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[交流] 高分子固化程度的测定与DSC图谱分析

这是审稿专家的原话如下:
Any residual heat of reaction. The manuscript does not show the degree of completion of the reaction. It is very important to achieve high reaction conversion because any unreacted functional groups in the polymeric network have potential to alter the material properties (modulus, adhesion, refractive index, etc.) later once they have chance to resume reaction. It is highly recommended to include DSC analysis. For instance, 1st temperature scan showing the heat of reaction and followed by 2nd temp. scan to verify any residual heat of reaction.
想请教下大家:DSC如何测定固化程度?实验该如何设置?图谱数据该如何处理?谢谢!
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