急求钛酸钾盐的XRD衍射的标准卡片数据 - 晶体 - 晶体解析

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Name and formula

Reference code: 00-035-0089

PDF index name: Potassium Titanium Oxide

Empirical formula: K2O17Ti8
Chemical formula: K2Ti8O17

Crystallographic parameters

Crystal system: Monoclinic
Space group: C

a (?):    15.6200
b (?):    3.7710
c (?):    11.9300
Alpha (°):    90.0000
Beta (°):    95.8000
Gamma (°):    90.0000

Volume of cell (10^6 pm^3): 699.12

RIR: -

Status, subfiles and quality

Status: Marked as deleted by ICDD
Subfiles: Inorganic
Quality: Indexed (I)

Comments

Deleted by: Deleted by 41-1100, has superior intensity values; Weissmann 6/90.
Color: White
Sample preparation: Made by heating potassium tetratitanate with water at 100 C for 3 days.

References

Primary reference: Marchand, R. et al., Mater. Res. Bull., 15, 1129, (1980)

Peak list

No. h k l    d [A]    2Theta[deg] I [%]
  1 2 0 0    7.75000 11.408    100.0
  2 2 0 -1    6.80000 13.009    70.0
  3 2 0 -3    3.66000 24.299    60.0
  4 1 1 -2    3.16000 28.218    20.0
  5 3 1 0    3.04000 29.356    70.0
  6 3 1 -1    2.99000 29.858    70.0
  7 2 0 -4    2.86900 31.149    60.0
  8 3 1 -2    2.77300 32.256    20.0
  9 3 1 2    2.64500 33.863    70.0
10 6 0 0    2.58500 34.674    60.0
11 4 0 -4    2.48100 36.176    20.0
12 3 1 3    2.34800 38.303    20.0
13 2 0 -5    2.33300 38.559    20.0
14 5 1 -3    2.12200 42.570    70.0
15 6 0 3    2.07700 43.539    70.0
16 8 0 0    1.94300 46.713    20.0
17 8 0 1    1.88400 48.267    60.0
18 4 0 -6    1.84000 49.498    20.0

Stick Pattern

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11楼2007-10-09 17:55:01

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Name and formula

Reference code: 00-040-0403

PDF index name: Potassium Titanium Oxide

Empirical formula: K2O13Ti6
Chemical formula: K2Ti6O13

Crystallographic parameters

Crystal system: Monoclinic
Space group: C2/m
Space group number: 12

a (?):    15.5930
b (?):    3.7960
c (?):    9.1080
Alpha (°):    90.0000
Beta (°):    99.7800
Gamma (°):    90.0000

Volume of cell (10^6 pm^3): 531.28
Z:    2.00

RIR: -

Subfiles and Quality

Subfiles: Inorganic
Corrosion
Quality: Indexed (I)

Comments

Sample preparation: Prepared from reaction of KNO3  with TiO2  (1:2).
Additional pattern: To replace 00-013-0574.

References

Primary reference: Andersen, E., Andersen, I., Skou, E., Solid State Ionics, 27, 181, (1988)

Peak list

No. h k l    d [A]    2Theta[deg] I [%]
  1 2 0 0    7.69900 11.484    100.0
  2 2 0 -1    6.40100 13.824    67.0
  3 0 0 2    4.49500 19.735    13.0
  4 1 1 0    3.68800 24.112    67.0
  5 3 1 0    3.05000 29.258    100.0
  6 3 1 -1    2.98200 29.940    67.0
  7 2 0 -3    2.96400 30.127    67.0
  8 1 1 -2    2.90500 30.753    13.0
  9 3 1 1    2.80200 31.913    33.0
10 1 1 2    2.79500 31.995    33.0
11 3 1 -2    2.65200 33.771    7.0
12 6 0 -1    2.58100 34.729    7.0
13 4 0 -4    2.09900 43.059    33.0
14 6 0 2    2.07800 43.517    33.0
15 3 1 3    2.03500 44.485    7.0
16 5 1 -3    2.00000 45.306    7.0
17 0 2 0    1.89800 47.889    100.0
18 5 1 -4    1.75500 52.070    7.0
19 7 1 2    1.66400 55.151    7.0
20 2 2 -3    1.59800 57.637    13.0
21 7 1 -4    1.56800 58.847    7.0
22 4 2 2    1.55300 59.472    7.0
23 5 1 -5    1.53600 60.198    7.0
24 6 2 -1    1.52900 60.503    7.0
25 0 0 6    1.49600 61.982    7.0
26 2 0 6    1.42400 65.495    7.0
27 4 2 -4    1.40800 66.335    7.0
28 6 2 2    1.40100 66.710    7.0

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12楼2007-10-09 17:55:17

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Name and formula

Reference code: 00-041-1100

PDF index name: Potassium Titanium Oxide

Empirical formula: K2O17Ti8
Chemical formula: K2Ti8O17

Crystallographic parameters

Crystal system: Monoclinic
Space group: C2/m
Space group number: 12

a (?):    15.6780
b (?):    3.7750
c (?):    11.9510
Alpha (°):    90.0000
Beta (°):    95.6700
Gamma (°):    90.0000

Calculated density (g/cm^3):    3.46
Volume of cell (10^6 pm^3): 703.85
Z:    2.00

RIR: -

Subfiles and Quality

Subfiles: Inorganic
Corrosion
Quality: Star (S)

