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青灯锁

银虫 (正式写手)

[求助] TPR问题的讨论 已有3人参与

我的审稿意见回复说TPR试验样品数据测得少,并不能说明峰位置相相对应的物种,可是别的文献都是这样确定的啊,求哪位高手指点一下该怎么回复呢?万分感谢,审稿意见原文:The interpretation of the TPR data is sometimes risky. E.g. shifting of rather broad peaks at low intensity levels is usually not conclusive without making an extensive series of experiments of samples with gradually increasing composition. The current number of samples is too small and their composition too broad to arrive at such conclusions. The conclusions about the presence of spinel type Ni or Co containing species needs to be revisited. It is well known that during TPR, due to its nature of being a dynamic technique, such species are easily formed in-situ.
Similar comments can be made about the apparent shifting of the high temperature (average) peaks. Usually this is due to the varying intensity of individual (sub) peaks. Without deconvolution of such average peaks it can be risky to make conclusions about their nature or the nature of the species involved.
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人要有梦想,万一实现了呢
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purez

金虫 (正式写手)

【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与,应助指数 +1
青灯锁: 金币+10, 有帮助, 谢谢啦 2014-08-23 11:04:56
liwentao2010: 金币+1, 谢谢回帖,欢迎常来交流 2014-08-23 12:01:03
此审稿人是行家,按说的做系列样品。

[ 发自手机版 http://muchong.com/3g ]
2楼2014-08-23 10:40:45
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_xmg

木虫 (正式写手)

【答案】应助回帖

★ ★ ★ ★ ★ ★
感谢参与,应助指数 +1
青灯锁: 金币+5, ★★★很有帮助, 谢谢啦 2014-08-24 12:05:01
liwentao2010: 金币+1, 谢谢回帖,欢迎常来交流 2014-08-25 13:31:35
那就再补做吧,除非你能例证文献说服他
3楼2014-08-23 12:19:57
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buctwanghao

铁杆木虫 (正式写手)

【答案】应助回帖

★ ★ ★ ★ ★ ★
感谢参与,应助指数 +1
青灯锁: 金币+5, ★★★很有帮助, 谢谢啦 2014-08-24 12:04:46
liwentao2010: 金币+1, 谢谢回帖,欢迎常来交流 2014-08-25 13:31:42
如果你真的觉得没问题,在审稿意见返回的时候引入文献,驳回审稿人就好了
你要是觉得有问题,就接着补数据吧,祝你文章接收
我颠覆了整个世界,只为扶正你的倒影
4楼2014-08-23 17:32:35
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