| 查看: 413 | 回复: 3 | ||
xiaofei523金虫 (正式写手)
|
[求助]
CIF错误
|
我昨天给大家看的那个错误改了以后觉得没什么问题了怎么还是出现下面的提示？？ 1H -benzo[d]imidzol-1-ol (1 mmol) was added to the solution of acetone (10 ml) with potassium carbonate (1.5 mmol) in a Schlenk flask. After stirring for 10 min, 1-chloro-2-(chloromethyl)benzene and (1 mmol) was added to the mixture. The mixture was refluxing for 5 h. After cooling down to the room temperature, stick-shaped crystals were formed, which was filtered off, washed with acetone and dried in the air. >>> "1H" *** There is an unexpected word or number as indicated. This may be because a loop is intended but the loop_ keyword has been missed out; or a phrase with several words is not enclosed in matching delimiting quote marks; or a text field (extending over several lines) is not properly closed with a final semicolon; or a data_ block header has not yet been seen. ERROR: Unexpected string (-benzo[d]imidzol-1-ol) at line 115 ERROR: Unexpected string ((1) at line 115 ERROR: Unexpected string (mmol)) at line 115 ERROR: Unexpected string (was) at line 115 ERROR: Unexpected string (added) at line 115 ERROR: Unexpected string (to) at line 115 ERROR: Unexpected string (the) at line 116 >>> "the" ERROR: Unexpected string (solution) at line 116 ERROR: Unexpected string (of) at line 116 ERROR: Unexpected string (acetone) at line 116 ERROR: Unexpected string ((10) at line 116 ERROR: Unexpected string (ml)) at line 116 ERROR: Unexpected string (with) at line 116 ERROR: Unexpected string (potassium) at line 116 ERROR: Unexpected string (carbonate) at line 116 ERROR: Unexpected string ((1.5) at line 117 >>> "(1.5" ERROR: Unexpected string (mmol)) at line 117 ERROR: Unexpected string (in) at line 117 ERROR: Unexpected string (a) at line 117 |
回复此楼» 猜你喜欢
江西科技师范大学物理化学课题组接收调剂生，12点开启，速来
已经有0人回复
-
【2026 考研调剂】哈尔滨工程大学 招收学硕调剂生（英语一、数学一）
已经有0人回复
-
无机化学论文润色/翻译怎么收费?
已经有237人回复
-
四川轻化工大学化学与环境工程学院 付昱教授课题组招收调剂硕士研究生
已经有11人回复
-
大连化物所招收有机背景的博士候选人
已经有0人回复
-
在MOF中，有没有羧基参加配位的情况
已经有2人回复
-
招2026年入学上海交通大学博士生，急！！！
已经有1人回复
-
理论计算合作
已经有0人回复
xiaofei523
金虫 (正式写手)
|
|
2楼2012-01-16 09:20:49
marise
木虫 (小有名气)
- 应助: 17 (小学生)
- 金币: 2303.2
- 红花: 1
- 帖子: 257
- 在线: 71.4小时
- 虫号: 434856
- 注册: 2007-08-19
- 性别: MM
- 专业: 英语翻译
3楼2012-01-16 11:54:34
marise
木虫 (小有名气)
- 应助: 17 (小学生)
- 金币: 2303.2
- 红花: 1
- 帖子: 257
- 在线: 71.4小时
- 虫号: 434856
- 注册: 2007-08-19
- 性别: MM
- 专业: 英语翻译
|
_publ_section_exptl_prep ; 1H -benzo[d]imidzol-1-ol (1 mmol) was added to the solution of acetone (10 ml) with potassium carbonate (1.5 mmol) in a Schlenk flask. After stirring for 10 min, 1-chloro-2-(chloromethyl)benzene and (1 mmol) was added to the mixture. The mixture was refluxing for 5 h. After cooling down to the room temperature, stick-shaped crystals were formed, which was filtered off, washed with acetone and dried in the air. ; _publ_section_exptl_refinement |
4楼2012-01-16 11:56:18
5