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1) There are some reflections which may be obscured by the beam stop.
See the list of most disagreeable reflections. These should be omitted using the OMIT instruction. Then the weighting scheme should be optimized and wR2 will drop to approximately 0.15.
2) Check the cell e.s.d.'s. Are these values really from the diffractometer or from XPREP?
3) The abstract should contain more information, e.g. the two molecules in the asymmetric unit. Please see the notes for authors for how to write an abstract.
4) You write that the H atoms were visible in a difference map. When I calculate a diff. map I can hardly see a few. Correct _publ_section_exptl_refinement accordingly.
5) C24...O2 is definitely not a C-H...O hydrogen bond.
6 Fig. 1: atom labels should not be written over bonds (C18) or atoms (N2, C20).
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sygdcbs: ½ð±Ò+2, ¡ï¡ï¡ïºÜÓаïÖú, ·Ç³£¸Ðл£¬Äܲ»Äܸø¸öqqºÅ»òÕßÓʼþ£¬·½±ãÇë½Ì 2012-12-01 11:40:56
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1) There are some reflections which may be obscured by the beam stop.
See the list of most disagreeable reflections. These should be omitted using the OMIT instruction. Then the weighting scheme should be optimized and wR2 will drop to approximately 0.15.
½ÐÄã°Ñ±»beam stopµ²×¡¶øÇ¿¶È¹ýµÍµÄµãɾµô£¬ÄãҪû¸ÅÄ²»·Á·¢Êý¾ÝÉÏÀ´£¬ÎÒ¸øÄã¿´¿´¡£

2) Check the cell e.s.d.'s. Are these values really from the diffractometer or from XPREP?
È·ÈÏһϾ§°ûµÄesd»ò½ÐsuÊǾ«Ð޵Ľá¹û£¬Ò²¾ÍÊǸúp4pÎļþÀïµÄÒ»Ñù£¬¶ø²»ÊÇÊÖ¶¯Êäµ½xprepÀïµÄ£¬Ã»É¶ÄѶȡ£

3) The abstract should contain more information, e.g. the two molecules in the asymmetric unit. Please see the notes for authors for how to write an abstract.
ÕªÒªÒª¸ü·áÂúһЩ¡£

4) You write that the H atoms were visible in a difference map. When I calculate a diff. map I can hardly see a few. Correct _publ_section_exptl_refinement accordingly.
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5) C24...O2 is definitely not a C-H...O hydrogen bond.
Õâ¸ö²»ÊÇÇâ¼ü£¬Òª´ÓÇâ¼üÁбíÖÐɾµô¡£

6 Fig. 1: atom labels should not be written over bonds (C18) or atoms (N2, C20).
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What_we_observe_is_not_nature_itself,_but_nature_exposed_to_our_method_of_questioning----Werner_Karl_Heisenberg
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