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20120931546

新虫 (初入文坛)

应助: 0 (幼儿园)
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虫号: 1974148
注册: 2012-09-04
专业: 中药制剂

[求助] 三个化合物，请哪位大侠帮忙鉴定一下，急求，谢谢！拜托了！非常感谢！已有1人参与

1. 碳谱数据（溶剂为氘代甲醇）为：
48.49，48.66，48.83，49.00，49.17，49.34，49.51，62.50，71.17，75.70，78.08，78.38，94.68，99.85，104.23，105.66，115.97，117.52，123.04，123.18，135.58，145.89，149.83，158.43，158.97，163.03，165.98，179.47

2.碳谱数据（溶剂为氘代甲醇）为：
17.89，48.49，48.66，48.83，49.00，49.17，49.34，49.51，68.53，69.70，71.36，72.08，72.20，73.90，75.71，77.18，78.15，94.84，99.92，102.41，104.70，105.60，116.03，117.66，123.08，123.54，135.61，145.83，149.80，158.49，159.32，162.97，166.01，179.40

3.碳谱数据（溶剂为氘代氯仿）为：
13.71，14.12，19.13，22.68，25.01，27.19，29.14，29.26，29.31，29.35，29.45，29.58，29.64，29.68，29.76，30.67，31.91，34.40，64.09，76.74，76.99，77.25，174.06

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seuseasoar

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11
1 .    quercetin 3-O-β-D-glucopyranosyl-(1→6)-β-D-glucopyranoside
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The Chinese Pharmaceutical Journal       2004       56       17-23
Chemical Constituents from The Leaves of Mahonia japonica
Tian-Jye Hsieh, Yang-Chang Wu, Wen-Li Lo, Su-Ching Chen, Shih-Hsien Kuo and Chung-Yi Chen
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
2 .    quercetin 3-rutinoside
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Phytochemistry       2003                229-237
Malonylated flavonol glycosides from the petals of Clitoria ternatea
Kohei Kazuma, Naonobu Noda, Masahiko Suzuki
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
3 .    rutin
相似度:71.4%
Planta Medica       1990       56       413-415
Flavonoid Glycosides and Other Hydrophilic Compounds from Flowers of Heterotheca inuloides
Christianeierga,JrrngardMerfort, and Günter Willuhn
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
4 .    Rutin
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Chemistry of Natural Compounds       2004       40       457-459
A NEW HYDROQUINONE DIGLUCOSIDE FROM Lysimachia fordiana
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5 .    rutin
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Acta Botanica Sinica       2004       46       618-620
Chemical Constituents of Smilax perfoliata
CHENG Yu-Biao, ZHANG Dong-Ming, YU Shi-Shan
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
6 .    Quercetin 3-O-β-D-rutinoside
C27H30O16    相似度:71.4%
Molecules       2008       13       1931-1941
Flavonoids and a New Polyacetylene from Bidens parviflora Willd
Yu-Lan Li, Jun Li, Nai-Li Wang and Xin-Sheng Yao
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
22
1 .    quercetin-3-O-[2-O-β-xylopyranosyl-6-O-α-rhamnopyranosyl]-β-glucopyranoside
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Planta Medica       2001       67       345-349
Alkaloids and Flavonoids from Peanut Skins
Hongxiang Lou,Huiqing Yuan, Yoshimitsu Yamazaki, Tsutomu Sasaki, Syuichi Oka
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
2 .    quercetin 3-O-β-glucopyranosyl(1→2)[α-rhamnopyranosyl(1→6)]-β-glucopyranoside
相似度:79.4%
Phytochemistry       2009       70       785-794
Flavonol tetraglycosides from fruits of Styphnolobium japonicum (Leguminosae) and the authentication of Fructus Sophorae and Flos Sophorae
Geoffrey C. Kite, Nigel C. Veitch, Martha E. Boalch, Gwilym P. Lewis, Christine J. Leon, Monique S.J. Simmonds
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3 .    quercetin-3-O-α-L-rhamnopyranosyl-(1→6)-β-D-glucopyranosyl-(1→3)-β-D-glucopyranoside
C33H40O21    相似度:79.4%
Journal of Asian Natural Products Research       2009       11       79-84
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Lu-Rong Xuac, Pei Zhoua,Yue-E Zhia, Jun Wub and Si Zhangb
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
4 .    quercetin glucosylrhamnosylgalactoside
相似度:79.4%
Phytochemistry       1991       30       2057-2060
Flavonol triglycosides containing galactose in tea
Andreas Finger, Ulrich H. Engelhardt, Victor Wray
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
5 .    quercetin-3-O-[β-D-glucopyranosyl-(1-3)-α-L-rhamnopyranosyl-(1-6)-β-D-galactopyranoside]
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Bioscience, Biotechnology, and Biochemistry       2000       64       2262-2265
Glycosidic Flavonoids as Rat-Liver Injury Preventing Compounds from Green Tea
Shingo WADA, Puming HE, Ikue HASHIMOTO, Naoharu WATANABE, Kimio SUGIYAMA
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
6 .    quercetin-3-O-glucoside-7-O-rutinoside
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33
1 .    10,12-Heptadecadiynoic acid
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Paulo T. Hennies, Maria H. C. Santana and Carlos R. D. Correia
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
2 .    solamin
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Hidefumi Makabe, Asuka Kuwabara, Yasunao Hattori, and Hiroyuki Konno
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
3 .    n-Octacos-9-enyl propionate
C31H60O2    相似度:78.2%
Chinese Journal of Chemistry       2007       25       843-848
New Aliphatic Alcohol and Ester Constituents from Rice Hulls of Oryza sativa
ILL-Min Chung, Mohd Ali, Se-Chul Chun, Cheng-Wu Jin, Dong-Ha Cho, Seung-Beom Hong and Ateeque Ahmad
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
4 .    (15S,16S)-15-methoxy-16-methyltetratriacontyl pivalate
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Tetrahedron       2013       69       6285-6296
The synthesis of methoxy and keto mycolic acids containing methyl-trans-cyclopropanes
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6 .    10,12-Tricosadiynoic acid
相似度:78.2%
Journal of the Brazilian Chemical Society       2001       12       64-72
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