²é¿´: 1319  |  »Ø¸´: 13

ɽʯÑÒ

½ð³æ (ÖøÃûдÊÖ)

[ÇóÖú] ¾§ÌåE±à¼­Òâ¼û£¬¼±ÇóÔõô½â¾ö

±¾ÈËÐÂÊÖ£¬¶Ô¾§ÌåÒ»Çϲ»Í¨¡£×î½üͶÁËһƪ¾§ÌåE±à¼­Ìá³ö´íÎóÈçÏ£¬Çë´óÏÀÃÇÖ¸½ÌÔõô¸ÄÕý¡£´íÎó£º
1.In the abstract and comments section, could you please provide standard uncertainties for all dihedral angles quoted
2.In '_publ_section_exptl_refinement' you have indicated that the Friedel pairs were merged,  This is, in fact, not the case.  Friedel pairs were refined in the structure and the absolute configuration determined from this data.  Could you please check and correct.
3. In '_publ_section_exptl_refinement' could you provide details of the disorder present in the structure.
4. In '_publ_section_exptl_refinement'  could you provide details of the location and refinement of the N-H proton in this compound.
±¾ÈËÊÇÒ©ÎﻯѧרҵµÄ£¬¶ÔÕâ¸öʵÔÚÊǸ㲻Ã÷°×£¬Ï£ÍûרҵÈËÊ¿°ï°ïæ°¡¡£ÒªÊÇÐèÒªÊý¾ÝÎÒ·¢µ½ÄãÃÇÓÊÏäÀлл°¡£¡
»Ø¸´´ËÂ¥

» ²ÂÄãϲ»¶

» ±¾Ö÷ÌâÏà¹Ø¼ÛÖµÌùÍÆ¼ö£¬¶ÔÄúͬÑùÓаïÖú:

ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
»ØÌûÖ§³Ö ( ÏÔʾ֧³Ö¶È×î¸ßµÄǰ 50 Ãû )

ɽʯÑÒ

½ð³æ (ÖøÃûдÊÖ)

ÒýÓûØÌû:
6Â¥: Originally posted by lgzhu1964 at 2012-04-06 21:46:40:
ÔõôÐÞµÄÔõôд£¬CIFÖÐÄÜ¿´³öÀ´£¨Ö÷ҪдռÓÐÂÊÊǶàÉÙ£©¼ü³¤ÏÞÖÆ¿´CIFÒ²¿É¿´insÎļþ£®

ллÀ²£¬µ«ÊÇÒª¿´ÄÇЩÊý¾Ý²ÅÄÜ¿´³öÀ´ÄØ £¿
8Â¥2012-04-08 11:14:52
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

ɽʯÑÒ

½ð³æ (ÖøÃûдÊÖ)

ËÍÏÊ»¨Ò»¶ä
ÒýÓûØÌû:
9Â¥: Originally posted by lgzhu1964 at 2012-04-08 14:14:40:
CIFÖÐÓÐÈçÏÂÊý¾Ý£º
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_o ...

ллÀ²£¬Õâ¸öÕÒµ½Á˷dz£¸Ðл
ÈõÈõµÄÔÙÎÊÒ»ÏÂÓйØN-HÖÊ×ÓµÄÎÊÌâ¡£ÔÚÄÄÄܹ»¿´µ½N-HµÄÐÞÊÎϸ½Ú£¿
10Â¥2012-04-08 14:31:10
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
ÆÕͨ»ØÌû

huahua1216

ÖÁ×ðľ³æ (ÎÄ̳¾«Ó¢)

¡¾´ð°¸¡¿Ó¦Öú»ØÌû

¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï
¸Ðл²ÎÓ룬ӦÖúÖ¸Êý +1
lijunjie84: ½ð±Ò+1, »¶Ó­»ØÌû½»Á÷£¡ 2012-04-06 15:48:52
ɽʯÑÒ: ½ð±Ò+10, ¡ïÓаïÖú, лл 2012-04-13 09:24:34
1. ¸ø³ö¶þÃæ½ÇµÄ±ê׼ƫ²î Ò»°ãÓÃxpµÄmpla°É
2.¼ì²éһϽâÎöʱFriedel pairsÓ¦¸Ã¾«ÐÞÁË£¬Ã»ÓÐmerged
3.¼òÒªÃèÊöÏÂÎÞÐòµÄ´¦Àí
4.N-HµÄ´¦Àí£¬Ò»°ãÊÇ´Ó¸µÀïҶͼÖÐÕÒµ½È»ºóÊʵ±ÏÞÖÆµÄ°É£¬¾ßÌå¿´×Ô¼ºµÄ½á¹¹

