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chenyuejiao

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[求助] 求助粉末衍射数据库（JCPDS）中的ZnSnO3卡片数据

求助粉末衍射数据库（JCPDS）中的ZnSnO3卡片数据
11-274 ZnSnO3
我这里只有晶面间距没有晶面的数据
希望哪位神仙可以帮忙把这个参数完整数据找出来多谢

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1楼 2012-01-09 22:44:31

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xhtangxh

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★
感谢参与，应助指数 +1
chenyuejiao(金币+2): 2012-01-10 10:33:10
huangjr(金币+1): 感谢回帖交流~ 2012-01-11 09:34:17

Card Information
Names: Zinc Tin Oxide
Formula: Zn Sn O3
PDF Number: 52-1381
Quality: indexed
Subfiles: inorganic COR

Cell and Symmetry Information
System: rhombohedral Space Group: R3    (no. 146)
a: 5.2835 c: 14.0913
Z: 6

Instrument Information
Radiation: CuKa Wavelength: 1.5418    Filter: Ni
Instrument(d): diffractometer
Instrument(I): diffractometer I type: unknown

Comments and Additional Information
Preparation: Prepared by an ion exchange reaction between solid alpha-Li2 Sn O3\ and a melt of Zn Cl2-K Cl at 350 C for 48 hours.

Literature References
General: Kovacheva, D., Petrov, K. Solid State Ionics  109 327 (1998)

Peak Data
Note : Wavelength of 1.5418 A
PeakList
   h    k    l    d    I
   0    0    3 4.6900    12
   1    0    1 4.3600    7
   0    1    2 3.8400    20
   1    0    4 2.7900    100
   1    1    0 2.6400    88
   0    1    5 2.4000    2
   0    0    6 2.3490    6
   1    1    3 2.3030    19
   2    0    2 2.1760    3
   0    2    4 1.9180    26
   1    0    7 1.8420    2
   1    1    6 1.7550    45
   1    2    2 1.6790    4
   0    1    8 1.6400    9
   2    1    4 1.5530    32
   3    0    0 1.5260    25
   3    0    3 1.4510    3
   2    0    8 1.3960    3
   1    1    9 1.3470    12
   1    0 10 1.3470    12
   2    2    0 1.3210    9
   3    0    6 1.2790    4
   1    2    8 1.2340    4
   0    2 10 1.1998    5
   1    3    4 1.1939    9
   2    2    6 1.1513    8
   3    0    9 1.0924    11
   2    1 10 1.0924    11
   4    0    4 1.0880    4
   1    0 13 1.0547    2
   3    1    8 1.0296    2
   2    2    9 1.0096    2
   3    2    4 1.0060    7
   4    1    0 0.9984    7
   0    1 14 0.9831    3
   4    1    3 0.9767    2

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2楼2012-01-10 08:52:31

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chenyuejiao

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引用回帖:

楼: Originally posted by xhtangxh at 2012-01-10 08:52:31:
Card Information
Names: Zinc Tin Oxide
Formula: Zn Sn O3
PDF Number: 52-1381
Quality: indexed
Subfiles: inorganic COR

Cell and Symmetry Information
System: rhombohedral Space Group: R3 ...

你这个不是我要的图谱这个我有我要的是11-274的图谱不过还是谢谢！

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3楼2012-01-10 10:32:02

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xhtangxh

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★
huangjr(金币+1): 感谢回帖交流~ 2012-01-11 09:34:53
chenyuejiao(金币+1): ★有帮助 2012-01-11 10:33:14

PDF No. 11-274是数据质量被列为不可靠的图谱类型，你要是发文章而引此作为标准的话，内行人可能会认为你水平很洼的。ICDD收录ZnSnO3的PDF数据总共4个，除11-274和52-1381外还有28-1486和89-95，其中11-274数据存在疑问，不足以确定物相结构，是不会有晶面指标数据的，而28-1486收录后被发现是Zn2SnO4和SnO2的混合物遭弃用，89-95则是根据52-1381数据精修后建立的，实为同一物相。

看看11-274的描述就知道这个数据无参考价值了：
Card Information
Names: Zinc Tin Oxide
Formula: Zn Sn O3
PDF Number: 11-274
Quality: questionable
Subfiles: inorganic

Cell and Symmetry Information
System: unknown

Instrument Information
Radiation: Wavelength:
Instrument(d): unknown
Instrument(I): unknown I type: unknown

Literature References
General: New Jersey Zinc Co., Palmerton, PA, USA. Private Communication ( )
... ...

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4楼2012-01-11 09:19:57

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chenyuejiao

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楼: Originally posted by xhtangxh at 2012-01-11 09:19:57:
PDF No. 11-274是数据质量被列为不可靠的图谱类型，你要是发文章而引此作为标准的话，内行人可能会认为你水平很洼的。ICDD收录ZnSnO3的PDF数据总共4个，除11-274和52-1381外还有28-1486和89-95，其中11-274数据存 ...

