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xiaofei523

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注册: 2008-06-01
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专业: 化学生物学与生物有机化学

[求助] 求助CIF 错误提示

哪位大侠看一哈！我在提交CIF文件中
_publ_section_exptl_prep
;
A mixture of 1H-benzo[d]imidazol-1-ol
(1 mmol) and 1-chloro-2-(chloromethyl)benzene (1 mmol)
was stirred in refluxing acetone (10 mL).
The progress of the reaction was monitored by TLC. After the completion
of the reaction, the mixture was cooled to room temperature,
stick-shaped crystals were formed, which was filtered off, washed with
ethanol and dried in the air.
;
这一栏提示下面错误，实在不知道哪里出错了？给指导一哈！非常感谢！

Please fix this problem before trying to resubmit. If you continue
ERROR: Unexpected string (A) at line 115
>>> "A"
*** There is an unexpected word or number as indicated. This may be because
a loop is intended but the loop_ keyword has been missed out; or a phrase
with several words is not enclosed in matching delimiting quote marks;
or a text field (extending over several lines) is not properly closed
with a final semicolon; or a data_ block header has not yet been seen.
ERROR: Unexpected string (mixture) at line 115
ERROR: Unexpected string (of) at line 115
ERROR: Unexpected string (1) at line 115
ERROR: Unexpected string (H) at line 115
ERROR: Unexpected string (-benzo[d]imidazol-1-ol) at line 115
ERROR: Unexpected string ((1) at line 115
ERROR: Unexpected string (mmol)) at line 115
ERROR: Unexpected string (and) at line 115
ERROR: Unexpected string (1-chloro-2-(chloromethyl)benzene) at line 116
>>> "1-chloro-2-(chloromethyl)benzene"
ERROR: Unexpected string ((1) at line 116
ERROR: Unexpected string (mmol)) at line 116
ERROR: Unexpected string (was) at line 116
ERROR: Unexpected string (stirred) at line 116
ERROR: Unexpected string (in) at line 116
ERROR: Unexpected string (acetone) at line 116
ERROR: Unexpected string ((10) at line 117
>>> "(10"
ERROR: Unexpected string (mL).The) at line 117
ERROR: Unexpected string (progress) at line 117
ERROR: Unexpected string (of) at line 117

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