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急求钛酸钾盐的XRD衍射的标准卡片数据
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| 急求K2Ti2O5、 K2Ti3O7、 K2Ti4O9、 K2Ti5O11、 K2Ti6O13、 K2Ti8O17和TiO2-B的XRD衍射的标准卡片数据，用于标定衍射峰，应助者鄙人沉重感谢，奖励金币20。 |
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Name and formula Reference code: 01-076-1682 Common name: Dipotassium dititanium oxide ICSD name: Potassium Titanium Oxide Empirical formula: K2O5Ti2 Chemical formula: K2Ti2O5 Crystallographic parameters Crystal system: Monoclinic Space group: C2/m Space group number: 12 a (?): 11.3700 b (?): 3.8000 c (?): 6.6200 Alpha (°): 90.0000 Beta (°): 100.1000 Gamma (°): 90.0000 Calculated density (g/cm^3): 2.99 Measured density (g/cm^3): 2.95 Volume of cell (10^6 pm^3): 281.59 Z: 2.00 RIR: 2.52 Subfiles and Quality Subfiles: Inorganic Corrosion ICSD Pattern Quality: Calculated (C) Comments ICSD collection code: 036097 Test from ICSD: At least one TF missing. Calc. density unusual but tolerable. References Primary reference: Calculated from ICSD using POWD-12++, (1997) Structure: Andersson, S., Wadsley, A.D., Acta Chem. Scand., 15, 663, (1961) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 0 0 1 6.51741 13.575 51.6 2 2 0 0 5.59690 15.821 0.3 3 -2 0 1 4.67013 18.988 21.8 4 2 0 1 3.91989 22.666 1.9 5 1 1 0 3.59831 24.722 0.9 6 0 0 2 3.25871 27.346 5.4 7 -1 1 1 3.22803 27.611 1.9 8 1 1 1 3.07754 28.990 100.0 9 -2 0 2 3.05906 29.169 42.4 10 4 0 0 2.79845 31.955 32.8 11 -4 0 1 2.75236 32.505 6.1 12 3 1 0 2.66237 33.636 3.8 13 2 0 2 2.62321 34.153 11.8 14 -3 1 1 2.58028 34.739 27.9 15 -1 1 2 2.48615 36.099 1.3 16 4 0 1 2.42205 37.088 4.3 17 3 1 1 2.36331 38.045 6.4 18 1 1 2 2.35039 38.262 1.6 19 -3 1 2 2.20111 40.970 7.4 20 0 0 3 2.17247 41.535 9.0 21 -2 0 3 2.15686 41.849 0.9 22 3 1 2 1.94590 46.639 1.7 23 -5 1 1 1.92889 47.075 2.0 24 2 0 3 1.91513 47.434 3.0 25 -1 1 3 1.90800 47.622 12.5 26 0 2 0 1.90000 47.835 19.5 27 -4 0 3 1.88309 48.292 8.7 28 6 0 0 1.86563 48.773 0.9 29 0 2 1 1.82407 49.959 1.8 30 1 1 3 1.81507 50.224 1.1 31 -3 1 3 1.79695 50.766 0.1 32 -5 1 2 1.78212 51.219 1.8 33 5 1 1 1.77793 51.349 6.5 34 -6 0 2 1.75740 51.993 5.5 35 6 0 1 1.71575 53.354 2.9 36 2 2 1 1.70974 53.556 1.7 37 -2 0 4 1.64368 55.893 0.8 38 0 2 2 1.64138 55.978 1.0 39 0 0 4 1.62935 56.428 1.9 40 -2 2 2 1.61402 57.013 6.9 41 3 1 3 1.58865 58.009 4.5 42 4 0 3 1.58657 58.092 4.0 43 4 2 0 1.57193 58.686 7.1 44 -5 1 3 1.56453 58.991 6.0 45 5 1 2 1.55981 59.187 4.6 46 -6 0 3 1.55671 59.317 1.3 47 2 2 2 1.53877 60.079 3.2 48 -4 0 4 1.52953 60.479 4.7 49 -1 1 4 1.51675 61.043 1.4 50 6 0 2 1.50898 61.391 