Comments

Color: White
Sample preparation: The compound is prepared by substituting for K+ the half of exchangeable protons in the protonic layered tetratitanate H2Ti4O9

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Name and formula

Reference code: 00-051-1890

PDF index name: Potassium Titanium Oxide

Empirical formula: K2O5Ti2
Chemical formula: K2Ti2O5

Crystallographic parameters

Crystal system: Monoclinic
Space group: P

a (?):    6.6050
b (?):    3.0690
c (?):    5.6650
Alpha (°):    90.0000
Beta (°):    99.8800
Gamma (°):    90.0000

Volume of cell (10^6 pm^3): 113.13

RIR: -

Subfiles and Quality

Subfiles: Inorganic
Corrosion
Quality: Star (S)

Comments

Sample preparation: TiO2  and K2CO3  prepared at high temperature.
Additional pattern: To replace 00-013-0448.
Temperature: Pattern taken at 25 C.

References

Primary reference: Ouhenia, S., Univ. Abderhamane Mira Bejaia, Algerie., Private Communication, (2000)

Peak list

No. h k l    d [A]    2Theta[deg] I [%]
  1 1 0 0    6.51380 13.583    100.0
  2 1 0 -1    4.65137 19.065    18.0
  3 2 0 0    3.25336 27.392    11.0
  4 0 1 0    3.04652 29.292    60.0
  5 0 0 2    2.79105 32.042    9.0
  6 1 0 -2    2.73882 32.670    14.0
  7 2 0 1    2.62201 34.169    14.0
  8 3 0 0    2.16796 41.625    12.0
  9 3 0 -1    2.14947 42.000    9.0
10 3 0 1    1.91402 47.463    9.0
11 1 0 -3    1.87644 48.474    5.0
12 2 0 -3    1.74968 52.240    5.0
13 4 0 0    1.62749 56.498    5.0
14 4 0 -2    1.52418 60.714    4.0

Stick Pattern

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14楼2007-10-09 17:56:05

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Name and formula

Reference code: 01-074-0275

Mineral name: Jeppeite, syn
Common name: Dipotassium hexatitanium(IV) oxide
ICSD name: Potassium Titanium Oxide

Empirical formula: K2O13Ti6
Chemical formula: K2Ti6O13

Crystallographic parameters

Crystal system: Monoclinic
Space group: C2/m
Space group number: 12

a (?):    15.5820
b (?):    3.8200
c (?):    9.1120
Alpha (°):    90.0000
Beta (°):    99.7640
Gamma (°):    90.0000

Calculated density (g/cm^3):    3.56
Measured density (g/cm^3):    3.58
Volume of cell (10^6 pm^3): 534.52
Z:    2.00

RIR:    1.28

Subfiles and Quality

Subfiles: Inorganic
Mineral
Corrosion
ICSD Pattern
Quality: Calculated (C)

Comments

Sample preparation: Prepared from a melt.
Additional pattern: See PDF 00-037-0426.
ICSD collection code: 025712

References

Primary reference: Calculated from ICSD using POWD-12++
Structure: Cid-Dresdner, H., Buerger, M.J., Z. Kristallogr., Kristallgeom., Kristallphys., Kristallchem., 117, 411, (1962)

