自由基捕获剂一般用DMPO,如果出现1:2:2:1的信号,说明有羟基自由基的存在。在下面这篇文献中有用DMPO测TiO2产生羟基自由基的实验内容,可参考。
Photolytic reaction mechanism and impacts of coexisting substances on photodegradation of bisphenol A by Bi2WO6 in water
请阅读以下综述文献:Probing paramagnetic species in titania-based heterogeneous photocatalysis by electron spin resonance (ESR) spectroscopy-A mini review. Chemical Engineering Journal.170, 353-362.