| 查看: 387 | 回复: 3 | |||
xiaofei523版主
|
[求助]
CIF错误
|
我昨天给大家看的那个错误改了以后觉得没什么问题了怎么还是出现下面的提示？？ 1H -benzo[d]imidzol-1-ol (1 mmol) was added to the solution of acetone (10 ml) with potassium carbonate (1.5 mmol) in a Schlenk flask. After stirring for 10 min, 1-chloro-2-(chloromethyl)benzene and (1 mmol) was added to the mixture. The mixture was refluxing for 5 h. After cooling down to the room temperature, stick-shaped crystals were formed, which was filtered off, washed with acetone and dried in the air. >>> "1H" *** There is an unexpected word or number as indicated. This may be because a loop is intended but the loop_ keyword has been missed out; or a phrase with several words is not enclosed in matching delimiting quote marks; or a text field (extending over several lines) is not properly closed with a final semicolon; or a data_ block header has not yet been seen. ERROR: Unexpected string (-benzo[d]imidzol-1-ol) at line 115 ERROR: Unexpected string ((1) at line 115 ERROR: Unexpected string (mmol)) at line 115 ERROR: Unexpected string (was) at line 115 ERROR: Unexpected string (added) at line 115 ERROR: Unexpected string (to) at line 115 ERROR: Unexpected string (the) at line 116 >>> "the" ERROR: Unexpected string (solution) at line 116 ERROR: Unexpected string (of) at line 116 ERROR: Unexpected string (acetone) at line 116 ERROR: Unexpected string ((10) at line 116 ERROR: Unexpected string (ml)) at line 116 ERROR: Unexpected string (with) at line 116 ERROR: Unexpected string (potassium) at line 116 ERROR: Unexpected string (carbonate) at line 116 ERROR: Unexpected string ((1.5) at line 117 >>> "(1.5" ERROR: Unexpected string (mmol)) at line 117 ERROR: Unexpected string (in) at line 117 ERROR: Unexpected string (a) at line 117 |
回复此楼» 猜你喜欢
26年博士招生
已经有16人回复
-
江西理工大学功能晶态材料方向刘遂军课题组招收2026年秋季入学博士研究生
已经有11人回复
-
无机化学论文润色/翻译怎么收费?
已经有141人回复
-
宁夏大学团簇新材料团队招收材料/化学/化工专业博士生
已经有0人回复
-
MIL-101有单晶样品吗
已经有1人回复
-
已删除
已经有3人回复
-
收调剂研究生
已经有2人回复
-
【2026 考研调剂】哈尔滨工程大学核科学与技术学院核化工系 招收调剂生
已经有3人回复
-
【2026 考研调剂】哈尔滨工程大学核科学与技术学院核化工系 招收调剂生
已经有1人回复
-
广州大学环境大分子材料研究所2026年研究生招生简章
已经有0人回复
xiaofei523
版主
|
|
2楼2012-01-16 09:20:49
3楼2012-01-16 11:54:34
|
_publ_section_exptl_prep ; 1H -benzo[d]imidzol-1-ol (1 mmol) was added to the solution of acetone (10 ml) with potassium carbonate (1.5 mmol) in a Schlenk flask. After stirring for 10 min, 1-chloro-2-(chloromethyl)benzene and (1 mmol) was added to the mixture. The mixture was refluxing for 5 h. After cooling down to the room temperature, stick-shaped crystals were formed, which was filtered off, washed with acetone and dried in the air. ; _publ_section_exptl_refinement |
4楼2012-01-16 11:56:18