Peak list

No. h k l    d [A]    2Theta[deg] I [%]
  1 0 0 1    8.98001    9.842    3.4
  2 2 0 0    7.67814 11.516    100.0
  3 -2 0 1    6.39610 13.834    52.6
  4 2 0 1    5.40088 16.400    1.0
  5 0 0 2    4.49001 19.757    8.6
  6 -2 0 2    4.19862 21.143    1.3
  7 4 0 0    3.83907 23.150    1.9
  8 -4 0 1    3.76857 23.589    4.7
  9 1 1 0    3.70702 23.986    23.7
10 2 0 2    3.61779 24.587    2.4
11 -1 1 1    3.47712 25.598    0.1
12 1 1 1    3.37811 26.362    1.6
13 4 0 1    3.33169 26.736    0.1
14 -4 0 2    3.19805 27.875    3.9
15 3 1 0    3.06147 29.146    56.9
16 0 0 3    2.99187 29.839    58.4
17 -2 0 3    2.96420 30.124    46.6
18 -1 1 2    2.91788 30.614    7.0
19 3 1 1    2.81190 31.798    17.9
20 1 1 2    2.80285 31.903    25.3
21 4 0 2    2.70044 33.148    33.5
22 -3 1 2    2.65804 33.692    7.3
23 2 0 3    2.64142 33.910    3.4
24 -4 0 3    2.57937 34.752    16.1
25 3 1 2    2.41787 37.155    2.1
26 5 1 0    2.39288 37.557    0.6
27 -1 1 3    2.37693 37.819    3.0
28 6 0 1    2.35820 38.131    1.0
29 1 1 3    2.28364 39.426    0.8
30 -2 0 4    2.25783 39.896    0.2
31 5 1 1    2.24031 40.222    3.0
32 4 0 3    2.18754 41.235    0.2
33 -6 0 3    2.13203 42.360    1.2
34 -4 0 4    2.09931 43.053    30.1
35 6 0 2    2.07712 43.536    29.3
36 3 1 3    2.03939 44.384    4.9
37 5 1 2    2.00298 45.235    3.9
38 -1 1 4    1.95612 46.381    1.7
39 -8 0 1    1.94580 46.642    1.9
40 0 2 0    1.91000 47.569    36.5
41 -3 1 4    1.90488 47.705    20.1
42 1 1 4    1.88639 48.202    3.2
43 0 2 1    1.86821 48.701    0.2
44 2 2 0    1.85351 49.113    3.4
45 -6 0 4    1.85045 49.200    4.5
46 -2 2 1    1.83014 49.782    2.2
47 8 0 1    1.81526 50.219    4.2
48 4 0 4    1.80794 50.436    4.3
49 0 0 5    1.79600 50.795    0.4
50 0 2 2    1.75746 51.991    11.4
51 -4 0 5    1.74428 52.414    0.6
52 -2 2 2    1.73856 52.600    0.4
53 3 1 4    1.72872 52.922    0.3
54 -7 1 3    1.72446 53.063    1.6
55 4 2 0    1.71005 53.546    0.3
56 -4 2 1    1.70368 53.762    0.6
57 2 0 5    1.68652 54.354    1.7
58 8 0 2    1.66584 55.085    10.5
59 -4 2 2    1.63981 56.036    0.7
60 -3 1 5    1.62260 56.684    1.8
61 0 2 3    1.61014 57.163    1.4
62 -2 2 3    1.60556 57.341    10.3
63 -8 0 4    1.59902 57.597    3.5
64 1 1 5    1.59094 57.917    1.3
65 -9 1 1    1.57665 58.493    2.2
66 -7 1 4    1.56968 58.778    7.8
67 4 2 2    1.55937 59.205    9.3
68 -9 1 2    1.54793 59.687    4.2
69 -6 2 1    1.53489 60.246    11.0
70 6 2 0    1.53023 60.449    9.0
71 -2 0 6    1.51817 60.980    0.8
72 7 1 3    1.50828 61.423    2.4
73 8 0 3    1.50408 61.613    1.4
74 0 0 6    1.49667 61.952    9.6
75 3 1 5    1.48477 62.504    1.7
76 -4 0 6    1.48210 62.629    1.2
77 -9 1 3    1.47890 62.780    0.6
78 10 0 1    1.47142 63.136    1.0
79 -2 2 4    1.45894 63.739    0.1
80 0 2 4    1.45474 63.945    0.3
81 -8 0 5    1.43876 64.741    0.1
82 2 0 6    1.42436 65.477    3.1
83 -7 1 5    1.41277 66.082    11.6
84 -1 1 6    1.40798 66.336    7.2
85 9 1 2    1.40595 66.444    14.1
86 -3 1 6    1.40187 66.663    8.8
87 -9 1 4    1.38425 67.625    0.6
88  -10 0 4    1.38133 67.787    0.4
89 1 1 6    1.36851 68.510    1.2
90 6 0 5    1.36530 68.693    0.9
91 -8 2 1    1.36305 68.823    1.0
92 7 1 4    1.35632 69.213    1.1
93 8 2 0    1.35327 69.391    2.1
94 8 0 4    1.35022 69.570    1.0
95 -8 2 2    1.34139 70.095    0.3
96 -6 2 4    1.32902 70.845    1.4
97  -11 1 2    1.31632 71.633    5.6
98 4 2 4    1.31337 71.819    3.4
99 6 2 3    1.31007 72.028    0.7
100 9 1 3    1.30171 72.564    0.1
101  -12 0 1    1.29801 72.804    0.2
102 3 1 6    1.29381 73.079    1.7
103 -8 0 6    1.28969 73.350    1.0
104 -4 2 5    1.28800 73.462    0.3
105 -4 0 7    1.28394 73.733    0.2
106  -10 0 5    1.27922 74.050    0.8
107 1 3 0    1.26898 74.749    0.5
108 2 2 5    1.26421 75.080    0.9
109  -12 0 3    1.25619 75.643    0.1
110 1 3 1    1.25406 75.794    0.1
111 12 0 1    1.23791 76.962    0.9
112 3 3 0    1.23568 77.127    2.1
113 -6 0 7    1.23373 77.271    2.4
114 2 0 7    1.23096 77.478    2.8
115 -3 1 7    1.22843 77.667    1.5
116 -8 2 4    1.22608 77.844    2.0
117  -11 1 4    1.22003 78.304    1.2
118 3 3 1    1.21669 78.560    1.5
119 11 1 2    1.20793 79.241    0.6
120 -3 3 2    1.20406 79.547    0.5
121 -5 1 7    1.19858 79.983    0.7
122  -10 2 2    1.19644 80.156    3.9
123 4 2 5    1.19423 80.334    4.2
124 -2 2 6    1.18847 80.804    0.5
125 0 2 6    1.17807 81.667    5.1
126 -1 3 3    1.17426 81.989    2.8
127 -4 2 6    1.17093 82.273    0.7
128 10 2 1    1.16564 82.728    0.8
129 1 3 3    1.16249 83.001    0.6
130 4 0 7    1.15907 83.301    0.2
131 5 3 1    1.15665 83.514    0.2
132  -11 1 5    1.14982 84.123    0.7
133 -7 1 7    1.14450 84.605    0.5
134 3 1 7    1.14182 84.850    2.6
135  -13 1 2    1.13898 85.111    3.4
136  -12 0 5    1.13733 85.264    0.8
137 11 1 3    1.13635 85.355    1.3
138 -6 2 6    1.12853 86.089    0.5
139 3 3 3    1.12604 86.326    0.6
140 0 0 8    1.12250 86.666    0.2
141 -5 3 3    1.11979 86.928    0.4
142  -13 1 3    1.11743 87.157    0.9
143 6 2 5    1.11071 87.819    0.3
144  -14 0 2    1.10982 87.907    0.4
145 -7 3 1    1.10450 88.441    0.1
146 8 2 4    1.10255 88.638    0.1
147 7 1 6    1.10027 88.870    0.3
148 1 3 4    1.09814 89.088    0.6
149 9 1 5    1.09585 89.324    0.3

