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急求硝酸铵标准PDF卡片！！！已有1人参与
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感谢参与，应助指数 +1
板青: 金币+50, ★★★★★最佳答案 2015-01-04 09:55:53
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有很多种晶相，但常温下晶相选第4个： 1. Card Information Names: Ammonium Nitrate Formula: N H4 N O3 PDF Number: 47-864 Quality: star Subfiles: inorganic Cell and Symmetry Information System: cubic Space Group: (no. 0) a: 4.358 Density (Dx): 1.606 Z: 1 Instrument Information Radiation: CuKa1 Wavelength: 1.54056 Instrument(d): diffractometer Instrument(I): diffractometer I type: unknown Comments and Additional Information Temperature: Pattern taken at 131 C. General: Pattern for the same specimen at 23 C used in data refinement as the external standard. Source: Ammonium nitrate 99.999% supplied by Aldrich Chemical Co., Lot No. 14012TW. Analysis: Analysis (wt.%): N O3 75.8 (with Nitron); Si 6.0 ppm, Mg 4.0 ppm, Fe 2.0 ppm, Na 2.0 ppm, Ti 0.5 ppm. General: No reflections with relative intensity equal to or greater than 1 observed for d<2.18. General: Form I. Literature References General: Heyding, R., Queen's Univ., Kingston,Ontario, Canada. Private Communication (1995) Unit Cell: Wyckoff, R. The Structure of Crystals, 2nd ed. 2 368 ( ) Peak Data PeakList 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 20.356 4.3590 95.0 ( 1 0 0) 10.178 0.1147 1.4414 1 28.966 3.0800 100.0 ( 1 1 0) 14.483 0.1623 2.0400 2 35.640 2.5170 2.0 ( 1 1 1) 17.820 0.1986 2.4963 3 41.403 2.1790 13.0 ( 2 0 0) 20.702 0.2295 2.8835 4 2. Card Information Names: Ammonium Nitrate Formula: N H4 N O3 PDF Number: 47-865 Quality: indexed Subfiles: inorganic Cell and Symmetry Information System: tetragonal Space Group: P4bm (no. 100) a: 5.706 c: 4.916 Density (Dx): 1.660 Z: 2 Instrument Information Radiation: CuKa1 Wavelength: 1.54056 Instrument(d): diffractometer Instrument(I): diffractometer I type: unknown Comments and Additional Information Temperature: Pattern taken at 90 C. General: Pattern for the same specimen at 23 C used in data refinement as the external standard. Source: Ammonium nitrate 99.999% supplied by Aldrich Chemical Co., Lot No. 14012TW. Analysis: Analysis (wt.%): N O3 75.8 (with Nitron); Si 6.0 ppm, Mg 4.0 ppm, Fe 2.0 ppm, Na 2.0 ppm, Ti 0.5 ppm. General: No reflections with relative intensity equal to or greater than 1 observed for d<1.58. General: Form II. Literature References General: Heyding, R., Queen's Univ., Kingston,Ontario, Canada. Private Communication (1995) Unit Cell: Wyckoff, R. The Structure of Crystals, 2nd ed. 2 369 ( ) Peak Data PeakList 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 16.900 5.2420 12.0 ( 1 1 0) 8.450 0.0954 1.1986 19.606 4.5240 