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急求钛酸钾盐的XRD衍射的标准卡片数据
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| 急求K2Ti2O5、 K2Ti3O7、 K2Ti4O9、 K2Ti5O11、 K2Ti6O13、 K2Ti8O17和TiO2-B的XRD衍射的标准卡片数据，用于标定衍射峰，应助者鄙人沉重感谢，奖励金币20。 |
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Name and formula Reference code: 01-080-2023 Common name: Potassium tecto-octatitanate ICSD name: Potassium Titanium Oxide Empirical formula: K2O17Ti8 Chemical formula: K2 ( Ti8O17 ) Crystallographic parameters Crystal system: Monoclinic Space group: C2/m Space group number: 12 a (?): 15.6780 b (?): 3.7750 c (?): 11.9510 Alpha (°): 90.0000 Beta (°): 95.6700 Gamma (°): 90.0000 Calculated density (g/cm^3): 3.46 Volume of cell (10^6 pm^3): 703.85 Z: 2.00 RIR: 2.02 Subfiles and Quality Subfiles: Inorganic Corrosion ICSD Pattern Quality: Calculated (C) Comments ICSD collection code: 069878 References Primary reference: Calculated from ICSD using POWD-12++, (1997) Structure: Sasaki, T., Watanabe, M., Fujiki, Y., Kitami, Y., Yokoyama, M., J. Solid State Chem., 92, 537, (1991) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 0 0 1 11.89250 7.428 3.0 2 2 0 0 7.80065 11.334 100.0 3 -2 0 1 6.83996 12.932 46.1 4 2 0 1 6.24581 14.169 0.3 5 0 0 2 5.94626 14.886 1.5 6 -2 0 2 4.97174 17.826 2.4 7 2 0 2 4.51865 19.630 0.6 8 0 0 3 3.96418 22.409 0.1 9 4 0 0 3.90032 22.781 1.2 10 -4 0 1 3.81952 23.270 0.4 11 1 1 0 3.66912 24.238 20.6 12 4 0 1 3.60221 24.695 0.2 13 -1 1 1 3.52922 25.214 0.1 14 1 1 1 3.48332 25.552 1.0 15 -4 0 2 3.41998 26.033 1.5 16 -1 1 2 3.15545 28.259 1.0 17 4 0 2 3.12291 28.560 1.1 18 1 1 2 3.09059 28.865 4.6 19 3 1 0 3.05497 29.209 32.4 20 -3 1 1 3.00118 29.745 32.1 21 0 0 4 2.97313 30.032 3.4 22 3 1 1 2.91837 30.609 6.5 23 -2 0 4 2.87430 31.090 20.5 24 -3 1 2 2.78379 32.128 3.7 25 -1 1 3 2.72448 32.847 0.3 26 2 0 4 2.69111 33.266 2.1 27 1 1 3 2.66208 33.639 5.4 28 3 1 2 2.65232 33.767 20.6 29 -6 0 1 2.59425 34.546 11.0 30 6 0 1 2.48587 36.103 2.0 31 5 1 0 2.40504 37.360 0.1 32 -5 1 1 2.39299 37.556 0.2 33 0 0 5 2.37851 37.793 0.1 34 3 1 3 2.35462 38.191 2.5 35 -1 1 4 2.33667 38.496 3.2 36 5 1 1 2.32320 38.728 0.5 37 1 1 4 2.28415 39.417 0.6 38 -6 0 3 2.27999 39.492 0.6 39 4 0 4 2.25933 39.869 0.3 40 2 0 5 2.21487 40.704 0.1 41 -3 1 4 2.19530 41.083 0.1 42 5 1 2 2.17281 41.528 0.2 43 -4 0 5 2.12622 42.481 18.7 44 6 0 3 2.08194 43.430 18.8 45 3 1 4 2.07142 43.662 3.3 46 -1 1 5 2.01735 44.895 0.4 47 5 1 3 1.99010 45.544 0.4 48 1 1 5 1.97500 45.912 0.8 49 -2 0 6 1.96801 46.085 0.5 50 -8 0 1 1.95556 46.395 1.4 51 8 0 0 1.95016 46.531 0.9 52 -5 1 4 1.94363 46.697 0.7 53 -3 1 5 1.93190 46.997 0.1 54 -7 1 1 1.92058 47.291 0.1 55 -8 0 2 1.90976 47.575 0.5 56 0 2 0 1.88750 48.172 20.8 57 7 1 1 1.86985 48.656 0.4 58 0 2 1 1.86417 48.814 0.2 59 -6 0 5 1.84831 49.260 2.3 60 -4 0 6 1.84204 49.439 1.5 61 2 2 0 1.83456 49.654 2.5 62 -2 2 1 1.81949 50.094 1.5 63 8 0 2 1.80111 50.641 1.2 64 -7 1 3 1.78812 51.035 0.3 65 7 1 2 1.78265 51.203 1.1 66 -1 1 6 1.75948 51.927 5.8 67 2 2 2 1.74166 52.499 0.1 68 1 1 6 1.72720 52.972 0.8 69 -8 0 4 1.70999 53.548 0.5 70 0 2 3 1.70418 53.745 0.3 71 4 0 6 1.70046 53.872 0.8 72 -2 0 7 1.69521 54.052 0.8 73 -4 2 1 1.69216 54.158 0.3 74 -2 2 3 1.67986 54.587 0.8 75 7 1 3 1.67252 54.847 6.9 76 -4 2 2 1.65253 55.567 0.2 77 2 0 7 1.62693 56.519 1.8 78 -4 0 7 1.61537 56.961 