Stick Pattern

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15楼2007-10-09 17:56:20

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Name and formula

Reference code: 01-076-1682

Common name: Dipotassium dititanium oxide
ICSD name: Potassium Titanium Oxide

Empirical formula: K2O5Ti2
Chemical formula: K2Ti2O5

Crystallographic parameters

Crystal system: Monoclinic
Space group: C2/m
Space group number: 12

a (?):    11.3700
b (?):    3.8000
c (?):    6.6200
Alpha (°):    90.0000
Beta (°): 100.1000
Gamma (°):    90.0000

Calculated density (g/cm^3):    2.99
Measured density (g/cm^3):    2.95
Volume of cell (10^6 pm^3): 281.59
Z:    2.00

RIR:    2.52

Subfiles and Quality

Subfiles: Inorganic
Corrosion
ICSD Pattern
Quality: Calculated (C)

Comments

ICSD collection code: 036097
Test from ICSD: At least one TF missing.
Calc. density unusual but tolerable.

References

Primary reference: Calculated from ICSD using POWD-12++, (1997)
Structure: Andersson, S., Wadsley, A.D., Acta Chem. Scand., 15, 663, (1961)

Peak list

No. h k l    d [A]    2Theta[deg] I [%]
  1 0 0 1    6.51741 13.575    51.6
  2 2 0 0    5.59690 15.821    0.3
  3 -2 0 1    4.67013 18.988    21.8
  4 2 0 1    3.91989 22.666    1.9
  5 1 1 0    3.59831 24.722    0.9
  6 0 0 2    3.25871 27.346    5.4
  7 -1 1 1    3.22803 27.611    1.9
  8 1 1 1    3.07754 28.990    100.0
  9 -2 0 2    3.05906 29.169    42.4
10 4 0 0    2.79845 31.955    32.8
11 -4 0 1    2.75236 32.505    6.1
12 3 1 0    2.66237 33.636    3.8
13 2 0 2    2.62321 34.153    11.8
14 -3 1 1    2.58028 34.739    27.9
15 -1 1 2    2.48615 36.099    1.3
16 4 0 1    2.42205 37.088    4.3
17 3 1 1    2.36331 38.045    6.4
18 1 1 2    2.35039 38.262    1.6
19 -3 1 2    2.20111 40.970    7.4
20 0 0 3    2.17247 41.535    9.0
21 -2 0 3    2.15686 41.849    0.9
22 3 1 2    1.94590 46.639    1.7
23 -5 1 1    1.92889 47.075    2.0
24 2 0 3    1.91513 47.434    3.0
25 -1 1 3    1.90800 47.622    12.5
26 0 2 0    1.90000 47.835    19.5
27 -4 0 3    1.88309 48.292    8.7
28 6 0 0    1.86563 48.773    0.9
29 0 2 1    1.82407 49.959    1.8
30 1 1 3    1.81507 50.224    1.1
31 -3 1 3    1.79695 50.766    0.1
32 -5 1 2    1.78212 51.219    1.8
33 5 1 1    1.77793 51.349    6.5
34 -6 0 2    1.75740 51.993    5.5
35 6 0 1    1.71575 53.354    2.9
36 2 2 1    1.70974 53.556    1.7
37 -2 0 4    1.64368 55.893    0.8
38 0 2 2    1.64138 55.978    1.0
39 0 0 4    1.62935 56.428    1.9
40 -2 2 2    1.61402 57.013    6.9
41 3 1 3    1.58865 58.009    4.5
42 4 0 3    1.58657 58.092    4.0
43 4 2 0    1.57193 58.686    7.1
44 -5 1 3    1.56453 58.991    6.0
45 5 1 2    1.55981 59.187    4.6
46 -6 0 3    1.55671 59.317    1.3
47 2 2 2    1.53877 60.079    3.2
48 -4 0 4    1.52953 60.479    4.7
49 -1 1 4    1.51675 61.043    1.4
50 6 0 2    1.50898 61.391    0.1
51 2 0 4    1.49491 62.033    1.7
52 -7 1 1    1.49038 62.242    3.1
53 7 1 0    1.47392 63.016    4.7
54 1 1 4    1.45380 63.991    1.8
55 -7 1 2    1.43271 65.048    1.4
56 0 2 3    1.43019 65.177    3.0
57 -2 2 3    1.42571 65.407    1.6
58 -8 0 1    1.42012 65.697    1.3
59 8 0 0    1.39922 66.806    0.3
60 7 1 1    1.39009 67.303    0.1
61 -8 0 2    1.37618 68.075    0.1
62 4 2 2    1.36420 68.756    0.1
63 -5 1 4    1.34882 69.653    1.2
64 5 1 3    1.34502 69.878    0.8
65 -4 2 3    1.33749 70.330    3.4
66 6 2 0    1.33119 70.712    0.4
67 -7 1 3    1.32310 71.210    0.5
68 -2 0 5    1.32132 71.320    1.0
69 3 1 4    1.31825 71.512    3.6
70 4 0 4    1.31161 71.930    0.3
71 6 0 3    1.30663 72.248    0.4
72 0 0 5    1.30348 72.450    0.3
73 -6 2 2    1.29014 73.320    2.4
74 -8 0 3    1.28324 73.780    0.5
75 6 2 1    1.27339 74.446    1.5
76 -4 0 5    1.26990 74.686    1.0
77 7 1 2    1.26818 74.804    1.9
78 1 3 0    1.25863 75.471    0.1
79 -1 1 5    1.24829 76.207    0.1
80 -2 2 4    1.24308 76.584    0.4
81 -1 3 1    1.24036 76.783    0.3
82 0 2 4    1.23685 77.041    1.3
83 -3 1 5    1.23323 77.309    4.7
84 1 3 1    1.23129 77.453    3.3
85 2 0 5    1.22301 78.077    0.6
86 4 2 3    1.21782 78.473    1.7
87 -6 2 3    1.20401 79.551    1.2
88 3 3 0    1.19944 79.915    0.3
89 -3 3 1    1.19144 80.561    4.1
90 9 1 0    1.18205 81.334    0.4
91 -9 1 2    1.17580 81.859    0.6
92 3 3 1    1.16753 82.565    1.1
93 -5 1 5    1.16473 82.807    0.6
94 5 1 4    1.16122 83.112    1.4
95 -3 3 2    1.14676 84.400    0.3
96 -8 2 1    1.13750 85.248    1.3
97 9 1 1    1.13046 85.907    0.1
98 8 2 0    1.12667 86.266    0.3
99 -9 1 3    1.11959 86.947    0.2
100 3 1 5    1.11681 87.218    0.2
101 -8 2 2    1.11454 87.440    0.1
102 4 0 5    1.10947 87.942    0.3
103 3 3 2    1.10559 88.331    0.2
104 -2 0 6    1.10313 88.579    0.6
105 -6 2 4    1.10056 88.841    0.7
106 -1 3 3    1.09850 89.051    1.2
107 8 0 3    1.09237 89.686    0.6

