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jiaojiao1030

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[求助] 求助XRD精修

最近投了一篇文章,所制物质带有杂质相,以下是审稿人的问题,不会,希望会的人提一点意见给我。
A Rietveld analysis of all the X-ray patterns should be done at least to clarify the real situation concerning the purity of the samples (samples are supposed to be pure on the basis of XRD in the main text while the authors suggests some impurities in the abstract !! The observation of Fig. 1 clearly revealed extra peaks at about 32°, 38°, ;; in 2theta). In addition a very brief description of the structure (even if the crystal type is well known) would be appreciated.
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