14.0 ( 1 0 1) 9.803 0.1105 1.3889 22.777 3.9010 60.0 ( 1 1 1) 11.388 0.1282 1.6107 26.236 3.3940 49.0 ( 1 2 0) 13.118 0.1473 1.8513 27.446 3.2470 22.0 ( 2 1 0) 13.723 0.1540 1.9351 27.698 3.2180 100.0 ( 0 2 1) 13.849 0.1554 1.9525 30.484 2.9300 12.0 ( 1 2 1) 15.242 0.1706 2.1444 30.601 2.9190 16.0 ( 0 0 2) 15.301 0.1713 2.1525 31.509 2.8370 9.0 ( 2 1 1) 15.754 0.1762 2.2147 34.155 2.6230 30.0 ( 2 2 0) 17.077 0.1906 2.3954 35.164 2.5500 6.0 ( 1 1 2) 17.582 0.1961 2.4640 37.136 2.4190 43.0 ( 1 3 0) 18.568 0.2067 2.5974 38.661 2.3270 43.0 ( 0 2 2) 19.331 0.2149 2.7001 39.818 2.2620 16.0 ( 2 0 2) 19.909 0.2210 2.7777 40.320 2.2350 3.0 ( 1 3 1) 20.160 0.2237 2.8113 40.758 2.2120 9.0 ( 1 2 2) 20.379 0.2260 2.8405 47.123 1.9270 3.0 ( 0 4 0) 23.561 0.2595 3.2606 47.410 1.9160 3.0 ( 3 2 1) 23.705 0.2610 3.2793 49.960 1.8240 7.0 ( 1 1 3) 24.980 0.2741 3.4447 51.501 1.7730 4.0 ( 1 4 1) 25.750 0.2820 3.5438 56.402 1.6300 4.0 ( 2 4 1) 28.201 0.3067 3.8547 3. Card Information Names: Ammonium Nitrate Formula: N H4 N O3 PDF Number: 47-866 Quality: star Subfiles: inorganic Cell and Symmetry Information System: orthorhombic Space Group: Pbnm (no. 62) a: 7.158 b: 7.710 c: 5.837 Density (Dx): 1.650 Z: 4 Instrument Information Radiation: CuKa1 Wavelength: 1.54056 Instrument(d): diffractometer Instrument(I): diffractometer I type: unknown Comments and Additional Information Temperature: Pattern taken at 48.5 C. General: Pattern for the same specimen at 23 C used in data refinement as the external standard. Source: Ammonium nitrate 99.999% supplied by Aldrich Chemical Co., Lot No. 14012TW. Analysis: Analysis (wt.%): N O3 75.8 (with Nitron); Si 6.0 ppm, Mg 4.0 ppm, Fe 2.0 ppm, Na 2.0 ppm, Ti 0.5 ppm. General: Form III. Pattern: To replace 00-044-0737. Pattern: See ICSD 24012 (PDF 01-073-1518); ICSD 26665 (PDF 01-074-0972). Literature References General: Heyding, R., Queen's Univ., Kingston,Ontario, Canada. Private Communication (1995) Unit Cell: Wyckoff, R. The Structure of Crystals, 2nd ed. 2 368 ( ) Peak Data PeakList 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 16.900 5.2420 12.0 ( 1 1 0) 8.450 0.0954 1.1986 19.606 4.5240 14.0 ( 1 0 1) 9.803 0.1105 1.3889 22.777 3.9010 60.0 ( 1 1 1) 11.388 0.1282 1.6107 26.236 3.3940 49.0 ( 1 2 0) 13.118 0.1473 1.8513 27.446 3.2470 22.0 ( 2 1 0) 13.723 0.1540 1.9351 27.698 3.2180 100.0 ( 0 2 1) 13.849 0.1554 1.9525 30.484 2.9300 12.0 ( 1 2 1) 15.242 0.1706 2.1444 30.601 2.9190 16.0 ( 0 0 2) 15.301 0.1713 2.1525 31.509 2.8370 9.0 ( 2 1 1) 15.754 0.1762 2.2147 34.155 2.6230 30.0 ( 2 2 0) 17.077 0.1906 2.3954 35.164 2.5500 6.0 ( 1 1 2) 17.582 0.1961 2.4640 37.136 2.4190 43.0 ( 1 3 0) 18.568 0.2067 2.5974 38.661 2.3270 43.0 ( 0 2 2) 19.331 