Stick Pattern

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16楼2007-10-09 17:56:34

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管辖: 生物材料

Name and formula

Reference code: 01-080-2023

Common name: Potassium tecto-octatitanate
ICSD name: Potassium Titanium Oxide

Empirical formula: K2O17Ti8
Chemical formula: K2 ( Ti8O17 )

Crystallographic parameters

Crystal system: Monoclinic
Space group: C2/m
Space group number: 12

a (?):    15.6780
b (?):    3.7750
c (?):    11.9510
Alpha (°):    90.0000
Beta (°):    95.6700
Gamma (°):    90.0000

Calculated density (g/cm^3):    3.46
Volume of cell (10^6 pm^3): 703.85
Z:    2.00

RIR:    2.02

Subfiles and Quality

Subfiles: Inorganic
Corrosion
ICSD Pattern
Quality: Calculated (C)

Comments

ICSD collection code: 069878

References

Primary reference: Calculated from ICSD using POWD-12++, (1997)
Structure: Sasaki, T., Watanabe, M., Fujiki, Y., Kitami, Y., Yokoyama, M., J. Solid State Chem., 92, 537, (1991)

Peak list

No. h k l    d [A]    2Theta[deg] I [%]
  1 0 0 1    11.89250    7.428    3.0
  2 2 0 0    7.80065 11.334    100.0
  3 -2 0 1    6.83996 12.932    46.1
  4 2 0 1    6.24581 14.169    0.3
  5 0 0 2    5.94626 14.886    1.5
  6 -2 0 2    4.97174 17.826    2.4
  7 2 0 2    4.51865 19.630    0.6
  8 0 0 3    3.96418 22.409    0.1
  9 4 0 0    3.90032 22.781    1.2
10 -4 0 1    3.81952 23.270    0.4
11 1 1 0    3.66912 24.238    20.6
12 4 0 1    3.60221 24.695    0.2
13 -1 1 1    3.52922 25.214    0.1
14 1 1 1    3.48332 25.552    1.0
15 -4 0 2    3.41998 26.033    1.5
16 -1 1 2    3.15545 28.259    1.0
17 4 0 2    3.12291 28.560    1.1
18 1 1 2    3.09059 28.865    4.6
19 3 1 0    3.05497 29.209    32.4
20 -3 1 1    3.00118 29.745    32.1
21 0 0 4    2.97313 30.032    3.4
22 3 1 1    2.91837 30.609    6.5
23 -2 0 4    2.87430 31.090    20.5
24 -3 1 2    2.78379 32.128    3.7
25 -1 1 3    2.72448 32.847    0.3
26 2 0 4    2.69111 33.266    2.1
27 1 1 3    2.66208 33.639    5.4
28 3 1 2    2.65232 33.767    20.6
29 -6 0 1    2.59425 34.546    11.0
30 6 0 1    2.48587 36.103    2.0
31 5 1 0    2.40504 37.360    0.1
32 -5 1 1    2.39299 37.556    0.2
33 0 0 5    2.37851 37.793    0.1
34 3 1 3    2.35462 38.191    2.5
35 -1 1 4    2.33667 38.496    3.2
36 5 1 1    2.32320 38.728    0.5
37 1 1 4    2.28415 39.417    0.6
38 -6 0 3    2.27999 39.492    0.6
39 4 0 4    2.25933 39.869    0.3
40 2 0 5    2.21487 40.704    0.1
41 -3 1 4    2.19530 41.083    0.1
42 5 1 2    2.17281 41.528    0.2
43 -4 0 5    2.12622 42.481    18.7
44 6 0 3    2.08194 43.430    18.8
45 3 1 4    2.07142 43.662    3.3
46 -1 1 5    2.01735 44.895    0.4
47 5 1 3    1.99010 45.544    0.4
48 1 1 5    1.97500 45.912    0.8
49 -2 0 6    1.96801 46.085    0.5
50 -8 0 1    1.95556 46.395    1.4
51 8 0 0    1.95016 46.531    0.9
52 -5 1 4    1.94363 46.697    0.7
53 -3 1 5    1.93190 46.997    0.1
54 -7 1 1    1.92058 47.291    0.1
55 -8 0 2    1.90976 47.575    0.5
56 0 2 0    1.88750 48.172    20.8
57 7 1 1    1.86985 48.656    0.4
58 0 2 1    1.86417 48.814    0.2
59 -6 0 5    1.84831 49.260    2.3
60 -4 0 6    1.84204 49.439    1.5
61 2 2 0    1.83456 49.654    2.5
62 -2 2 1    1.81949 50.094    1.5
63 8 0 2    1.80111 50.641    1.2
64 -7 1 3    1.78812 51.035    0.3
65 7 1 2    1.78265 51.203    1.1
