| 查看: 1908 | 回复: 13 | ||
| 当前只显示满足指定条件的回帖，点击这里查看本话题的所有回帖 | ||
elwew木虫 (正式写手)
|
[求助]
编辑给的回信是这样，是不是就发不了单晶了？还有什么补救办法吗
|
|
|
I have reviewed your structure report and before going into any detail I would like to ask whether there is a possibility to find a better crystal? You report only 1862 observed reflections but 268 refined parameters. Since the data/parameter ratio for a properly refined structure should approximately be 10 your data set contains not enough data to refine such a number of parameters. In additon, there are no negative intensities in the data set. Have they been merged? Probably because there were too much of them due to a either very small or unsufficiently diffracting crystal? If I additionally take into account that for a refinement with a low data/parameter ratio R values are lower due to statistic effects, your structure from my point of view does not meet the standards of Acta E. |
回复此楼» 猜你喜欢
MOF合成
已经有0人回复
-
请问各位大佬ACS投稿状态这样是成功了吗？
已经有6人回复
-
无机化学论文润色/翻译怎么收费?
已经有114人回复
» 本主题相关价值贴推荐，对您同样有帮助:
什么叫大修？文章大修是不是非得对原论文作大的改动？
已经有25人回复- 没有送审，编辑说超出杂志范围，请大家帮忙看看！
已经有13人回复
- 求问我这样用DMOL3算吸附过程对不对
已经有7人回复
- 回答网友关于单晶结构精修的问题
已经有22人回复
- 又收到一位德国教授回信让我申洪堡，肿么办
已经有32人回复
- 单晶培养中可溶与不可溶溶剂的比例问题
已经有14人回复
- 导师又回信了，求指点
已经有46人回复
- 如何取出单晶金属配合物？
已经有7人回复
- 我发了封催稿的信。编辑回信“I need ECM # for search”。ECM是什么意思呀？
已经有4人回复
- 单晶数据能不能发SCI？
已经有11人回复
- 【求助】投稿回信中的单晶结构问题？？？急！！
已经有11人回复
- 关于给编辑的回信
已经有3人回复
marise
木虫 (小有名气)
- 应助: 17 (小学生)
- 金币: 2303.2
- 红花: 1
- 帖子: 257
- 在线: 71.4小时
- 虫号: 434856
- 注册: 2007-08-19
- 性别: MM
- 专业: 英语翻译
elwew4楼2012-04-03 09:14:43