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fengzhou85银虫 (小有名气)
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[求助]
求助如何修改审稿人的意见
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第一篇英文，三个审稿人，大修。其中两个人的意见是修改引言，结论，摘要，不涉及到具体内容。但是另外一个审稿人的意见非常具体，还提到要求补做实验。但是老板认为不需要（相关参考文献中也没有采用这种实验方法进行分析的），大家帮忙看看，提点意见给我，先谢谢了。 具体的修改意见为： The part for the TG-DSC analysis must be rewritten again, since there are several misunderstandings. In the case of simultaneous measurement of DSC and TG, two different effects can be observed from the DSC signal, in the degradation area of the studied sample. The first one is the decomposition of the sample which is always an exothermic event for a DSC measurement and the second one is the mass loss due to the decomposition which is an endothermic effect. The DSC signal in this case will present a plateau or an endothermic/exothermic peak since the final signal is the sum of the exothermic phenomenon due to the decomposition, and the endothermic one due to the mass loss of the sample. The shape depends on the enthalpy of the two events. In addition, two steps of mass loss have been recorded for the samples under study. The first one can be found in the area of 30 - 200 C, with one step of mass loss for the samples RSF and ALK-SF and two overlapped mass loss steps for the other samples. The author must discuss this difference while taking into account that no direct information can be obtained about the part of the sample that decomposes, from the TG measurements. The samples must be studied with TG-MS or other techniques in order to be sure about the decomposition scheme. The second area of mass loss is among 200 – 400 C, during which two overlapped decomposition steps are obvious. This is more obvious from the DTG figure. For this area also other techniques must be used for the determination of the decomposition scheme. Using the above comments the possibility of the silane grafting must be discussed. |
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fengzhou85
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关键是这个审稿人的意见，我也不是很明白，下面我简要的分析一下，希望大家帮忙看看我分析的对不对，谢谢！ In the case of simultaneous measurement of DSC and TG, two different effects can be observed from the DSC signal, in the degradation area of the studied sample. The first one is the decomposition of the sample which is always an exothermic event for a DSC measurement and the second one is the mass loss due to the decomposition which is an endothermic effect. The DSC signal in this case will present a plateau or an endothermic/exothermic peak since the final signal is the sum of the exothermic phenomenon due to the decomposition, and the endothermic one due to the mass loss of the sample. The shape depends on the enthalpy of the two events. （好像是说了一下样品分解，DSC曲线显示的放热效应；分解引起的质量损失会造成DSC显示吸热效应，这些内容好像与本文的具体内容没有关系？） In addition, two steps of mass loss have been recorded for the samples under study. The first one can be found in the area of 30 - 200 C, with one step of mass loss for the samples RSF and ALK-SF and two overlapped mass loss steps for the other samples. The author must discuss this difference while taking into account that no direct information can be obtained about the part of the sample that decomposes, from the TG measurements.（这个问题我的理解是：讨论DSC曲线不同的原因） The samples must be studied with TG-MS or other techniques in order to be sure about the decomposition scheme. The second area of mass loss is among 200 – 400 C, during which two overlapped decomposition steps are obvious. This is more obvious from the DTG figure. For this area also other techniques must be used for the determination of the decomposition scheme. Using the above comments the possibility of the silane grafting must be discussed.（要想获得分解反应，必须要补做试验） 所以，这个审稿人的具体意见是不是修改后面两个问题？ |
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ll9999
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9楼2013-01-06 16:31:51
fengzhou85
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10楼2013-01-06 16:35:13