66 -1 1 6    1.75948 51.927    5.8
67 2 2 2    1.74166 52.499    0.1
68 1 1 6    1.72720 52.972    0.8
69 -8 0 4    1.70999 53.548    0.5
70 0 2 3    1.70418 53.745    0.3
71 4 0 6    1.70046 53.872    0.8
72 -2 0 7    1.69521 54.052    0.8
73 -4 2 1    1.69216 54.158    0.3
74 -2 2 3    1.67986 54.587    0.8
75 7 1 3    1.67252 54.847    6.9
76 -4 2 2    1.65253 55.567    0.2
77 2 0 7    1.62693 56.519    1.8
78 -4 0 7    1.61537 56.961    0.3
79 0 2 4    1.59350 57.816    0.7
80 -5 1 6    1.59016 57.949    0.9
81 -8 0 5    1.58689 58.079    1.4
82 -9 1 1    1.58026 58.346    2.0
83 -2 2 4    1.57773 58.449    4.9
84  -10 0 1    1.56697 58.890    0.3
85 10 0 0    1.55988 59.184    6.0
86 -1 1 7    1.55552 59.366    3.8
87 7 1 4    1.55336 59.457    2.3
88  -10 0 2    1.54704 59.725    3.0
89 9 1 1    1.54375 59.865    2.2
90 4 2 3    1.53784 60.119    4.8
91 6 2 0    1.52627 60.622    3.2
92 -3 1 7    1.52279 60.775    2.3
93 -9 1 3    1.51128 61.288    0.3
94 4 0 7    1.50412 61.611    2.0
95 -6 2 2    1.50059 61.772    1.1
96 -6 0 7    1.49003 62.258    3.1
97 -2 0 8    1.48657 62.420    4.4
98 10 0 2    1.47373 63.025    0.6
99 -2 2 5    1.46926 63.239    0.3
100 -6 2 3    1.45393 63.985    0.1
101 3 1 7    1.44947 64.205    0.6
102 -9 1 4    1.44678 64.339    0.3
103 -7 1 6    1.44143 64.606    1.0
104 -4 0 8    1.43715 64.822    1.2
105 7 1 5    1.43446 64.959    2.9
106 9 1 3    1.42084 65.659    1.5
107 -4 2 5    1.41155 66.147    6.1
108 6 2 3    1.39836 66.852    6.4
109 -1 1 8    1.38906 67.359    2.4
110 -9 1 5    1.37128 68.352    0.3
111 -3 1 8    1.36832 68.521    1.2
112 -2 2 6    1.36198 68.884    0.3
113 -8 2 1    1.35809 69.110    0.7
114 4 2 5    1.35521 69.277    0.4
115 -6 0 8    1.34926 69.627    0.1
116 5 1 7    1.34036 70.157    1.7
117 8 2 1    1.33724 70.345    1.1
118  -11 1 1    1.33315 70.593    0.2
119 8 0 6    1.32616 71.021    0.5
120  -11 1 2    1.32204 71.276    3.0
121 -4 2 6    1.31830 71.509    1.8
122 3 1 8    1.30719 72.212    1.0
123 8 2 2    1.30305 72.478    0.7
124 12 0 0    1.30011 72.668    0.3
125  -12 0 2    1.29713 72.861    0.1
126  -11 1 3    1.29555 72.965    0.1
127  -10 0 6    1.28940 73.369    0.6
128 2 0 9    1.28214 73.853    0.1
129 12 0 1    1.27883 74.076    0.1
130  -12 0 3    1.27317 74.461    0.1
131 -8 2 4    1.26727 74.867    0.2
132 4 2 6    1.26337 75.138    0.4
133 -2 2 7    1.26121 75.289    0.3
134 8 2 3    1.25633 75.633    0.2
135 1 3 0    1.25426 75.780    0.4
136 10 0 5    1.24916 76.144    0.1
137 -6 2 6    1.24470 76.466    0.6
138 -3 1 9    1.23929 76.861    0.1
139  -12 0 4    1.23690 77.037    0.1
140 2 2 7    1.23233 77.376    1.0
141 -1 3 2    1.22923 77.607    0.7
142 -4 2 7    1.22803 77.697    1.0
143 1 3 2    1.22529 77.904    0.8
144 3 3 0    1.22304 78.074    1.1
145 -3 3 1    1.21951 78.344    1.3
146 4 0 9    1.21555 78.648    0.6
147 -8 2 5    1.21465 78.718    0.8
148  -11 1 5    1.20782 79.250    0.1
149  -10 2 1    1.20565 79.421    0.1
150 -3 3 2    1.20349 79.592    0.2
151 12 0 3    1.20074 79.811    0.1
152 -5 1 9    1.19650 80.151    1.6
153 -2 0 10    1.19311 80.425    0.9
154 0 0 10    1.18925 80.740    0.1
155 3 1 9    1.18794 80.847    0.2
156 9 1 6    1.18262 81.287    0.1
157 4 2 7    1.17631 81.816    1.0
158 11 1 4    1.17260 82.130    0.6

