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tingting7673

铜虫 (初入文坛)

[求助] 审稿意见里晶体学数据问题 已有1人参与

文章审稿意见回来啦,晶体学数据问题,求助各位高手大侠:

审稿意见:We see from the CIF that there are 2 Uiso/Uij restrained atom sites, 7 distance or angle restraints and 20 least-squares restraints  used in the refinement.   So that the reader can be  fully aware of what was done to generate the reported models,  we should be told - at least in the "_refine_special_details" section of the CIF or in an ESI text  - exactly what these restraints were and why they were necessary.   [An easy way to show what restraints were employed(but not why they were needed) is to include the relevant lines from the SHELXL.ins file in the  "_refine_special_details" section of the CIF.  This should now be done.]

好像是说ins文件里的几处限定需要在cif文件中refine_special_details 后面写出是什么限定以及为什么这么做,我的ins文件中的限定主要有这几个地方:

dfix 0.95 0.02 o10 h1a o10 h1b
dfix 1.55 0.02 h1a h1b
dfix 3.00 0.02 k1 h1a k1 h1b
isor 0.001 0.001 o11 O11'
dfix 0.85 0.01 o9 h99
dfix 0.85 0.01 o9 h98
dfix 1.39 0.01 h99 h98

各位高手能不能告诉我怎么写啊,万分感谢中啊!
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xi2004

至尊木虫 (职业作家)

直接把.res的hklf4 end上面的内容拷贝到cif中。
xi2004-emuch@163.com
4楼2014-06-03 18:01:16
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