| 查看: 362 | 回复: 3 | |||
| 当前只显示满足指定条件的回帖，点击这里查看本话题的所有回帖 | |||
xiaofei523金虫 (正式写手)
|
[求助]
CIF错误
|
||
我昨天给大家看的那个错误改了以后觉得没什么问题了怎么还是出现下面的提示？？ 1H -benzo[d]imidzol-1-ol (1 mmol) was added to the solution of acetone (10 ml) with potassium carbonate (1.5 mmol) in a Schlenk flask. After stirring for 10 min, 1-chloro-2-(chloromethyl)benzene and (1 mmol) was added to the mixture. The mixture was refluxing for 5 h. After cooling down to the room temperature, stick-shaped crystals were formed, which was filtered off, washed with acetone and dried in the air. >>> "1H" *** There is an unexpected word or number as indicated. This may be because a loop is intended but the loop_ keyword has been missed out; or a phrase with several words is not enclosed in matching delimiting quote marks; or a text field (extending over several lines) is not properly closed with a final semicolon; or a data_ block header has not yet been seen. ERROR: Unexpected string (-benzo[d]imidzol-1-ol) at line 115 ERROR: Unexpected string ((1) at line 115 ERROR: Unexpected string (mmol)) at line 115 ERROR: Unexpected string (was) at line 115 ERROR: Unexpected string (added) at line 115 ERROR: Unexpected string (to) at line 115 ERROR: Unexpected string (the) at line 116 >>> "the" ERROR: Unexpected string (solution) at line 116 ERROR: Unexpected string (of) at line 116 ERROR: Unexpected string (acetone) at line 116 ERROR: Unexpected string ((10) at line 116 ERROR: Unexpected string (ml)) at line 116 ERROR: Unexpected string (with) at line 116 ERROR: Unexpected string (potassium) at line 116 ERROR: Unexpected string (carbonate) at line 116 ERROR: Unexpected string ((1.5) at line 117 >>> "(1.5" ERROR: Unexpected string (mmol)) at line 117 ERROR: Unexpected string (in) at line 117 ERROR: Unexpected string (a) at line 117 |
回复此楼» 猜你喜欢
中南大学易小艺课题组诚招2026申请-考核制博士生
已经有0人回复
-
海南师范大学招收化学博士（光电功能材料课题组招收博士研究生）
已经有10人回复
-
无机化学论文润色/翻译怎么收费?
已经有208人回复
-
求助几个团簇的cif
已经有0人回复
-
急求该反应的详细机理
已经有5人回复
-
【Ei | Scopus 双检索】2026年智能交通与未来出行国际会议（CSTFM 2026）
已经有0人回复
-
【EI|Scopus 双检索】2026年第六届机器人与人工智能国际会议（JCRAI 2026）
已经有0人回复
marise
木虫 (小有名气)
- 应助: 17 (小学生)
- 金币: 2303.2
- 红花: 1
- 帖子: 257
- 在线: 71.4小时
- 虫号: 434856
- 注册: 2007-08-19
- 性别: MM
- 专业: 英语翻译
|
_publ_section_exptl_prep ; 1H -benzo[d]imidzol-1-ol (1 mmol) was added to the solution of acetone (10 ml) with potassium carbonate (1.5 mmol) in a Schlenk flask. After stirring for 10 min, 1-chloro-2-(chloromethyl)benzene and (1 mmol) was added to the mixture. The mixture was refluxing for 5 h. After cooling down to the room temperature, stick-shaped crystals were formed, which was filtered off, washed with acetone and dried in the air. ; _publ_section_exptl_refinement |
4楼2012-01-16 11:56:18
marise
木虫 (小有名气)
- 应助: 17 (小学生)
- 金币: 2303.2
- 红花: 1
- 帖子: 257
- 在线: 71.4小时
- 虫号: 434856
- 注册: 2007-08-19
- 性别: MM
- 专业: 英语翻译
3楼2012-01-16 11:54:34