Stick Pattern

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17楼2007-10-09 17:56:47

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应助: 0 (幼儿园)
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管辖: 生物材料

Name and formula

Reference code: 01-084-2057

Common name: Dipotassium catena-octatitanate
ICSD name: Potassium Titanium Oxide

Empirical formula: K2O17Ti8
Chemical formula: K2 ( Ti8O17 )

Crystallographic parameters

Crystal system: Monoclinic
Space group: C2/m
Space group number: 12

a (?):    15.6780
b (?):    3.7750
c (?):    11.9510
Alpha (°):    90.0000
Beta (°):    95.6700
Gamma (°):    90.0000

Calculated density (g/cm^3):    3.46
Volume of cell (10^6 pm^3): 703.85
Z:    2.00

RIR:    2.01

Subfiles and Quality

Subfiles: Inorganic
Corrosion
ICSD Pattern
Quality: Calculated (C)

Comments

ICSD collection code: 203089
Test from ICSD: No R value given.
At least one TF missing.

References

Primary reference: Calculated from ICSD using POWD-12++, (1997)
Structure: Sasaki, T., Fujiki, Y., J. Solid State Chem., 83, 45, (1989)

Peak list

No. h k l    d [A]    2Theta[deg] I [%]
  1 0 0 1    11.89250    7.428    3.0
  2 2 0 0    7.80065 11.334    100.0
  3 -2 0 1    6.83996 12.932    46.0
  4 2 0 1    6.24581 14.169    0.3
  5 0 0 2    5.94626 14.886    1.6
  6 -2 0 2    4.97174 17.826    2.3
  7 2 0 2    4.51865 19.630    0.6
  8 0 0 3    3.96418 22.409    0.1
  9 4 0 0    3.90032 22.781    1.2
10 -4 0 1    3.81952 23.270    0.4
11 1 1 0    3.66912 24.238    20.2
12 4 0 1    3.60221 24.695    0.2
13 -1 1 1    3.52922 25.214    0.1
14 1 1 1    3.48332 25.552    1.0
15 -4 0 2    3.41998 26.033    1.5
16 -1 1 2    3.15545 28.259    1.0
17 4 0 2    3.12291 28.560    1.1
18 1 1 2    3.09059 28.865    4.6
19 3 1 0    3.05497 29.209    32.3
20 -3 1 1    3.00118 29.745    32.0
21 0 0 4    2.97313 30.032    3.4
22 3 1 1    2.91837 30.609    6.5
23 -2 0 4    2.87430 31.090    20.3
24 -3 1 2    2.78379 32.128    3.7
25 -1 1 3    2.72448 32.847    0.3
26 2 0 4    2.69111 33.266    2.1
27 1 1 3    2.66208 33.639    5.4
28 3 1 2    2.65232 33.767    20.3
29 -6 0 1    2.59425 34.546    11.0
30 6 0 1    2.48587 36.103    1.9
31 5 1 0    2.40504 37.360    0.1
32 -5 1 1    2.39299 37.556    0.2
33 0 0 5    2.37851 37.793    0.1
34 3 1 3    2.35462 38.191    2.4
35 -1 1 4    2.33667 38.496    3.1
36 5 1 1    2.32320 38.728    0.5
37 1 1 4    2.28415 39.417    0.6
38 -6 0 3    2.27999 39.492    0.6
39 4 0 4    2.25933 39.869    0.3
40 2 0 5    2.21487 40.704    0.1
41 -3 1 4    2.19530 41.083    0.1
42 5 1 2    2.17281 41.528    0.2
43 -4 0 5    2.12622 42.481    18.3
44 6 0 3    2.08194 43.430    18.2
45 3 1 4    2.07142 43.662    3.3
46 -1 1 5    2.01735 44.895    0.5
47 5 1 3    1.99010 45.544    0.4
48 1 1 5    1.97500 45.912    0.9
49 -2 0 6    1.96801 46.085    0.5
50 -8 0 1    1.95556 46.395    1.3
51 8 0 0    1.95016 46.531    0.9
52 -5 1 4    1.94363 46.697    0.7
53 -3 1 5    1.93190 46.997    0.1
54 -7 1 1    1.92058 47.291    0.1
55 -8 0 2    1.90976 47.575    0.4
56 0 2 0    1.88750 48.172    20.1
57 7 1 1    1.86985 48.656    0.4
58 0 2 1    1.86417 48.814    0.2
59 -6 0 5    1.84831 49.260    2.1
60 -4 0 6    1.84204 49.439    1.4
61 2 2 0    1.83456 49.654    2.3
62 -2 2 1    1.81949 50.094    1.4
63 8 0 2    1.80111 50.641    1.2
64 -7 1 3    1.78812 51.035    0.3
65 7 1 2    1.78265 51.203    1.1
66 -1 1 6    1.75948 51.927    5.5
67 2 2 2    1.74166 52.499    0.1
68 1 1 6    1.72720 52.972    0.8
69 -8 0 4    1.70999 53.548    0.4
70 0 2 3    1.70418 53.745    0.3
