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xiaofei523

金虫 (正式写手)

[求助] 求助CIF 错误提示

哪位大侠看一哈!我在提交CIF文件中
_publ_section_exptl_prep
;
A mixture of 1H-benzo[d]imidazol-1-ol
(1 mmol) and 1-chloro-2-(chloromethyl)benzene (1 mmol)
was stirred in refluxing acetone (10 mL).
The progress of the reaction was monitored by TLC. After the completion
of the reaction, the mixture was cooled to room temperature,
stick-shaped crystals were formed, which was filtered off, washed with
ethanol and dried in the air.
;
这一栏提示下面错误,实在不知道哪里出错了?给指导一哈!非常感谢!


Please fix this problem before trying to resubmit. If you continue
ERROR: Unexpected string (A) at line 115
>>> "A"
*** There is an unexpected word or number as indicated. This may be because
    a loop is intended but the loop_ keyword has been missed out; or a phrase
    with several words is not enclosed in matching delimiting quote marks;
    or a text field (extending over several lines) is not properly closed
    with a final semicolon; or a data_ block header has not yet been seen.
ERROR: Unexpected string (mixture) at line 115
ERROR: Unexpected string (of) at line 115
ERROR: Unexpected string (1) at line 115
ERROR: Unexpected string (H) at line 115
ERROR: Unexpected string (-benzo[d]imidazol-1-ol) at line 115
ERROR: Unexpected string ((1) at line 115
ERROR: Unexpected string (mmol)) at line 115
ERROR: Unexpected string (and) at line 115
ERROR: Unexpected string (1-chloro-2-(chloromethyl)benzene) at line 116
>>> "1-chloro-2-(chloromethyl)benzene"
ERROR: Unexpected string ((1) at line 116
ERROR: Unexpected string (mmol)) at line 116
ERROR: Unexpected string (was) at line 116
ERROR: Unexpected string (stirred) at line 116
ERROR: Unexpected string (in) at line 116
ERROR: Unexpected string (acetone) at line 116
ERROR: Unexpected string ((10) at line 117
>>> "(10"
ERROR: Unexpected string (mL).The) at line 117
ERROR: Unexpected string (progress) at line 117
ERROR: Unexpected string (of) at line 117
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xiaoshan1988

木虫 (小有名气)

【答案】应助回帖

★
感谢参与,应助指数 +1
xiaofei523(金币+2): ★有帮助 谢谢! 2012-01-15 19:19:45
drg1984(金币+1): 感谢热心帮助! 2012-01-15 22:57:56
你的cif里面出现了不该出现的字符了。看看是不是语法出现错误 了。标点符号之类的
2楼2012-01-15 17:39:06
已阅   关注TA 给TA发消息 送TA红花 TA的回帖

xiaoshan1988

木虫 (小有名气)

【答案】应助回帖

★
xiaofei523(金币+2): ★有帮助 谢谢! 2012-01-15 19:19:35
drg1984(金币+1): 感谢热心帮助! 2012-01-15 22:58:09
看看 115  116   117行是不是标点符号或者语法这类的错了
3楼2012-01-15 17:39:50
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