²é¿´: 1080  |  »Ø¸´: 3
µ±Ç°Ö»ÏÔʾÂú×ãÖ¸¶¨Ìõ¼þµÄ»ØÌû£¬µã»÷ÕâÀï²é¿´±¾»°ÌâµÄËùÓлØÌû

tingting7673

Í­³æ (³õÈëÎÄ̳)

[ÇóÖú] Éó¸åÒâ¼ûÀï¾§ÌåѧÊý¾ÝÎÊÌâ ÒÑÓÐ1È˲ÎÓë

ÎÄÕÂÉó¸åÒâ¼û»ØÀ´À²£¬¾§ÌåѧÊý¾ÝÎÊÌ⣬ÇóÖú¸÷λ¸ßÊÖ´óÏÀ£º

Éó¸åÒâ¼û£ºWe see from the CIF that there are 2 Uiso/Uij restrained atom sites, 7 distance or angle restraints and 20 least-squares restraints  used in the refinement.   So that the reader can be  fully aware of what was done to generate the reported models,  we should be told - at least in the "_refine_special_details" section of the CIF or in an ESI text  - exactly what these restraints were and why they were necessary.   [An easy way to show what restraints were employed(but not why they were needed) is to include the relevant lines from the SHELXL.ins file in the  "_refine_special_details" section of the CIF.  This should now be done.]

ºÃÏñÊÇ˵insÎļþÀïµÄ¼¸´¦ÏÞ¶¨ÐèÒªÔÚcifÎļþÖÐrefine_special_details ºóÃæÐ´³öÊÇʲôÏÞ¶¨ÒÔ¼°ÎªÊ²Ã´Õâô×ö£¬ÎÒµÄinsÎļþÖеÄÏÞ¶¨Ö÷ÒªÓÐÕ⼸¸öµØ·½£º

dfix 0.95 0.02 o10 h1a o10 h1b
dfix 1.55 0.02 h1a h1b
dfix 3.00 0.02 k1 h1a k1 h1b
isor 0.001 0.001 o11 O11'
dfix 0.85 0.01 o9 h99
dfix 0.85 0.01 o9 h98
dfix 1.39 0.01 h99 h98

¸÷λ¸ßÊÖÄܲ»ÄܸæËßÎÒÔõôд°¡£¬Íò·Ö¸ÐлÖа¡£¡
»Ø¸´´ËÂ¥

» ²ÂÄãϲ»¶

» ±¾Ö÷ÌâÏà¹Ø¼ÛÖµÌùÍÆ¼ö£¬¶ÔÄúͬÑùÓаïÖú:

ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

xi2004

ÖÁ×ðľ³æ (Ö°Òµ×÷¼Ò)

Ö±½Ó°Ñ.resµÄhklf4 endÉÏÃæµÄÄÚÈÝ¿½±´µ½cifÖС£
xi2004-emuch@163.com
4Â¥2014-06-03 18:01:16
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
²é¿´È«²¿ 4 ¸ö»Ø´ð

jackdeng

ר¼Ò¹ËÎÊ (ÖøÃûдÊÖ)

¡¾´ð°¸¡¿Ó¦Öú»ØÌû

¸Ðл²ÎÓ룬ӦÖúÖ¸Êý +1
´ÓÄãµÄdfix¿ÉÒÔ¿´³öÄãÊǶÔË®ÉϵÄÇâÔ­×Ó×öÁËÏÞÖÆ£¬ÏÞÖÆÁËÆäÓëĸÌåOÑõÔ­×Ó£¬½ðÊôKÀë×Ó£¬ÒÔ¼°HÓëHÖ®¼äµÄ¾àÀ룬Äã¿ÉÒÔ˵Ã÷ÕâÑù×öµÄÔ­Òò£¬±ÈÈ磬ΪʲôҪÏÞÖÆHÓëKÖ®¼äµÄ¾àÀ룬ÊDz»ÊÇΪÁË·ÀÖ¹ÆäÔÚxpÖÐÓмüµÄÐγɣ¬Ë®·Ö×ÓÊÇ·ñÎÞÐò£¬ÎªÊ²Ã´ÒªÏÞÖÆÎª0.85ºÍ0.95Á½ÖÖ¾àÀ룿O11ºÍO11¡®ÊÇÎÞÐòÖеÄÁ½¸ö²¿·Ö£¬ÄãֻҪ˵Ã÷¸ÃÔ­×ÓÊÇÎÞÐòµÄ£¨ÈÈÕñ¶¯½Ï´ó£©£¬¾«ÐÞʱÁ½²¿·ÖµÄÕ¼ÓÐÂÊ·Ö±ðÊǶàÉÙ¾ÍÐÐÁË¡£
2Â¥2014-06-03 08:15:08
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

tingting7673

Í­³æ (³õÈëÎÄ̳)