0.2149 2.7001 39.818 2.2620 16.0 ( 2 0 2) 19.909 0.2210 2.7777 40.320 2.2350 3.0 ( 1 3 1) 20.160 0.2237 2.8113 40.758 2.2120 9.0 ( 1 2 2) 20.379 0.2260 2.8405 47.123 1.9270 3.0 ( 0 4 0) 23.561 0.2595 3.2606 47.410 1.9160 3.0 ( 3 2 1) 23.705 0.2610 3.2793 49.960 1.8240 7.0 ( 1 1 3) 24.980 0.2741 3.4447 51.501 1.7730 4.0 ( 1 4 1) 25.750 0.2820 3.5438 56.402 1.6300 4.0 ( 2 4 1) 28.201 0.3067 3.8547 4. Card Information Names: Ammonium Nitrate Nitrammite, syn [NR] Formula: N H4 N O3 PDF Number: 47-867 Quality: star Subfiles: inorganic mineral Cell and Symmetry Information System: orthorhombic Space Group: Pnmm (no. 59) a: 4.9288 b: 5.4408 c: 5.7529 Density (Dx): 1.723 Z: 2 Instrument Information Radiation: CuKa1 Wavelength: 1.54056 Instrument(d): diffractometer Standard: Si Instrument(I): diffractometer I type: unknown Comments and Additional Information Colour: White Temperature: Pattern taken at 25 C. Source: Ammonium nitrate 99.999% supplied by Aldrich Chemical Co., Lot No. 14012TW. Analysis: Analysis (wt.%): N O3 75.8 (with Nitron); Si 6.0 ppm, Mg 4.0 ppm, Fe 2.0 ppm, Na 2.0 ppm, Ti 0.5 ppm. General: Form IV. Literature References General: Heyding, R., Queen's Univ., Kingston,Ontario, Canada. Private Communication (1995) Unit Cell: Wyckoff, R. The Structure of Crystals, 2nd ed. 2 371 ( ) Peak Data PeakList 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 17.982 4.9290 31.0 ( 1 0 0) 8.991 0.1014 1.2747 22.473 3.9530 46.0 ( 0 1 1) 11.237 0.1265 1.5895 24.339 3.6540 3.0 ( 1 1 0) 12.170 0.1368 1.7195 28.918 3.0850 100.0 ( 1 1 1) 14.459 0.1621 2.0367 31.059 2.8770 11.0 ( 0 0 2) 15.530 0.1738 2.1839 32.902 2.7200 64.0 ( 0 2 0) 16.451 0.1838 2.3100 36.130 2.4840 9.0 ( 1 0 2) 18.065 0.2013 2.5295 37.734 2.3820 8.0 ( 1 2 0) 18.867 0.2099 2.6378 39.855 2.2600 43.0 ( 1 1 2) 19.928 0.2212 2.7802 40.133 2.2450 32.0 ( 2 1 0) 20.066 0.2227 2.7987 43.231 2.0910 4.0 ( 2 1 1) 21.616 0.2391 3.0049 45.886 1.9760 4.0 ( 0 2 2) 22.943 0.2530 3.1797 49.640 1.8350 4.0 ( 1 2 2) 24.820 0.2725 3.4241 50.403 1.8090 1.0 ( 0 1 3) 25.202 0.2764 3.4733 51.068 1.7870 6.0 ( 1 0 3) 25.534 0.2798 3.5161 51.594 1.7700 1.0 ( 2 1 2) 25.797 0.2825 3.5498 52.878 1.7300 3.0 ( 0 3 1) 26.439 0.2890 3.6319 56.326 1.6320 5.0 ( 1 3 1) 28.163 0.3064 3.8500 58.355 1.5800 4.0 ( 3 0 1) 29.178 0.3165 3.9767 58.640 1.5730 2.0 ( 3 1 0) 29.320 0.3179 3.9944 61.209 1.5130 4.0 ( 2 0 3) 30.604 0.3305 4.1528 62.119 1.4930 4.0 ( 1 2 3) 31.059 0.3349 4.2084 63.443 1.4650 3.0 ( 1 3 2) 31.721 0.3413 4.2889 63.637 1.4610 3.0 ( 2 3 0) 31.818 0.3422 4.3006 64.777 1.4380 2.0 ( 0 0 4) 32.389 0.3477 4.3694 68.651 1.3660 3.0 ( 3 2 1) 34.326 0.3660 4.5997 68.997 1.3600 2.0 ( 0 4 0) 34.498 0.3676 4.6200 70.297 1.3380 2.0 ( 1 1 4) 