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急求钛酸钾盐的XRD衍射的标准卡片数据
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| 急求K2Ti2O5、 K2Ti3O7、 K2Ti4O9、 K2Ti5O11、 K2Ti6O13、 K2Ti8O17和TiO2-B的XRD衍射的标准卡片数据，用于标定衍射峰，应助者鄙人沉重感谢，奖励金币20。 |
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Name and formula Reference code: 01-074-0275 Mineral name: Jeppeite, syn Common name: Dipotassium hexatitanium(IV) oxide ICSD name: Potassium Titanium Oxide Empirical formula: K2O13Ti6 Chemical formula: K2Ti6O13 Crystallographic parameters Crystal system: Monoclinic Space group: C2/m Space group number: 12 a (?): 15.5820 b (?): 3.8200 c (?): 9.1120 Alpha (°): 90.0000 Beta (°): 99.7640 Gamma (°): 90.0000 Calculated density (g/cm^3): 3.56 Measured density (g/cm^3): 3.58 Volume of cell (10^6 pm^3): 534.52 Z: 2.00 RIR: 1.28 Subfiles and Quality Subfiles: Inorganic Mineral Corrosion ICSD Pattern Quality: Calculated (C) Comments Sample preparation: Prepared from a melt. Additional pattern: See PDF 00-037-0426. ICSD collection code: 025712 References Primary reference: Calculated from ICSD using POWD-12++ Structure: Cid-Dresdner, H., Buerger, M.J., Z. Kristallogr., Kristallgeom., Kristallphys., Kristallchem., 117, 411, (1962) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 0 0 1 8.98001 9.842 3.4 2 2 0 0 7.67814 11.516 100.0 3 -2 0 1 6.39610 13.834 52.6 4 2 0 1 5.40088 16.400 1.0 5 0 0 2 4.49001 19.757 8.6 6 -2 0 2 4.19862 21.143 1.3 7 4 0 0 3.83907 23.150 1.9 8 -4 0 1 3.76857 23.589 4.7 9 1 1 0 3.70702 23.986 23.7 10 2 0 2 3.61779 24.587 2.4 11 -1 1 1 3.47712 25.598 0.1 12 1 1 1 3.37811 26.362 1.6 13 4 0 1 3.33169 26.736 0.1 14 -4 0 2 3.19805 27.875 3.9 15 3 1 0 3.06147 29.146 56.9 16 0 0 3 2.99187 29.839 58.4 17 -2 0 3 2.96420 30.124 46.6 18 -1 1 2 2.91788 30.614 7.0 19 3 1 1 2.81190 31.798 17.9 20 1 1 2 2.80285 31.903 25.3 21 4 0 2 2.70044 33.148 33.5 22 -3 1 2 2.65804 33.692 7.3 23 2 0 3 2.64142 33.910 3.4 24 -4 0 3 2.57937 34.752 16.1 25 3 1 2 2.41787 37.155 2.1 26 5 1 0 2.39288 37.557 0.6 27 -1 1 3 2.37693 37.819 3.0 28 6 0 1 2.35820 38.131 1.0 29 1 1 3 2.28364 39.426 0.8 30 -2 0 4 2.25783 39.896 0.2 31 5 1 1 2.24031 40.222 3.0 32 4 0 3 2.18754 41.235 0.2 33 -6 0 3 2.13203 42.360 1.2 34 -4 0 4 2.09931 43.053 30.1 35 6 0 2 2.07712 43.536 29.3 36 3 1 3 2.03939 44.384 4.9 37 5 1 2 2.00298 45.235 3.9 38 -1 1 4 1.95612 46.381 1.7 39 -8 0 1 1.94580 46.642 1.9 40 0 2 0 1.91000 47.569 36.5 41 -3 1 4 1.90488 47.705 20.1 42 1 1 4 1.88639 48.202 3.2 43 0 2 1 1.86821 48.701 0.2 44 2 2 0 1.85351 49.113 3.4 45 -6 0 4 1.85045 49.200 4.5 46 -2 2 1 1.83014 49.782 2.2 47 8 0 1 1.81526 50.219 4.2 48 4 0 4 1.80794 50.436 4.3 49 0 0 5 1.79600 50.795 0.4 50 0 2 2 1.75746 51.991 11.4 51 -4 0 5 1.74428 52.414 0.6 52 -2 2 2 1.73856 52.600 0.4 53 3 1 4 1.72872 52.922 0.3 54 -7 1 3 1.72446 53.063 1.6 55 4 2 0 1.71005 53.546 0.3 56 -4 2 1 1.70368 53.762 0.6 57 2 0 5 1.68652 54.354 1.7 58 8 0 2 1.66584 55.085 10.5 59 -4 2 2 1.63981 56.036 0.7 60 -3 1 5 1.62260 56.684 1.8 61 0 2 3 1.61014 57.163 1.4 62 -2 2 3 1.60556 57.341 10.3 63 -8 0 4 1.59902 57.597 3.5 64 1 1 5 1.59094 57.917 1.3 65 -9 1 1 1.57665 58.493 2.2 66 -7 1 4 1.56968 58.778 7.8 67 4 2 2 1.55937 59.205 9.3 68 -9 1 2 1.54793 59.687 4.2 69 -6 2 1 1.53489 60.246 11.0 70 6 2 0 1.53023 60.449 9.0 71 -2 0 6 1.51817 60.980 