¸Ðл´óÏÀ£¬¹Ø¼üÊÇÔõôÔÚcifÖÐrefine_special_details µÄºóÃæÓñê×¼Ó¢ÎÄд°¡£¬¼±Çó°¡£¬Àϰ弱´ßÖС£¡£¡£
3Â¥2014-06-03 13:59:40
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
×î¾ßÈËÆøÈÈÌûÍÆ¼ö [²é¿´È«²¿] ×÷Õß »Ø/¿´ ×îºó·¢±í
[»ù½ðÉêÇë] ɽ¶«Ê¡ÃæÉÏÏîÄ¿ÏÞ¶îÆÀÉó +4 ʯÈð0426 2026-03-19 4/200 2026-03-22 08:50 by Wei_ren
[¿¼ÑÐ] ÉúÎïѧ071000 329·ÖÇóµ÷¼Á +4 ÎÒ°®ÉúÎïÉúÎﰮΠ2026-03-17 4/200 2026-03-22 08:34 by hxsm
[¿¼ÑÐ] Çóµ÷¼ÁԺУÐÅÏ¢ +4 CX 330 2026-03-21 4/200 2026-03-21 23:48 by ms629
[¿¼ÑÐ] ²ÄÁϹ¤³Ìר˶ 348·ÖÇóµ÷¼Á +3 ¶¬´Ç. 2026-03-17 5/250 2026-03-21 18:47 by ѧԱ8dgXkO
[¿¼ÑÐ] 297Çóµ÷¼Á +3 ϲ»¶»¹ÊDz»¸ÊÐÄ 2026-03-20 3/150 2026-03-21 18:33 by ѧԱ8dgXkO
[¿¼ÑÐ] 313Çóµ÷¼Á +4 ËÁÈþ·¡Ò¼22 2026-03-19 4/200 2026-03-21 17:33 by ColorlessPI
[¿¼ÑÐ] ²ÄÁÏѧѧ˶080502 337Çóµ÷¼Á-Ò»Ö¾Ô¸»ªÖпƼ¼´óѧ +4 ˳˳˳mr 2026-03-18 5/250 2026-03-21 10:22 by luoyongfeng
[¿¼ÑÐ] 301Çóµ÷¼Á +10 yyÒªÉϰ¶Ñ½ 2026-03-17 10/500 2026-03-21 03:14 by JourneyLucky
[¿¼ÑÐ] Ò»Ö¾Ô¸»ªÄÏʦ´ó 070300£¨»¯Ñ§£©304·ÖÇóµ÷¼Á +3 0703ÎäÜ·»ÛÑ©304 2026-03-18 3/150 2026-03-21 00:48 by JourneyLucky
[¿¼ÑÐ] 294Çóµ÷¼Á²ÄÁÏÓ뻯¹¤×¨Ë¶ +15 ݤÎÉ­ÁÖ 2026-03-18 15/750 2026-03-20 23:28 by JourneyLucky
[¿¼ÑÐ] 317Çóµ÷¼Á +5 Éê×ÓÉêÉê 2026-03-19 9/450 2026-03-20 22:26 by JourneyLucky
[¿¼ÑÐ] 0817 »¯Ñ§¹¤³Ì 299·ÖÇóµ÷¼Á ÓпÆÑо­Àú ÓжþÇøÎÄÕ +22 rare12345 2026-03-18 22/1100 2026-03-20 20:39 by zhukairuo
[¿¼ÑÐ] Çóµ÷¼Á +3 eation27 2026-03-20 3/150 2026-03-20 19:32 by JourneyLucky
[¿¼ÑÐ] Ò»Ö¾Ô¸Öйúº£Ñó´óѧ£¬ÉúÎïѧ£¬301·Ö£¬Çóµ÷¼Á +5 1ËïÎò¿Õ 2026-03-17 6/300 2026-03-19 23:46 by zcl123
[¿¼ÑÐ] 085601²ÄÁϹ¤³Ìר˶Çóµ÷¼Á +10 Ľº®mio 2026-03-16 10/500 2026-03-19 15:26 by ¶¡¶¡*
[¿¼ÑÐ] ²ÄÁϹ¤³Ìר˶µ÷¼Á +5 204818@lcx 2026-03-17 6/300 2026-03-18 22:55 by 204818@lcx
[¿¼ÑÐ] 344Çóµ÷¼Á +6 knight344 2026-03-16 7/350 2026-03-18 20:13 by walc
[¿¼ÑÐ] 326Çóµ÷¼Á +5 Éϰ¶µÄСÆÏ 2026-03-15 6/300 2026-03-17 17:26 by ruiyingmiao
[¿¼ÑÐ] »úеר˶325£¬Ñ°ÕÒµ÷¼ÁԺУ +3 y9999 2026-03-15 5/250 2026-03-16 19:58 by y9999
[¿¼ÑÐ] 327Çóµ÷¼Á +6 ʰ¹âÈÎȾ 2026-03-15 11/550 2026-03-15 22:47 by ʰ¹âÈÎȾ
ÐÅÏ¢Ìáʾ
ÇëÌî´¦ÀíÒâ¼û