35.148 0.3737 4.6960 71.276 1.3220 2.0 ( 2 2 3) 35.638 0.3782 4.7528 74.539 1.2720 1.0 ( 0 2 4) 37.270 0.3931 4.9396 5. Card Information Names: Ammonium Nitrate Formula: N H4 N O3 PDF Number: 43-1431 Quality: questionable Subfiles: inorganic EXP Cell and Symmetry Information System: orthorhombic Space Group: Pccn (no. 56) a: 7.984 b: 8.002 c: 9.817 Density (Dm): 1.760 Z: 8 Instrument Information Radiation: CrKa1 Wavelength: 2.2896 Instrument(d): diffractometer Instrument(I): diffractometer I type: unknown Comments and Additional Information Temperature: Pattern taken at -35.2 C. Pattern: To replace 00-011-0036. Quality: O assigned because average Delta2 theta is 0.056. Pattern: See ICSD 27453 (PDF 01-074-1629). Literature References General: Engel, W., Herrmann, M., Fraunhofer-Institutfur Chemische Technologie, Germany. ICDD Grant-in-Aid (1992) Peak Data PeakList 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 18.054 4.9093 22.0 ( 0 0 2) 9.027 0.1018 1.2799 20.170 4.3988 2.0 10.085 0.1137 1.4284 21.231 4.1813 3.0 ( 1 0 2) 10.616 0.1196 1.5027 22.185 4.0037 44.0 ( 0 2 0) 11.093 0.1249 1.5694 22.238 3.9943 44.0 ( 2 0 0) 11.119 0.1252 1.5730 22.645 3.9234 10.0 11.322 0.1274 1.6015 26.161 3.4035 2.0 13.080 0.1469 1.8461 26.512 3.3593 1.0 ( 1 2 1) 13.256 0.1488 1.8704 28.792 3.0982 100.0 ( 2 0 2) 14.396 0.1614 2.0280 29.121 3.0640 13.0 14.560 0.1632 2.0507 30.953 2.8866 16.0 ( 2 1 2) 15.477 0.1732 2.1767 31.644 2.8251 89.0 ( 2 2 0) 15.822 0.1770 2.2240 32.971 2.7144 9.0 ( 2 2 1) 16.486 0.1842 2.3147 33.473 2.6748 11.0 16.737 0.1869 2.3490 35.472 2.5286 17.0 ( 1 3 0) 17.736 0.1977 2.4849 35.535 2.5242 18.0 ( 3 1 0) 17.767 0.1981 2.4891 36.095 2.4864 2.0 18.047 0.2011 2.5271 36.672 2.4485 6.0 ( 2 2 2) 18.336 0.2042 2.5661 37.266 2.4108 1.0 ( 2 1 3) 18.633 0.2074 2.6062 38.394 2.3426 11.0 ( 0 3 2) 19.197 0.2134 2.6822 40.109 2.2463 13.0 ( 3 1 2) 20.054 0.2226 2.7972 40.355 2.2331 2.0 20.178 0.2239 2.8136 43.316 2.0871 2.0 ( 2 0 4) 21.658 0.2396 3.0105 44.828 2.0201 10.0 ( 3 2 2) 22.414 0.2475 3.1103 44.870 2.0183 9.0 22.435 0.2477 3.1130 45.325 1.9991 6.0 ( 3 1 3) 22.663 0.2501 3.1429 45.457 1.9937 5.0 ( 4 0 0) 22.728 0.2508 3.1516 50.657 1.8005 6.0 ( 4 1 2) 25.328 0.2777 3.4896 51.959 1.7584 1.0 ( 3 3 2) 25.980 0.2843 3.5732 60.974 1.5183 5.0 ( 5 0 2) 30.487 0.3293 4.1384 61.291 1.5112 4.0 ( 2 0 6) 30.646 0.3309 4.1579 64.560 1.4423 2.0 ( 4 2 4) 32.280 0.3467 4.3563 69.184 1.3568 2.0 ( 5 3 1) 34.592 0.3685 4.6310 69.245 1.3557 2.0 34.623 0.3688 4.6346 75.137 1.2634 3.0 ( 5 3 3) 37.569 0.3958 4.9734 75.295 1.2611 3.0 ( 6 2 0) 37.647 0.3965 4.9823 75.338 1.2605 5.0 37.669 0.3967 4.9847 79.512 1.2045 4.0 39.756 0.4151 5.2166 |
2楼2015-01-04 09:06:48
3楼2015-01-04 09:56:06