²»¶®µÄ»°Çë½Ì½âÎöµÄÀÏʦ°É
2Â¥2012-04-06 11:24:33
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

lgzhu1964

ÖÁ×ðľ³æ (ÖøÃûдÊÖ)

¡ï
lijunjie84: ½ð±Ò+1, nice£¡£¡£¡ 2012-04-06 15:49:09
1.ÕªÒªÓëÆÀÂÛ²¿·ÖËùÓжþÃæ½ÇÔö¼ÓÆ«²îÖµ£¨ÓÃÀ¨ºÅÀ¨ÆðÀ´£©£»
2.ÔÚʵÑ龫ÐÞ²¿·Ö£¬ÄãÖ¸³öÁËFriedal¶ÔºÏ²¢ÁË£¬µ«ÊÂʵÉϲ»ÊÇÈç´Ë£¬ÇëÔÙ¼ì²é²¢¸ÄÕý£®
3.ÇëÔÚʵÑ龫ÐÞ²¿·ÖÌṩÓйؽṹÖÐÎÞÐòµÄÏêϸÐÅÏ¢£®¼´ÄãÕâ¸ö½á¹¹ÖÐÓÐÎÞÐò£¬Ó¦¸Ã¼ÓÒÔÃèÊö£®
4.ÔÚʵÑ龫ÐÞ²¿·ÖÇëÌṩÓйØN-HÖÊ×ÓÈ·¶¨Ó뾫ÐÞµÄϸ½Ú£¬¼´ÄãÊÇÈçºÎ¼ÓÕâ¸öÇâµÄ£¬ÈçºÎ¾«Ð޵ģ¬ÀýÈçÓзñ¼ü³¤ÏÞÖÆµÈ£®

» ±¾ÌûÒÑ»ñµÃµÄºì»¨£¨×îÐÂ10¶ä£©

3Â¥2012-04-06 11:26:30
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

ɽʯÑÒ

½ð³æ (ÖøÃûдÊÖ)

ÒýÓûØÌû:
2Â¥: Originally posted by huahua1216 at 2012-04-06 11:24:33:
1. ¸ø³ö¶þÃæ½ÇµÄ±ê׼ƫ²î Ò»°ãÓÃxpµÄmpla°É
2.¼ì²éһϽâÎöʱFriedel pairsÓ¦¸Ã¾«ÐÞÁË£¬Ã»ÓÐmerged
3.¼òÒªÃèÊöÏÂÎÞÐòµÄ´¦Àí
4.N-HµÄ´¦Àí£¬Ò»°ãÊÇ´Ó¸µÀïҶͼÖÐÕÒµ½È»ºóÊʵ±ÏÞÖÆµÄ°É£¬¾ßÌå¿´×Ô¼ºµÄ½á¹¹

²»¶®µÄ ...

ºÇºÇ£¬Ð»Ð»¡£ÎÒ»¹ÏëÇë½Ìһϣ¬µÚ¶þ¸öÎÊÌâÊÇÏëÈÃÎÒ½«Friendel pairs Merged Â𣿲»ÊÇÎÒ×Ô¼º´¦ÀíµÄ¾§Ì壬ÎÒÒªÔõôÃèÊöÎÞÐòÄØ£¿
4Â¥2012-04-06 18:39:55
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

ɽʯÑÒ

½ð³æ (ÖøÃûдÊÖ)

ËÍÏÊ»¨Ò»¶ä
ÒýÓûØÌû:
3Â¥: Originally posted by lgzhu1964 at 2012-04-06 11:26:30:
1.ÕªÒªÓëÆÀÂÛ²¿·ÖËùÓжþÃæ½ÇÔö¼ÓÆ«²îÖµ£¨ÓÃÀ¨ºÅÀ¨ÆðÀ´£©£»
2.ÔÚʵÑ龫ÐÞ²¿·Ö£¬ÄãÖ¸³öÁËFriedal¶ÔºÏ²¢ÁË£¬µ«ÊÂʵÉϲ»ÊÇÈç´Ë£¬ÇëÔÙ¼ì²é²¢¸ÄÕý£®
3.ÇëÔÚʵÑ龫ÐÞ²¿·ÖÌṩÓйؽṹÖÐÎÞÐòµÄÏêϸÐÅÏ¢£®¼´ÄãÕâ¸ö½á¹¹ÖÐ ...