0.1 51 2 0 4 1.49491 62.033 1.7 52 -7 1 1 1.49038 62.242 3.1 53 7 1 0 1.47392 63.016 4.7 54 1 1 4 1.45380 63.991 1.8 55 -7 1 2 1.43271 65.048 1.4 56 0 2 3 1.43019 65.177 3.0 57 -2 2 3 1.42571 65.407 1.6 58 -8 0 1 1.42012 65.697 1.3 59 8 0 0 1.39922 66.806 0.3 60 7 1 1 1.39009 67.303 0.1 61 -8 0 2 1.37618 68.075 0.1 62 4 2 2 1.36420 68.756 0.1 63 -5 1 4 1.34882 69.653 1.2 64 5 1 3 1.34502 69.878 0.8 65 -4 2 3 1.33749 70.330 3.4 66 6 2 0 1.33119 70.712 0.4 67 -7 1 3 1.32310 71.210 0.5 68 -2 0 5 1.32132 71.320 1.0 69 3 1 4 1.31825 71.512 3.6 70 4 0 4 1.31161 71.930 0.3 71 6 0 3 1.30663 72.248 0.4 72 0 0 5 1.30348 72.450 0.3 73 -6 2 2 1.29014 73.320 2.4 74 -8 0 3 1.28324 73.780 0.5 75 6 2 1 1.27339 74.446 1.5 76 -4 0 5 1.26990 74.686 1.0 77 7 1 2 1.26818 74.804 1.9 78 1 3 0 1.25863 75.471 0.1 79 -1 1 5 1.24829 76.207 0.1 80 -2 2 4 1.24308 76.584 0.4 81 -1 3 1 1.24036 76.783 0.3 82 0 2 4 1.23685 77.041 1.3 83 -3 1 5 1.23323 77.309 4.7 84 1 3 1 1.23129 77.453 3.3 85 2 0 5 1.22301 78.077 0.6 86 4 2 3 1.21782 78.473 1.7 87 -6 2 3 1.20401 79.551 1.2 88 3 3 0 1.19944 79.915 0.3 89 -3 3 1 1.19144 80.561 4.1 90 9 1 0 1.18205 81.334 0.4 91 -9 1 2 1.17580 81.859 0.6 92 3 3 1 1.16753 82.565 1.1 93 -5 1 5 1.16473 82.807 0.6 94 5 1 4 1.16122 83.112 1.4 95 -3 3 2 1.14676 84.400 0.3 96 -8 2 1 1.13750 85.248 1.3 97 9 1 1 1.13046 85.907 0.1 98 8 2 0 1.12667 86.266 0.3 99 -9 1 3 1.11959 86.947 0.2 100 3 1 5 1.11681 87.218 0.2 101 -8 2 2 1.11454 87.440 0.1 102 4 0 5 1.10947 87.942 0.3 103 3 3 2 1.10559 88.331 0.2 104 -2 0 6 1.10313 88.579 0.6 105 -6 2 4 1.10056 88.841 0.7 106 -1 3 3 1.09850 89.051 1.2 107 8 0 3 1.09237 89.686 0.6 Stick Pattern |
16楼2007-10-09 17:56:34
3楼2007-10-08 19:20:12
4楼2007-10-09 10:28:32
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Name and formula Reference code: 00-013-0447 PDF index name: Potassium Titanium Oxide Empirical formula: K2O9Ti4 Chemical formula: K2Ti4O9 Crystallographic parameters Crystal system: Unknown RIR: - Status, subfiles and quality Status: Marked as deleted by ICDD Subfiles: Inorganic Quality: Doubtful (O) Comments Deleted by: Deleted by 27-447. References Primary reference: Berry et al., J. Inorg. Nucl. Chem., 14, 231, (1960) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 8.66000 10.206 100.0 2 6.15000 14.391 45.0 3 3.93000 22.607 12.0 4 3.74000 23.772 14.0 5 3.67000 24.232 10.0 6 3.17000 28.127 45.0 7 2.94000 30.378 50.0 8 2.87000 31.138 45.0 9 2.79000 32.054 10.0 10 2.71000 33.027 25.0 11 2.65000 33.797 40.0 12 2.19000 41.187 30.0 13 2.09000 43.254 30.0 14 1.89000 48.104 30.0 Stick Pattern |
5楼2007-10-09 17:50:16