71 4 0 6    1.70046 53.872    0.8
72 -2 0 7    1.69521 54.052    0.8
73 -4 2 1    1.69216 54.158    0.3
74 -2 2 3    1.67986 54.587    0.7
75 7 1 3    1.67252 54.847    6.5
76 -4 2 2    1.65253 55.567    0.2
77 2 0 7    1.62693 56.519    1.8
78 -4 0 7    1.61537 56.961    0.3
79 0 2 4    1.59350 57.816    0.6
80 -5 1 6    1.59016 57.949    0.9
81 -8 0 5    1.58689 58.079    1.3
82 -9 1 1    1.58026 58.346    1.9
83 -2 2 4    1.57773 58.449    4.7
84  -10 0 1    1.56697 58.890    0.3
85 10 0 0    1.55988 59.184    5.7
86 -1 1 7    1.55552 59.366    3.6
87 7 1 4    1.55336 59.457    2.3
88  -10 0 2    1.54704 59.725    2.9
89 9 1 1    1.54375 59.865    2.1
90 4 2 3    1.53784 60.119    4.6
91 6 2 0    1.52627 60.622    3.2
92 -3 1 7    1.52279 60.775    2.3
93 -9 1 3    1.51128 61.288    0.3
94 4 0 7    1.50412 61.611    1.8
95 -6 2 2    1.50059 61.772    1.0
96 -6 0 7    1.49003 62.258    2.9
97 -2 0 8    1.48657 62.420    4.1
98 10 0 2    1.47373 63.025    0.6
99 -2 2 5    1.46926 63.239    0.3
100 -6 2 3    1.45393 63.985    0.1
101 3 1 7    1.44947 64.205    0.5
102 -9 1 4    1.44678 64.339    0.3
103 -7 1 6    1.44143 64.606    1.0
104 -4 0 8    1.43715 64.822    1.2
105 7 1 5    1.43446 64.959    2.7
106 9 1 3    1.42084 65.659    1.5
107 -4 2 5    1.41155 66.147    5.7
108 6 2 3    1.39836 66.852    6.0
109 -1 1 8    1.38906 67.359    2.2
110 -9 1 5    1.37128 68.352    0.2
111 -3 1 8    1.36832 68.521    1.1
112 -2 2 6    1.36198 68.884    0.3
113 -8 2 1    1.35809 69.110    0.7
114 4 2 5    1.35521 69.277    0.4
115 -6 0 8    1.34926 69.627    0.1
116 5 1 7    1.34036 70.157    1.6
117 8 2 1    1.33724 70.345    1.0
118  -11 1 1    1.33315 70.593    0.2
119 8 0 6    1.32616 71.021    0.5
120  -11 1 2    1.32204 71.276    2.6
121 -4 2 6    1.31830 71.509    1.5
122 3 1 8    1.30719 72.212    0.9
123 8 2 2    1.30305 72.478    0.7
124 12 0 0    1.30011 72.668    0.3
125  -12 0 2    1.29713 72.861    0.1
126  -11 1 3    1.29555 72.965    0.1
127  -10 0 6    1.28940 73.369    0.6
128 2 0 9    1.28214 73.853    0.1
129 12 0 1    1.27883 74.076    0.1
130  -12 0 3    1.27317 74.461    0.1
131 -8 2 4    1.26727 74.867    0.2
132 4 2 6    1.26337 75.138    0.4
133 -2 2 7    1.26121 75.289    0.3
134 8 2 3    1.25633 75.633    0.2
135 1 3 0    1.25426 75.780    0.3
136 10 0 5    1.24916 76.144    0.1
137 -6 2 6    1.24470 76.466    0.6
138 -3 1 9    1.23929 76.861    0.1
139  -12 0 4    1.23690 77.037    0.1
140 2 2 7    1.23233 77.376    1.0
141 -1 3 2    1.22923 77.607    0.7
142 -4 2 7    1.22803 77.697    0.9
143 1 3 2    1.22529 77.904    0.7
144 3 3 0    1.22304 78.074    1.0
145 -3 3 1    1.21951 78.344    1.3
146 4 0 9    1.21555 78.648    0.6
147 -8 2 5    1.21465 78.718    0.7
148  -11 1 5    1.20782 79.250    0.1
149  -10 2 1    1.20565 79.421    0.1
150 -3 3 2    1.20349 79.592    0.2
151 12 0 3    1.20074 79.811    0.1
152 -5 1 9    1.19650 80.151    1.5
153 -2 0 10    1.19311 80.425    0.9
154 0 0 10    1.18925 80.740    0.1
155 3 1 9    1.18794 80.847    0.2
156 9 1 6    1.18262 81.287    0.1
157 4 2 7    1.17631 81.816    0.9
158 11 1 4    1.17260 82.130    0.5

Stick Pattern

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18楼2007-10-09 17:57:02

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

Metallic

应助: (幼儿园)
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虫号: 352121

纳米镍粉，辛苦了，怎么才能把20金币给你？请版主帮忙转20金币给纳米镍粉，可以吗？

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19楼2007-10-09 22:49:08

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