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kulumisa

银虫 (初入文坛)

[求助] 油酸铟前驱体如何合成 已有2人参与

哪位大神有合成油酸铟前驱体的方法,请详细指点啊,急急急急急急急
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kulumisa

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引用回帖:
2楼: Originally posted by bullbilly at 2015-04-07 11:56:03
Into the mixture of 80.0 mL of deionized water and 10.0 mL of anhydrous ethanol was dissolved 9.16 g (30.0 mmol) of sodium oleate at 80 °C under stirring to give a light yellow solution (A). A 1.96  ...

谢谢您啦,一切顺利

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5楼2017-02-07 22:54:49
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bullbilly

木虫 (知名作家)

【答案】应助回帖

感谢参与,应助指数 +1
Into the mixture of 80.0 mL of deionized water and 10.0 mL of anhydrous ethanol was dissolved 9.16 g (30.0 mmol) of sodium oleate at 80 °C under stirring to give a light yellow solution (A). A 1.96 g (10.0 mmol) portion of InCl3·4H2O was dissolved into the mixture of 10.0 mL of deionized water and 4 mL of anhydrous ethanol to form a colorless solution (B). Solution B was slowly added to solution A to produce the opalescent precipitate. The precipitate was washed with deionized water several times and dried at 60 °C in air for 30 min and then at 75 °C in vacuum for 24 h to give brown stick powders

J. Phys. Chem. C, 2007, 111 (49), pp 18039–18043.
2楼2015-04-07 11:56:03
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wws19851024

铜虫 (小有名气)

【答案】应助回帖

感谢参与,应助指数 +1
可以参考油酸铁的合成吧,没有做过,只是建议。。。
3楼2015-04-07 15:59:45
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kulumisa

银虫 (初入文坛)

引用回帖:
3楼: Originally posted by wws19851024 at 2015-04-07 15:59:45
可以参考油酸铁的合成吧,没有做过,只是建议。。。

谢谢您,哈哈

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4楼2017-02-07 22:54:01
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