ллŶ£¬ÎÒÔÙÇë½Ìһϣ¬ÄǸö½á¹¹ÓÐÒ»¸ö±½»·ÎÞÐò£¬¾ßÌåÒªÔõôÃèÊöÄØ£¿»¹ÓÐ×îºóÒ»¸ö¼ü³¤µÄÏÞÖÆÖ®ÀàµÄÎÒÓ¦¸ÃÔÚÄÄÀï¿´£¿
Ps£ºÎÒÊÇÕÒÈ˰ïæ¾«Ð޵ľ§Ì壬ËùÒÔ»ù±¾Éϲ»¶®¡£Ð»Ð»°¡
5Â¥2012-04-06 18:43:01
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

lgzhu1964

ÖÁ×ðľ³æ (ÖøÃûдÊÖ)

ÒýÓûØÌû:
5Â¥: Originally posted by ɽʯÑÒ at 2012-04-06 18:43:01:
ллŶ£¬ÎÒÔÙÇë½Ìһϣ¬ÄǸö½á¹¹ÓÐÒ»¸ö±½»·ÎÞÐò£¬¾ßÌåÒªÔõôÃèÊöÄØ£¿»¹ÓÐ×îºóÒ»¸ö¼ü³¤µÄÏÞÖÆÖ®ÀàµÄÎÒÓ¦¸ÃÔÚÄÄÀï¿´£¿
Ps£ºÎÒÊÇÕÒÈ˰ïæ¾«Ð޵ľ§Ì壬ËùÒÔ»ù±¾Éϲ»¶®¡£Ð»Ð»°¡

ÔõôÐÞµÄÔõôд£¬CIFÖÐÄÜ¿´³öÀ´£¨Ö÷ҪдռÓÐÂÊÊǶàÉÙ£©¼ü³¤ÏÞÖÆ¿´CIFÒ²¿É¿´insÎļþ£®
6Â¥2012-04-06 21:46:40
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

vink

ľ³æ (ÖøÃûдÊÖ)

¡¾´ð°¸¡¿Ó¦Öú»ØÌû

¸Ðл²ÎÓ룬ӦÖúÖ¸Êý +1
±ðÕÛÌÚÁË£¬ÕÒÈ˰ïæ°É£¬ÓÐÎÞÐò£¬ÄãÒ»»á°ë»áŪ²»Ã÷°×µÄ£¬ºÎ¿ö¶¼Í¶¸åÁË£¬ÄÄÀïÓÐÄÇô¶àʱ¼äµÈ¡£
7Â¥2012-04-07 10:01:00
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

lgzhu1964

ÖÁ×ðľ³æ (ÖøÃûдÊÖ)

¡¾´ð°¸¡¿Ó¦Öú»ØÌû

¸Ðл²ÎÓ룬ӦÖúÖ¸Êý +1
ÒýÓûØÌû:
8Â¥: Originally posted by ɽʯÑÒ at 2012-04-08 11:14:52:
ллÀ²£¬µ«ÊÇÒª¿´ÄÇЩÊý¾Ý²ÅÄÜ¿´³öÀ´ÄØ £¿