0.8 72 7 1 3 1.50828 61.423 2.4 73 8 0 3 1.50408 61.613 1.4 74 0 0 6 1.49667 61.952 9.6 75 3 1 5 1.48477 62.504 1.7 76 -4 0 6 1.48210 62.629 1.2 77 -9 1 3 1.47890 62.780 0.6 78 10 0 1 1.47142 63.136 1.0 79 -2 2 4 1.45894 63.739 0.1 80 0 2 4 1.45474 63.945 0.3 81 -8 0 5 1.43876 64.741 0.1 82 2 0 6 1.42436 65.477 3.1 83 -7 1 5 1.41277 66.082 11.6 84 -1 1 6 1.40798 66.336 7.2 85 9 1 2 1.40595 66.444 14.1 86 -3 1 6 1.40187 66.663 8.8 87 -9 1 4 1.38425 67.625 0.6 88 -10 0 4 1.38133 67.787 0.4 89 1 1 6 1.36851 68.510 1.2 90 6 0 5 1.36530 68.693 0.9 91 -8 2 1 1.36305 68.823 1.0 92 7 1 4 1.35632 69.213 1.1 93 8 2 0 1.35327 69.391 2.1 94 8 0 4 1.35022 69.570 1.0 95 -8 2 2 1.34139 70.095 0.3 96 -6 2 4 1.32902 70.845 1.4 97 -11 1 2 1.31632 71.633 5.6 98 4 2 4 1.31337 71.819 3.4 99 6 2 3 1.31007 72.028 0.7 100 9 1 3 1.30171 72.564 0.1 101 -12 0 1 1.29801 72.804 0.2 102 3 1 6 1.29381 73.079 1.7 103 -8 0 6 1.28969 73.350 1.0 104 -4 2 5 1.28800 73.462 0.3 105 -4 0 7 1.28394 73.733 0.2 106 -10 0 5 1.27922 74.050 0.8 107 1 3 0 1.26898 74.749 0.5 108 2 2 5 1.26421 75.080 0.9 109 -12 0 3 1.25619 75.643 0.1 110 1 3 1 1.25406 75.794 0.1 111 12 0 1 1.23791 76.962 0.9 112 3 3 0 1.23568 77.127 2.1 113 -6 0 7 1.23373 77.271 2.4 114 2 0 7 1.23096 77.478 2.8 115 -3 1 7 1.22843 77.667 1.5 116 -8 2 4 1.22608 77.844 2.0 117 -11 1 4 1.22003 78.304 1.2 118 3 3 1 1.21669 78.560 1.5 119 11 1 2 1.20793 79.241 0.6 120 -3 3 2 1.20406 79.547 0.5 121 -5 1 7 1.19858 79.983 0.7 122 -10 2 2 1.19644 80.156 3.9 123 4 2 5 1.19423 80.334 4.2 124 -2 2 6 1.18847 80.804 0.5 125 0 2 6 1.17807 81.667 5.1 126 -1 3 3 1.17426 81.989 2.8 127 -4 2 6 1.17093 82.273 0.7 128 10 2 1 1.16564 82.728 0.8 129 1 3 3 1.16249 83.001 0.6 130 4 0 7 1.15907 83.301 0.2 131 5 3 1 1.15665 83.514 0.2 132 -11 1 5 1.14982 84.123 0.7 133 -7 1 7 1.14450 84.605 0.5 134 3 1 7 1.14182 84.850 2.6 135 -13 1 2 1.13898 85.111 3.4 136 -12 0 5 1.13733 85.264 0.8 137 11 1 3 1.13635 85.355 1.3 138 -6 2 6 1.12853 86.089 0.5 139 3 3 3 1.12604 86.326 0.6 140 0 0 8 1.12250 86.666 0.2 141 -5 3 3 1.11979 86.928 0.4 142 -13 1 3 1.11743 87.157 0.9 143 6 2 5 1.11071 87.819 0.3 144 -14 0 2 1.10982 87.907 0.4 145 -7 3 1 1.10450 88.441 0.1 146 8 2 4 1.10255 88.638 0.1 147 7 1 6 1.10027 88.870 0.3 148 1 3 4 1.09814 89.088 0.6 149 9 1 5 1.09585 89.324 0.3 Stick Pattern |
15楼2007-10-09 17:56:20
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4楼2007-10-09 10:28:32
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Name and formula Reference code: 00-013-0447 PDF index name: Potassium Titanium Oxide Empirical formula: K2O9Ti4 Chemical formula: K2Ti4O9 Crystallographic parameters Crystal system: Unknown RIR: - Status, subfiles and quality Status: Marked as deleted by ICDD Subfiles: Inorganic Quality: Doubtful (O) Comments Deleted by: Deleted by 27-447. References Primary reference: Berry et al., J. Inorg. Nucl. Chem., 14, 231, (1960) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 8.66000 10.206 100.0 2 6.15000 14.391 45.0 3 3.93000 22.607 12.0 4 3.74000 23.772 14.0 5 3.67000 24.232 10.0 6 3.17000 28.127 45.0 7 2.94000 30.378 50.0 8 2.87000 31.138 45.0 9 2.79000 32.054 10.0 10 2.71000 33.027 25.0 11 2.65000 33.797 40.0 12 2.19000 41.187 30.0 13 2.09000 43.254 30.0 14 1.89000 48.104 30.0 Stick Pattern |
5楼2007-10-09 17:50:16