0.3 79 0 2 4 1.59350 57.816 0.7 80 -5 1 6 1.59016 57.949 0.9 81 -8 0 5 1.58689 58.079 1.4 82 -9 1 1 1.58026 58.346 2.0 83 -2 2 4 1.57773 58.449 4.9 84 -10 0 1 1.56697 58.890 0.3 85 10 0 0 1.55988 59.184 6.0 86 -1 1 7 1.55552 59.366 3.8 87 7 1 4 1.55336 59.457 2.3 88 -10 0 2 1.54704 59.725 3.0 89 9 1 1 1.54375 59.865 2.2 90 4 2 3 1.53784 60.119 4.8 91 6 2 0 1.52627 60.622 3.2 92 -3 1 7 1.52279 60.775 2.3 93 -9 1 3 1.51128 61.288 0.3 94 4 0 7 1.50412 61.611 2.0 95 -6 2 2 1.50059 61.772 1.1 96 -6 0 7 1.49003 62.258 3.1 97 -2 0 8 1.48657 62.420 4.4 98 10 0 2 1.47373 63.025 0.6 99 -2 2 5 1.46926 63.239 0.3 100 -6 2 3 1.45393 63.985 0.1 101 3 1 7 1.44947 64.205 0.6 102 -9 1 4 1.44678 64.339 0.3 103 -7 1 6 1.44143 64.606 1.0 104 -4 0 8 1.43715 64.822 1.2 105 7 1 5 1.43446 64.959 2.9 106 9 1 3 1.42084 65.659 1.5 107 -4 2 5 1.41155 66.147 6.1 108 6 2 3 1.39836 66.852 6.4 109 -1 1 8 1.38906 67.359 2.4 110 -9 1 5 1.37128 68.352 0.3 111 -3 1 8 1.36832 68.521 1.2 112 -2 2 6 1.36198 68.884 0.3 113 -8 2 1 1.35809 69.110 0.7 114 4 2 5 1.35521 69.277 0.4 115 -6 0 8 1.34926 69.627 0.1 116 5 1 7 1.34036 70.157 1.7 117 8 2 1 1.33724 70.345 1.1 118 -11 1 1 1.33315 70.593 0.2 119 8 0 6 1.32616 71.021 0.5 120 -11 1 2 1.32204 71.276 3.0 121 -4 2 6 1.31830 71.509 1.8 122 3 1 8 1.30719 72.212 1.0 123 8 2 2 1.30305 72.478 0.7 124 12 0 0 1.30011 72.668 0.3 125 -12 0 2 1.29713 72.861 0.1 126 -11 1 3 1.29555 72.965 0.1 127 -10 0 6 1.28940 73.369 0.6 128 2 0 9 1.28214 73.853 0.1 129 12 0 1 1.27883 74.076 0.1 130 -12 0 3 1.27317 74.461 0.1 131 -8 2 4 1.26727 74.867 0.2 132 4 2 6 1.26337 75.138 0.4 133 -2 2 7 1.26121 75.289 0.3 134 8 2 3 1.25633 75.633 0.2 135 1 3 0 1.25426 75.780 0.4 136 10 0 5 1.24916 76.144 0.1 137 -6 2 6 1.24470 76.466 0.6 138 -3 1 9 1.23929 76.861 0.1 139 -12 0 4 1.23690 77.037 0.1 140 2 2 7 1.23233 77.376 1.0 141 -1 3 2 1.22923 77.607 0.7 142 -4 2 7 1.22803 77.697 1.0 143 1 3 2 1.22529 77.904 0.8 144 3 3 0 1.22304 78.074 1.1 145 -3 3 1 1.21951 78.344 1.3 146 4 0 9 1.21555 78.648 0.6 147 -8 2 5 1.21465 78.718 0.8 148 -11 1 5 1.20782 79.250 0.1 149 -10 2 1 1.20565 79.421 0.1 150 -3 3 2 1.20349 79.592 0.2 151 12 0 3 1.20074 79.811 0.1 152 -5 1 9 1.19650 80.151 1.6 153 -2 0 10 1.19311 80.425 0.9 154 0 0 10 1.18925 80.740 0.1 155 3 1 9 1.18794 80.847 0.2 156 9 1 6 1.18262 81.287 0.1 157 4 2 7 1.17631 81.816 1.0 158 11 1 4 1.17260 82.130 0.6 Stick Pattern |
17楼2007-10-09 17:56:47
3楼2007-10-08 19:20:12
4楼2007-10-09 10:28:32
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Name and formula Reference code: 00-013-0447 PDF index name: Potassium Titanium Oxide Empirical formula: K2O9Ti4 Chemical formula: K2Ti4O9 Crystallographic parameters Crystal system: Unknown RIR: - Status, subfiles and quality Status: Marked as deleted by ICDD Subfiles: Inorganic Quality: Doubtful (O) Comments Deleted by: Deleted by 27-447. References Primary reference: Berry et al., J. Inorg. Nucl. Chem., 14, 231, (1960) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 8.66000 10.206 100.0 2 6.15000 14.391 45.0 3 3.93000 22.607 12.0 4 3.74000 23.772 14.0 5 3.67000 24.232 10.0 6 3.17000 28.127 45.0 7 2.94000 30.378 50.0 8 2.87000 31.138 45.0 9 2.79000 32.054 10.0 10 2.71000 33.027 25.0 11 2.65000 33.797 40.0 12 2.19000 41.187 30.0 13 2.09000 43.254 30.0 14 1.89000 48.104 30.0 Stick Pattern |
5楼2007-10-09 17:50:16