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[求助]
做GPC图谱时纵坐标的Mv代表什么已有3人参与
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求各位高人指点，我是新接触高分子研究的，在绘制GPC流出曲线时，横坐标是留出时间，纵坐标是Mv，可是我从GPC仪器上导出的TXT文档里面没有直接的Mv这个数值，希望各位有识之士，可以帮忙指点一下。谢谢了。纵坐标除了是Mv可以做，其它别的值可以当作纵坐标做图吗？还有就是这几个字母分别代表什么意思rid1A/ELU rid1A/MMD Cum.Dist./MMD？真心希望有人可以耐心讲解，谢谢。 以下是我样品测出的GPC数据 Sample : 2# Inject date : Wednesday 04/15/15 10:43:08 Inject volume : 50.000 ul Concentration : 1.000 g/l Project : C:\HPCHEM\1\DATA\20150415\20150402.D\rid10 Calibration : ps2013.CAL Export file : C:\Documents and Settings\jzh\Desktop\Default.txt Operator : zxs Account : Calibration MH-K : 1.000000 ml/g univ. Calibration MH-K : 0.000000 ml/g Calibration MH-A : 0.000000 - univ. Calibration MH-A : 0.000000 - Internal Standard Calibration : 50.000 ml Internal Standard Acquisition : ------- ml Data Interval : 0.430 s Eluent : THF Flow : 1.000 ml/min Column 1 : ....? Temperature : 23.000 C Detector 1 : rid1A Delay : 0.000 ml Baseline from : 6.488 to : 8.167 min Integration from : 6.488 to : 8.167 min rid1A Mn: 1.536E+4 g/mol Mw: 2.454E+4 g/mol Mz: 3.612E+4 g/mol Mv: 0.000E+0 g/mol D: 1.598E+0 [n]: 0.000E+0 ml/g Vp: 7.229E+0 ml Mp: 2.291E+4 g/mol A: 7.809E+3 ml*V 10% : 7.7087e3 g/mol 30% : 1.3569e4 g/mol 50% : 2.0202e4 g/mol 70% : 2.9318e4 g/mol 90% : 4.7335e4 g/mol Agilent slice report start : Slice No. Retention time Molar mass log(Molar mass) rid1A/ELU rid1A/MMD Cum.Dist./MMD 1.00000E+0 6.48799E+0 1.28775E+5 5.10983E+0 0.00000E+0 0.00000E+0 1.00000E+2 2.00000E+0 6.49513E+0 1.26669E+5 5.10267E+0 1.32570E+1 1.69335E-3 9.99993E+1 3.00000E+0 6.50228E+0 1.24597E+5 5.09551E+0 2.79481E+1 3.56877E-3 9.99975E+1 4.00000E+0 6.50942E+0 1.22558E+5 5.08834E+0 4.40337E+1 5.62097E-3 9.99942E+1 5.00000E+0 6.51656E+0 1.20552E+5 5.08117E+0 6.10056E+1 7.78497E-3 9.99894E+1 6.00000E+0 6.52371E+0 1.18578E+5 5.07400E+0 7.96836E+1 1.01652E-2 9.99829E+1 7.00000E+0 6.53085E+0 1.16635E+5 5.06683E+0 9.96807E+1 1.27122E-2 9.99747E+1 8.00000E+0 6.53800E+0 1.14724E+5 5.05966E+0 1.21224E+2 1.54548E-2 9.99646E+1 9.00000E+0 6.54514E+0 1.12844E+5 5.05248E+0 1.44376E+2 1.84007E-2 9.99525E+1 1.00000E+1 6.55228E+0 1.10994E+5 5.04530E+0 1.68861E+2 2.15147E-2 9.99382E+1 1.10000E+1 6.55943E+0 1.09174E+5 5.03812E+0 1.96113E+2 2.49793E-2 9.99215E+1 1.20000E+1 6.56657E+0 1.07383E+5 5.03093E+0 2.25558E+2 2.87211E-2 9.99022E+1 1.30000E+1 6.57372E+0 1.05621E+5 5.02375E+0 2.57399E+2 3.27658E-2 9.98801E+1 1.40000E+1 6.58086E+0 1.03887E+5 5.01656E+0 2.91671E+2 3.71177E-2 9.98550E+1 1.50000E+1 6.58800E+0 1.02181E+5 5.00937E+0 3.27503E+2 4.16656E-2 