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The Data/Parameter ratio for this structure is 4.86, which is below the generous RSC cut-off value of 5. Õâ¸öÊý¾Ý´ÓÄÄÀïµÃÀ´£¿
The number of restraints is reported as 647. I am very curious as to why so many are suddenly needed,Õâ¸öÊý¾Ý´ÓÄÄÀïÀ´£¿
The number of restraints is reported as 6, Õâ¸öÊý¾ÝÀ´×Ժ䦣¿ÕâҲ̫רҵÁË£¡
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The authors have applied squeeze to this model, which has improved the R-factors and the structure generally. The values for the density, F and mu  need to be adjusted to take account of the new chemical formula. The presence of the solvent water should really be corroborated by using another (non-crystallographic) method such as TGA or DSC.
Coverage is reported as 25.10, which satisfies the requirements, but the the completeness is reported as 0.973, which is too low.
The Data/Parameter ratio for this structure is 4.86, which is below the generous RSC cut-off value of 5.
The number of restraints is reported as 647. I am very curious as to why so many are suddenly needed, when the previously submitted structure has none, and the model itself has not changed much? I would suggest that most of these restraints are unnecessary.
Structure scw762s (CCDC 1041245): C30 H38 Cl4 Cu N6 O5
Thank you for recollecting the data for this structure.
Coverage is reported as 25.00, which satisfies the requirements, but the the completeness is reported as 0.952, which is too low. Please give a reason for this, and bear this in mind for future collections.
The number of restraints is reported as 6, but no details about these restraints were given in the _refine_special_details section of the cif file. This information can also be provided by making use of the restraint CIF dictionary items. This is not a RSC requirement, however please consider adding all information about restraints and constraints to the cif - this makes the file much more useful for future readers.
C11, C12 and C14 are probably disordered, by looking the shape of the thermal ellipsoids. Please comment if any attempt was made to model this.
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5. squeezeÃüÁîÓÃÁËÖ®ºóȷʵÐèÒªÆäËûÊֶαÈÈçDSC¡¢TG»òÕßÔªËØ·ÖÎöÀ´È·¶¨ÄãsqueezeµôµÄµ½µØÊÇʲô£¬¼Ó½øÈ¥ÖØÐÂË㻯ѧʽ
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