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【答案】应助回帖
感谢参与，应助指数 +1
PDF#85-2330: QM=Calculated(C); d=Calculated; I=Calculated
Zirconium Chromium Iron
Zr ( Cr0.25 Fe0.75 )2
Radiation=CuKa1 Lambda=1.54060 Filter=
Calibration= 2T=20.469-88.848 I/Ic(RIR)=4.58
Ref: Calculated from ICSD using POWD-12++ (1997)
Hexagonal - Profile Analysis, P63/mmc (194) Z=4 mp=
CELL: 5.006 x 5.006 x 8.193 <90.0 x 90.0 x 120.0> P.S=hP12 (?)
Density(c)=7.508 Density(m)=7.59A Mwt=200.99 Vol=177.81 F(30)=999.9(.0000,31/0)
Ref: Canet, O., Latroche, M., Bouree-Vigneron, F., Percheron-Guegan, A.
J. Alloys Compds., v210 p129 (1994)
Strong Lines: 2.14/X 2.31/9 2.10/7 2.50/5 1.41/3 1.31/2 1.36/2 1.25/2 2.17/1 2.05/1
FIZ=080493: REM TEM 25 C.
Rietveld profile refinement applied F Nearly identical result for Fe/Cr=.6/.4 (misprint for.
ITF Structural study of Zr (Cr1-x Fex)2 D(y) (0.4<x<0.75;2<y<3) by means of neutron powder diffraction h f a (P63/MMC) NO2
2-Theta d(?) I(v) ( h k l ) Theta 1/(2d) 2pi/d n^2
20.469 4.3353 0.4 ( 1 0 0) 10.234 0.1153 1.4493
21.676 4.0965 0.3 ( 0 0 2) 10.838 0.1221 1.5338
23.193 3.8319 0.7 ( 1 0 1) 11.596 0.1305 1.6397
29.986 2.9775 3.9 ( 1 0 2) 14.993 0.1679 2.1102
35.846 2.5030 42.0 ( 1 1 0) 17.923 0.1998 2.5103
38.944 2.3107 81.2 ( 1 0 3) 19.472 0.2164 2.7191
41.630 2.1677 13.3 ( 2 0 0) 20.815 0.2307 2.8986
42.279 2.1359 100.0 ( 1 1 2) 21.140 0.2341 2.9418
43.133 2.0956 69.5 ( 2 0 1) 21.566 0.2386 2.9983
44.181 2.0482 12.6 ( 0 0 4) 22.090 0.2441 3.0676
47.411 1.9160 7.0 ( 2 0 2) 23.705 0.2610 3.2794
49.155 1.8520 7.7 ( 1 0 4) 24.578 0.2700 3.3927
53.960 1.6978 0.3 ( 2 0 3) 26.980 0.2945 3.7007
56.080 1.6386 0.1 ( 2 1 0) 28.040 0.3051 3.8345
57.292 1.6068 0.7 ( 2 1 1) 28.646 0.3112 3.9104
58.148 1.5852 0.1 ( 1 1 4) 29.074 0.3154 3.9638
60.337 1.5328 7.0 ( 1 0 5) 30.168 0.3262 4.0992
60.835 1.5214 2.8 ( 2 1 2) 30.417 0.3286 4.1299
62.316 1.4888 0.4 ( 2 0 4) 31.158 0.3358 4.2204
64.420 1.4451 9.9 ( 3 0 0) 32.210 0.3460 4.3479
65.538 1.4231 0.2 ( 3 0 1) 32.769 0.3513 4.4150
66.488 1.4051 39.1 ( 2 1 3) 33.244 0.3558 4.4717
68.680 1.3655 6.4 ( 0 0 6) 34.340 0.3662 4.6014
68.835 1.3628 28.4 ( 3 0 2) 34.417 0.3669 4.6105
72.212 1.3072 33.8 ( 2 0 5) 36.106 0.3825 4.8068
74.027 1.2795 5.7 ( 2 1 4) 37.013 0.3908 4.9105
74.177 1.2773 3.0 ( 3 0 3) 37.089 0.3914 4.9191
75.974 1.2515 28.3 ( 2 2 0) 37.987 0.3995 5.0205
79.676 1.2024 0.2 ( 3 1 0) 39.838 0.4158 5.2255
79.970 1.1987 0.5 ( 1 1 6) 39.985 0.4171 5.2416
80.117 1.1969 0.4 ( 2 2 2) 40.058 0.4177 5.2496
80.704 1.1897 0.2 ( 3 1 1) 40.352 0.4203 5.2815
81.436 1.1808 0.2 ( 3 0 4) 40.718 0.4234 5.3211
83.334 1.1587 7.2 ( 2 1 5) 41.667 0.4315 5.4228
83.625 1.1554 13.5 ( 2 0 6) 41.813 0.4328 5.4382
85.950 1.1300 3.0 ( 1 0 7) 42.975 0.4425 5.5605
88.848 1.1005 19.2 ( 3 1 3) 44.424 0.4544 5.7096 |
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