谢谢你的建议但是我测出来的XRD就和11-274完全吻合怎么办呀

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5楼2012-01-11 10:32:56

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【答案】应助回帖

感谢参与，应助指数 +1
chenyuejiao(金币+1): 2012-02-23 10:35:39

求PDF粉末衍射数据库软件，那位好心的能帮帮忙啊，急用！！！

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6楼2012-02-14 16:57:41

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【答案】应助回帖

关于ZnSnO3文章（if＞3.0），95％做得都是11-0274的，大胆的用吧

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7楼2012-08-24 15:33:57

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求助粉末Casio3的晶体结构；
以下是测得的PDF卡片信息，我是新手，求高人指点
PDF#73-1110: QM=Calculated; d=Calculated; I=Calculated
Wollastonite, 1A
Ca Si O3
Radiation=CuKa1 Lambda=1.54060 Filter=
Calibration= d-Cutoff=17.7 I/Ic(RIR)=0.87
Ref= Calculated from ICSD using POWD-12++ (1997)

Triclinic - (Unknown),  P-1 (2) Z=6 mp=
Cell=7.94x7.32x7.07<90.03x95.37x103.43> Pearson=aP30 (?)
Density(c)=2.909 Density(m)=3.070 Mwt=116.16 Vol=397.82 F(30)=94.7(.0067,47)
Ref= Ito, T., Sadanaga, R., Takeuchi, Y., Tokonami, M.
Proc. Jpn. Acad., 45 913 (1969)
Strong Line: 2.98/X 3.32/4 3.09/3 3.52/3 1.83/2 3.84/2 2.48/2 2.18/2 2.31/2 2.19/1
FIZ=023567: At least one TF missing.
Specimen from Hokizawa, Japan.
See PDF 00-042-0547.
Pyroxenoid group.
Calc.
density unusual but tolerable.
See PDF 01-076-0186.
The Existence of Partial Mirrors in Wollastonite i15 (P1-) ABX3
d(A)    I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
7.6870 11.7 4.5 1 0 0      11.502 5.751 0.0650 0.8174
7.1179 0.2 0.1 0 1 0      12.425 6.213 0.0702 0.8827
7.0371 1.3 0.6 0 0 1      12.568 6.284 0.0711 0.8929
5.9621 0.1 0.1 -1 1 0      14.846 7.423 0.0839 1.0539
5.4591 1.4 0.8 -1 0 1      16.223 8.111 0.0916 1.1510
5.0628 0.3 0.2 0 -1 1      17.502 8.751 0.0988 1.2410
4.9478 3.5 2.1 1 0 1      17.913 8.956 0.1011 1.2699
4.9478 3.5 2.1 0 1 1      17.913 8.956 0.1011 1.2699
4.7041 2.1 1.3 1 1 0      18.849 9.424 0.1063 1.3357
4.6788 4.2 2.7 -1 1 1      18.952 9.476 0.1069 1.3429
4.4294 1.8 1.2 1 -1 1      20.030 10.015 0.1129 1.4185
4.0521 10.3 7.6 -1 -1 1      21.917 10.958 0.1234 1.5506
3.8435 20.3 15.7 2 0 0      23.122 11.561 0.1301 1.6348
3.7696 5.4 4.3 -2 1 0      23.582 11.791 0.1326 1.6668
3.5186 28.6 24.2 0 0 2      25.291 12.646 0.1421 1.7857
3.5186 28.6 24.2 -2 0 1      25.291 12.646 0.1421 1.7857
3.4429 7.2 6.2 -2 1 1      25.856 12.928 0.1452 1.8249
3.3228 40.7 36.5 -1 0 2      26.808 13.404 0.1505 1.8909
3.2442 2.0 1.8 2 0 1      27.470 13.735 0.1541 1.9367
3.2061 2.4 2.2 0 -2 1      27.803 13.901 0.1560 1.9597
3.2061 2.4 2.2 -1 2 1      27.803 13.901 0.1560 1.9597
3.1834 5.8 5.4 0 -1 2      28.005 14.003 0.1571 1.9737
3.1066 11.5 11.0 -1 1 2      28.713 14.356 0.1609 2.0225
3.0887 28.7 27.7 2 1 0      28.883 14.441 0.1619 2.0343
3.0887 28.7 27.7 1 0 2      28.883 14.441 0.1619 2.0343
2.9811 100.0 100.0 1 2 0      29.949 14.975 0.1677 2.1077
2.9811 100.0 100.0 -2 2 0      29.949 14.975 0.1677 2.1077
2.9235 7.1 7.2 -1 -1 2      30.553 15.277 0.1710 2.1492
2.9235 7.1 7.2 -2 -1 1      30.553 15.277 0.1710 2.1492
2.8013 3.0 3.2 -1 -2 1      31.921 15.960 0.1785 2.2430
