includes all type of water samples even wastewater, correct? Wastewater can be a very complex matrix.

审稿人1觉得水样分析之前不要过滤,因为过滤会滤去颗粒物,而水中污染物的分析不仅包含溶于水的,还应包含颗粒物吸附的。但是文献基本都过滤了,这应该是一个常规程序吧?所以审稿人2是这么认为的。但是他们都认为要考虑基质的影响,可是我见过的水样分析的基本不做基质影响啊!我修改的时候,是纯水和实际水样各自处理了进样,比较峰面积,大小在20%以内表示基质不受影响。有没有具体做过水样基质影响的啊?我不确定我做的对不对。请大侠们帮忙!十分感谢!!

[ Last edited by 自私的猫1988 on 2014-12-9 at 15:16 ]
回复此楼
会当凌绝顶一览众山小
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

智能机器人

Robot (super robot)

我们都爱小木虫

找到一些相关的精华帖子,希望有用哦~

科研从小木虫开始,人人为我,我为人人
相关版块跳转 我要订阅楼主 童心111 的主题更新
最具人气热帖推荐 [查看全部] 作者 回/看 最后发表
[职场人生] 40+中年人失业后,还能找到好工作吗? +11 xqy2009 2026-10-13 13/650 2026-10-15 21:32 by bear2007
[有机交流] 用NBS溴化时溶剂除了CCl4外还有什么 +3 18834002860 2026-10-12 6/300 2026-10-15 14:30 by 长沙摩尔信息科�
[基金申请] 申请科研项目纯靠实力能成功吗? 200+7 David1982 2026-10-13 11/550 2026-10-15 10:30 by zyqchem
[硕博家园] 极限拉扯,如何抉择 +11 Isak0320 2026-10-12 15/750 2026-10-14 21:55 by 猫鱼不是鱼
[论文投稿] 二审4个多月了还是Awaiting Reviewer Scores 10+3 纳斯达克ML 2026-10-11 4/200 2026-10-14 17:30 by babero
[有机交流] OpenAI又攻克数学难题了,离AI做有机合成还有多远? +8 wangyl_123 2026-10-10 13/650 2026-10-14 15:12 by zuesli
[教师之家] 课题组会帮你通过考核么? +4 好运来~9527 2026-10-10 7/350 2026-10-13 08:41 by xli1984
[公派出国] 售一区SCI文章T0P,我:8O.551.O54,科目全,可十急 +5 qR2AdCWTVtkw 2026-10-09 9/450 2026-10-11 22:34 by XQNyDCa1Tk5n
[找工作] 售SCI一区T0P文章,我:8.O55.1.O.54,科目全,可十急 +5 qR2AdCWTVtkw 2026-10-09 8/400 2026-10-11 22:26 by XQNyDCa1Tk5n
[公派出国] 售SCI一区文章,我:8O5.5.1.O5.4,科目全,可伽急 +5 qR2AdCWTVtkw 2026-10-09 10/500 2026-10-11 22:26 by XQNyDCa1Tk5n
[考博] 售SCI一区T0P文章,我:8.O55.1.O.54,科目全,可十急 +5 qR2AdCWTVtkw 2026-10-09 9/450 2026-10-11 22:15 by XQNyDCa1Tk5n
[考博] 售SCI一区文章,我:8.O.55.1.O.54,科目齐全,可伽急 +3 qR2AdCWTVtkw 2026-10-09 7/350 2026-10-11 22:11 by XQNyDCa1Tk5n
[教师之家] 售SCI文章,我:8O5.5.1.O.54,科目齐全,可+急 (EPI+-1)(金币-50) +5 qR2AdCWTVtkw 2026-10-09 10/500 2026-10-11 22:06 by XQNyDCa1Tk5n
[教师之家] 售SCI一区T0P文章,我:8.O.55.1.O.5.4,科目全,可+急 (EPI+-1)(金币-50) +5 qR2AdCWTVtkw 2026-10-09 10/500 2026-10-11 14:25 by VOMexwnDzOFZ
[教师之家] 售SCI文章,我:8O.5.5.1O.54,科目全,可十急 (EPI+-1)(金币-50) +4 qR2AdCWTVtkw 2026-10-09 7/350 2026-10-11 14:05 by VOMexwnDzOFZ
[考研] 售SCI文章,我:8O.5.5.1O.54,科目全,可十急 +5 qR2AdCWTVtkw 2026-10-09 8/400 2026-10-11 13:51 by VOMexwnDzOFZ
[硕博家园] 售SCI-T0P文章,我:8O.5.5.1.O.54,科目齐全,可+急 +5 qR2AdCWTVtkw 2026-10-09 8/400 2026-10-11 13:45 by VOMexwnDzOFZ
[找工作] 售SCI一区T0P文章,我:8O.55.1.O.5.4,科目齐全,可+急 +3 qR2AdCWTVtkw 2026-10-09 7/350 2026-10-11 10:54 by VOMexwnDzOFZ
[找工作] 售SCI一区T0P文章,我:8O.55.1.O.5.4,科目齐全,可+急 +4 qR2AdCWTVtkw 2026-10-09 7/350 2026-10-11 10:34 by VOMexwnDzOFZ
[公派出国] 售SCI一区T0P文章,我:8O.55.1.O.54,科目全,可伽急 +4 qR2AdCWTVtkw 2026-10-09 4/200 2026-10-11 03:14 by M0zrYVSAnxpE
信息提示
请填处理意见