9.98267E+1 1.60000E+1 6.59515E+0 1.00503E+5 5.00218E+0 3.66777E+2 4.66487E-2 9.97950E+1 1.70000E+1 6.60229E+0 9.88517E+4 4.99498E+0 4.08605E+2 5.19539E-2 9.97595E+1 1.80000E+1 6.60943E+0 9.72272E+4 4.98779E+0 4.53007E+2 5.75835E-2 9.97201E+1 1.90000E+1 6.61658E+0 9.56290E+4 4.98059E+0 5.00021E+2 6.35423E-2 9.96765E+1 2.00000E+1 6.62372E+0 9.40567E+4 4.97339E+0 5.48566E+2 6.96925E-2 9.96285E+1 2.10000E+1 6.63087E+0 9.25098E+4 4.96619E+0 6.00981E+2 7.63313E-2 9.95759E+1 2.20000E+1 6.63801E+0 9.09879E+4 4.95898E+0 6.56283E+2 8.33335E-2 9.95183E+1 2.30000E+1 6.64515E+0 8.94907E+4 4.95178E+0 7.14523E+2 9.07053E-2 9.94556E+1 2.40000E+1 6.65230E+0 8.80177E+4 4.94457E+0 7.75864E+2 9.84675E-2 9.93874E+1 2.50000E+1 6.65944E+0 8.65686E+4 4.93736E+0 8.38944E+2 1.06447E-1 9.93135E+1 2.60000E+1 6.66659E+0 8.51431E+4 4.93015E+0 9.06578E+2 1.15000E-1 9.92337E+1 2.70000E+1 6.67373E+0 8.37407E+4 4.92294E+0 9.77804E+2 1.24006E-1 9.91475E+1 2.80000E+1 6.68087E+0 8.23610E+4 4.91572E+0 1.05257E+3 1.33457E-1 9.90546E+1 2.90000E+1 6.68802E+0 8.10038E+4 4.90851E+0 1.13104E+3 1.43373E-1 9.89547E+1 3.00000E+1 6.69516E+0 7.96686E+4 4.90129E+0 1.21144E+3 1.53530E-1 9.88474E+1 3.10000E+1 6.70231E+0 7.83552E+4 4.89407E+0 1.29716E+3 1.64357E-1 9.87327E+1 3.20000E+1 6.70945E+0 7.70631E+4 4.88685E+0 1.38688E+3 1.75688E-1 9.86099E+1 3.30000E+1 6.71659E+0 7.57921E+4 4.87962E+0 1.48046E+3 1.87502E-1 9.84787E+1 3.40000E+1 6.72374E+0 7.45417E+4 4.87240E+0 1.57793E+3 1.99805E-1 9.83388E+1 3.50000E+1 6.73088E+0 7.33118E+4 4.86517E+0 1.67703E+3 2.12312E-1 9.81898E+1 3.60000E+1 6.73803E+0 7.21019E+4 4.85795E+0 1.78148E+3 2.25490E-1 9.80316E+1 3.70000E+1 6.74517E+0 7.09117E+4 4.85072E+0 1.89010E+3 2.39193E-1 9.78637E+1 3.80000E+1 6.75231E+0 6.97410E+4 4.84349E+0 2.00231E+3 2.53346E-1 9.76856E+1 3.90000E+1 6.75946E+0 6.85894E+4 4.83626E+0 2.11815E+3 2.67955E-1 9.74971E+1 4.00000E+1 6.76660E+0 6.74566E+4 4.82902E+0 2.23532E+3 2.82727E-1 9.72979E+1 4.10000E+1 6.77375E+0 6.63423E+4 4.82179E+0 2.35775E+3 2.98161E-1 9.70878E+1 4.20000E+1 6.78089E+0 6.52463E+4 4.81456E+0 2.48437E+3 3.14122E-1 9.68663E+1 4.30000E+1 6.78803E+0 6.41682E+4 4.80732E+0 2.61456E+3 3.30530E-1 9.66330E+1 4.40000E+1 6.79518E+0 6.31077E+4 4.80008E+0 2.74826E+3 3.47376E-1 9.63877E+1 4.50000E+1 6.80232E+0 6.20646E+4 4.79284E+0 2.88285E+3 3.64333E-1 9.61300E+1 4.60000E+1 6.80947E+0 6.10386E+4 4.78560E+0 3.02264E+3 3.81944E-1 9.58599E+1 4.70000E+1 6.81661E+0 6.00293E+4 4.77836E+0 3.16646E+3 4.00061E-1 9.55767E+1 4.80000E+1 6.82375E+0 5.90367E+4 4.77112E+0 3.31342E+3 4.18571E-1 9.52803E+1 4.90000E+1 6.83090E+0 