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xiaofei523金虫 (正式写手)
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[求助]
CIF错误
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我昨天给大家看的那个错误改了以后觉得没什么问题了怎么还是出现下面的提示？？ 1H -benzo[d]imidzol-1-ol (1 mmol) was added to the solution of acetone (10 ml) with potassium carbonate (1.5 mmol) in a Schlenk flask. After stirring for 10 min, 1-chloro-2-(chloromethyl)benzene and (1 mmol) was added to the mixture. The mixture was refluxing for 5 h. After cooling down to the room temperature, stick-shaped crystals were formed, which was filtered off, washed with acetone and dried in the air. >>> "1H" *** There is an unexpected word or number as indicated. This may be because a loop is intended but the loop_ keyword has been missed out; or a phrase with several words is not enclosed in matching delimiting quote marks; or a text field (extending over several lines) is not properly closed with a final semicolon; or a data_ block header has not yet been seen. ERROR: Unexpected string (-benzo[d]imidzol-1-ol) at line 115 ERROR: Unexpected string ((1) at line 115 ERROR: Unexpected string (mmol)) at line 115 ERROR: Unexpected string (was) at line 115 ERROR: Unexpected string (added) at line 115 ERROR: Unexpected string (to) at line 115 ERROR: Unexpected string (the) at line 116 >>> "the" ERROR: Unexpected string (solution) at line 116 ERROR: Unexpected string (of) at line 116 ERROR: Unexpected string (acetone) at line 116 ERROR: Unexpected string ((10) at line 116 ERROR: Unexpected string (ml)) at line 116 ERROR: Unexpected string (with) at line 116 ERROR: Unexpected string (potassium) at line 116 ERROR: Unexpected string (carbonate) at line 116 ERROR: Unexpected string ((1.5) at line 117 >>> "(1.5" ERROR: Unexpected string (mmol)) at line 117 ERROR: Unexpected string (in) at line 117 ERROR: Unexpected string (a) at line 117 |
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marise
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_publ_section_exptl_prep ; 1H -benzo[d]imidzol-1-ol (1 mmol) was added to the solution of acetone (10 ml) with potassium carbonate (1.5 mmol) in a Schlenk flask. After stirring for 10 min, 1-chloro-2-(chloromethyl)benzene and (1 mmol) was added to the mixture. The mixture was refluxing for 5 h. After cooling down to the room temperature, stick-shaped crystals were formed, which was filtered off, washed with acetone and dried in the air. ; _publ_section_exptl_refinement |
4楼2012-01-16 11:56:18
marise
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3楼2012-01-16 11:54:34
