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I have reviewed your structure report and before going into any detail I would like to ask whether there is a possibility to find a better crystal? You report only 1862 observed reflections but 268 refined parameters. Since the data/parameter ratio for a properly refined structure should approximately be 10 your data set contains not enough data to refine such a number of parameters. In additon, there are no negative intensities in the data set. Have they been merged? Probably because there were too much of them due to a either very small or unsufficiently diffracting crystal? If I additionally take into account that for a refinement with a low data/parameter ratio R values are lower due to statistic effects, your structure from my point of view does not meet the standards of Acta E. |
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- ×¢²á: 2010-05-17
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7Â¥2012-04-03 20:51:40
elwew
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3Â¥2012-04-03 08:38:00
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lijunjie84: ½ð±Ò+1, »¶Ó»ØÌû½»Á÷£¡£¡£¡ 2012-04-03 12:03:20
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5Â¥2012-04-03 09:21:39









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