5.80603E+4 4.76388E+0 3.46345E+3 4.37466E-1 9.49703E+1 5.00000E+1 6.83804E+0 5.71000E+4 4.75664E+0 3.61365E+3 4.56379E-1 9.46465E+1 5.10000E+1 6.84518E+0 5.61554E+4 4.74939E+0 3.76823E+3 4.75844E-1 9.43088E+1 5.20000E+1 6.85233E+0 5.52263E+4 4.74215E+0 3.92628E+3 4.95744E-1 9.39568E+1 5.30000E+1 6.85947E+0 5.43126E+4 4.73490E+0 4.08661E+3 5.15930E-1 9.35903E+1 5.40000E+1 6.86662E+0 5.34138E+4 4.72765E+0 4.24903E+3 5.36377E-1 9.32090E+1 5.50000E+1 6.87376E+0 5.25298E+4 4.72041E+0 4.41049E+3 5.56703E-1 9.28127E+1 5.60000E+1 6.88090E+0 5.16603E+4 4.71316E+0 4.57496E+3 5.77405E-1 9.24018E+1 5.70000E+1 6.88805E+0 5.08052E+4 4.70591E+0 4.74193E+3 5.98423E-1 9.19756E+1 5.80000E+1 6.89519E+0 4.99641E+4 4.69866E+0 4.90989E+3 6.19564E-1 9.15341E+1 5.90000E+1 6.90234E+0 4.91369E+4 4.69141E+0 5.07862E+3 6.40802E-1 9.10771E+1 6.00000E+1 6.90948E+0 4.83234E+4 4.68416E+0 5.24518E+3 6.61766E-1 9.06048E+1 6.10000E+1 6.91662E+0 4.75232E+4 4.67691E+0 5.41324E+3 6.82918E-1 9.01173E+1 6.20000E+1 6.92377E+0 4.67362E+4 4.66965E+0 5.58267E+3 7.04243E-1 8.96143E+1 6.30000E+1 6.93091E+0 4.59622E+4 4.66240E+0 5.75178E+3 7.25529E-1 8.90958E+1 6.40000E+1 6.93806E+0 4.52010E+4 4.65515E+0 5.92035E+3 7.46747E-1 8.85619E+1 6.50000E+1 6.94520E+0 4.44523E+4 4.64789E+0 6.08558E+3 7.67544E-1 8.80126E+1 6.60000E+1 6.95234E+0 4.37160E+4 4.64064E+0 6.25064E+3 7.88320E-1 8.74483E+1 6.70000E+1 6.95949E+0 4.29919E+4 4.63339E+0 6.41585E+3 8.09117E-1 8.68689E+1 6.80000E+1 6.96663E+0 4.22797E+4 4.62613E+0 6.57936E+3 8.29701E-1 8.62745E+1 6.90000E+1 6.97378E+0 4.15793E+4 4.61888E+0 6.74096E+3 8.50045E-1 8.56652E+1 7.00000E+1 6.98092E+0 4.08905E+4 4.61162E+0 6.89822E+3 8.69845E-1 8.50412E+1 7.10000E+1 6.98806E+0 4.02130E+4 4.60437E+0 7.05382E+3 8.89436E-1 8.44030E+1 7.20000E+1 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8.10966E+0 2.81575E+3 3.44959E+0 1.97122E+2 2.30035E-2 6.82091E-2 2.29000E+2 8.11681E+0 2.76533E+3 3.44175E+0 1.68451E+2 1.96168E-2 5.14840E-2 2.30000E+2 8.12395E+0 2.71570E+3 3.43388E+0 1.41018E+2 1.63873E-2 3.73252E-2 2.31000E+2 8.13109E+0 2.66685E+3 3.42600E+0 1.14932E+2 1.33273E-2 2.56237E-2 2.32000E+2 8.13824E+0 2.61879E+3 3.41810E+0 9.01242E+1 1.04278E-2 1.62228E-2 2.33000E+2 8.14538E+0 2.57148E+3 3.41018E+0 6.60516E+1 7.62565E-3 9.07617E-3 2.34000E+2 8.15253E+0 2.52493E+3 3.40225E+0 4.30124E+1 4.95488E-3 4.08469E-3 2.35000E+2 8.15967E+0 2.47911E+3 3.39430E+0 2.09763E+1 2.41141E-3 1.15516E-3 2.36000E+2 8.16681E+0 2.43403E+3 3.38633E+0 3.53577E-10 4.05403E-14 4.86164E-15 Agilent slice report end : |
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