CIFÖÐÓÐÈçÏÂÊý¾Ý£º
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group

ÆäÖУº _atom_site_occupancy£¬¾ÍÊÇÕ¼ÓÐÂÊ£®

» ±¾ÌûÒÑ»ñµÃµÄºì»¨£¨×îÐÂ10¶ä£©

9Â¥2012-04-08 14:14:40
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
Ïà¹Ø°æ¿éÌø×ª ÎÒÒª¶©ÔÄÂ¥Ö÷ ɽʯÑÒ µÄÖ÷Ìâ¸üÐÂ
×î¾ßÈËÆøÈÈÌûÍÆ¼ö [²é¿´È«²¿] ×÷Õß »Ø/¿´ ×îºó·¢±í
[¿¼ÑÐ] ¿¼Ñл¯Ñ§Ñ§Ë¶µ÷¼Á£¬Ò»Ö¾Ô¸985 +3 ÕÅvvvv 2026-03-15 5/250 2026-03-16 20:25 by ÕÅvvvv
[¿¼ÑÐ] 0703»¯Ñ§µ÷¼Á£¬Çó¸÷λÀÏʦÊÕÁô +8 ÇïÓÐľ±± 2026-03-14 8/400 2026-03-16 15:21 by ŶŶ123
[¿¼ÑÐ] 070303Ò»Ö¾Ô¸Î÷±±´óѧѧ˶310ÕÒµ÷¼Á +5 dÈçÔ¸Éϰ¶ 2026-03-12 8/400 2026-03-16 15:19 by peike
[¿¼ÑÐ] 0703 ÎïÀí»¯Ñ§µ÷¼Á +3 ÎÒ¿ÉÒÔÉϰ¶µÄ¶Ô 2026-03-13 5/250 2026-03-16 10:50 by ÎÒ¿ÉÒÔÉϰ¶µÄ¶ÔÂ
[¿¼ÑÐ] 290Çóµ÷¼Á +5 ¿×Ö¾ºÆ 2026-03-12 10/500 2026-03-16 09:01 by ÓàêÍ&
[¿¼ÑÐ] 327Çóµ÷¼Á +6 ʰ¹âÈÎȾ 2026-03-15 11/550 2026-03-15 22:47 by ʰ¹âÈÎȾ
[¿¼ÑÐ] 0856ר˶279Çóµ÷¼Á +5 ¼ÓÓͼÓÓÍ£¡? 2026-03-15 5/250 2026-03-15 11:58 by 2020015
[¿¼ÑÐ] ²ÄÁÏÓ뻯¹¤ 323 Ó¢Ò»+Êý¶þ+Îﻯ£¬Ò»Ö¾Ô¸£º¹þ¹¤´ó ±¾È˱¾¿ÆË«Ò»Á÷ +4 ×ÔÓɵÄ_·ÉÏè 2026-03-13 5/250 2026-03-14 19:39 by hmn_wj
[¿¼ÑÐ] 265Çóµ÷¼Á +4 Íþ»¯±ý07 2026-03-12 4/200 2026-03-14 17:23 by userper
[»ù½ðÉêÇë] ÏÖÔÚÈçºÎ»Ø±ÜÈ¥ÄêµÄijһ¸öר¼Ò£¬²»ÖªµÀÃû×Ö +3 zk200107 2026-03-12 6/300 2026-03-14 17:13 by zk200107
[¿¼ÑÐ] ²ÄÁÏ080500µ÷¼ÁÇóÊÕÁô +3 Ò»¿Åmeteor 2026-03-13 3/150 2026-03-14 10:54 by peike
[¿¼ÑÐ] 330Çóµ÷¼Á +3 ?½´¸øµ÷¼Á¹òÁË 2026-03-13 3/150 2026-03-14 10:13 by JourneyLucky
[¿¼ÑÐ] 266Çóµ÷¼Á +4 ѧԱ97LZgn 2026-03-13 4/200 2026-03-14 08:37 by zhukairuo
[¿¼ÑÐ] ÕÐÊÕ0805£¨²ÄÁÏ£©µ÷¼Á +3 18595523086 2026-03-13 3/150 2026-03-14 00:33 by 123%¡¢
[¿¼ÑÐ] 26¿¼Ñе÷¼Á +3 ying123. 2026-03-10 3/150 2026-03-14 00:18 by JourneyLucky
[¿¼ÑÐ] 2026¿¼Ñе÷¼Á+±¾¿ÆÑӱߴóѧ+ɽ¶«´óѧ+ÉúÎﻯѧÓë·Ö×ÓÉúÎïѧ+ÓÐÏîÄ¿¾­Ñé +3 ccdsscjy 2026-03-10 3/150 2026-03-14 00:12 by JourneyLucky
[¿¼ÑÐ] 307Çóµ÷¼Á +5 ³¬¼¶ÒÁ°º´óÍõ 2026-03-12 5/250 2026-03-13 15:56 by °ô°ôÇòÊÖ
[¿¼ÑÐ] ²ÄÁÏר˶274Ò»Ö¾Ô¸ÉÂÎ÷ʦ·¶´óѧÇóµ÷¼Á +4 Ñ¦ÔÆÅô 2026-03-13 4/200 2026-03-13 10:40 by ѧԱ8dgXkO
[¿¼ÑÐ] 321Çóµ÷¼Á£¨Ê³Æ·/ר˶£© +3 xc321 2026-03-12 6/300 2026-03-13 08:45 by xc321
[¿¼ÑÐ] 290Çóµ÷¼Á +3 ¿Â»´È» 2026-03-10 8/400 2026-03-11 13:48 by ¿Â»´È»
ÐÅÏ¢Ìáʾ
ÇëÌî´¦ÀíÒâ¼û