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Please add details of the absortion correction to the CIF at_exptl_absorpt_process_details    ?

You have described your attempts to model the water molecules as multi-site- it would be useful to add this information to the description of the x-ray experiment in the ESI and to the CIF.  This is particularly relevant to your description of H-bonding.

There are checkCIF alerts, which may be related to the poor model for this electron density:

DIFMN02_ALERT_2_C The minimum difference density is < -0.1*ZMAX*0.75
_refine_diff_density_min given = -0.673
Test value = -0.600
DIFMN03_ALERT_1_C The minimum difference density is < -0.1*ZMAX*0.75
The relevant atom site should be identified.
DIFMX01_ALERT_2_C The maximum difference density is > 0.1*ZMAX*0.75
_refine_diff_density_max given = 0.711
Test value = 0.600
DIFMX02_ALERT_1_C The maximum difference density is > 0.1*ZMAX*0.75
The relevant atom site should be identified.

The closest atom site to these areas of residual electron density should be identified in the CIF and an indication of what you have tried to model this also included.
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