2.8013 3.0 3.2 -2 2 1      31.921 15.960 0.1785 2.2430
2.7449 1.0 1.1 2 1 1      32.595 16.297 0.1822 2.2891
2.7295 6.6 7.2 -2 0 2      32.783 16.392 0.1832 2.3019
2.7224 4.4 4.8 1 1 2      32.871 16.436 0.1837 2.3079
2.6848 1.2 1.3 -2 1 2      33.346 16.673 0.1862 2.3403
2.6848 1.2 1.3 1 2 1      33.346 16.673 0.1862 2.3403
2.6130 1.6 1.8 -3 1 0      34.290 17.145 0.1914 2.4046
2.5623 6.6 7.7 3 0 0      34.989 17.495 0.1951 2.4521
2.5314 4.1 4.8 -1 2 2      35.431 17.715 0.1975 2.4821
2.5314 4.1 4.8 0 -2 2      35.431 17.715 0.1975 2.4821
2.5247 2.4 2.8 -3 1 1      35.529 17.764 0.1980 2.4887
2.4766 16.9 20.3 0 2 2      36.242 18.121 0.2019 2.5371
2.4766 16.9 20.3 1 -2 2      36.242 18.121 0.2019 2.5371
2.4312 0.1 0.1 -1 3 0      36.942 18.471 0.2057 2.5844
2.4312 0.1 0.1 -2 -1 2      36.942 18.471 0.2057 2.5844
2.3808 1.6 2.0 3 -1 1      37.754 18.877 0.2100 2.6391
2.3726 1.1 1.4 0 3 0      37.889 18.944 0.2107 2.6482
2.3564 6.9 8.7 -3 2 0      38.159 19.080 0.2122 2.6664
2.3521 8.9 11.3 2 2 0      38.233 19.117 0.2126 2.6713
2.3457 7.4 9.4 0 0 3      38.341 19.170 0.2132 2.6786
2.3364 6.4 8.2 3 0 1      38.500 19.250 0.2140 2.6893
2.3364 6.4 8.2 -1 -2 2      38.500 19.250 0.2140 2.6893
2.3065 15.4 19.9 -1 3 1      39.019 19.510 0.2168 2.7242
2.3065 15.4 19.9 -1 0 3      39.019 19.510 0.2168 2.7242
2.2856 1.5 2.0 -3 2 1      39.391 19.695 0.2188 2.7491
2.2822 1.5 2.0 -2 -2 1      39.451 19.725 0.2191 2.7531
2.2641 0.2 0.3 0 -3 1      39.780 19.890 0.2208 2.7751
2.2432 0.8 1.1 0 -1 3      40.166 20.083 0.2229 2.8010
2.2286 0.2 0.3 2 1 2      40.442 20.221 0.2244 2.8194
2.2147 3.8 5.1 1 2 2      40.706 20.353 0.2258 2.8370
2.2147 3.8 5.1 2 -2 2      40.706 20.353 0.2258 2.8370
2.1867 12.3 16.8 3 -2 1      41.251 20.625 0.2287 2.8734
2.1867 12.3 16.8 1 0 3      41.251 20.625 0.2287 2.8734
2.1826 15.6 21.3 -2 3 1      41.331 20.666 0.2291 2.8787
2.1826 15.6 21.3 2 2 1      41.331 20.666 0.2291 2.8787
2.1733 5.3 7.3 -3 0 2      41.516 20.758 0.2301 2.8910
2.1427 0.1 0.1 1 -1 3      42.137 21.069 0.2333 2.9323
2.1382 0.2 0.3 2 -3 1      42.230 21.115 0.2338 2.9385
2.1313 0.1 0.1 1 3 0      42.374 21.187 0.2346 2.9481
2.0940 1.1 1.6 -2 0 3      43.167 21.583 0.2388 3.0006
2.0877 1.5 2.1 3 1 1      43.303 21.651 0.2395 3.0096
2.0695 0.7 1.0 -1 -3 1      43.704 21.852 0.2416 3.0361
2.0695 0.7 1.0 -2 1 3      43.704 21.852 0.2416 3.0361
2.0397 0.5 0.7 1 1 3      44.376 22.188 0.2451 3.0805
2.0279 4.9 7.2 -3 2 2      44.647 22.323 0.2466 3.0983
2.0279 4.9 7.2 -2 -2 2      44.647 22.323 0.2466 3.0983
2.0135 0.4 0.6 3 -1 2      44.984 22.492 0.2483 3.1205
2.0135 0.4 0.6 1 3 1      44.984 22.492 0.2483 3.1205
2.0075 0.3 0.4 -1 3 2      45.126 22.563 0.2491 3.1298
1.9824 4.0 6.0 3 0 2      45.730 22.865 0.2522 3.1695
1.9788 2.3 3.5 -1 2 3      45.817 22.908 0.2527 3.1752
1.9533 0.4 0.6 -2 -1 3      46.451 23.226 0.2560 3.2168
1.9466 0.8 1.2 0 3 2      46.621 23.311 0.2569 3.2279
1.9466 0.8 1.2 -4 1 1      46.621 23.311 0.2569 3.2279
1.9409 2.4 3.7 0 2 3      46.764 23.382 0.2576 3.2372
1.9409 2.4 3.7 -3 3 1      46.764 23.382 0.2576 3.2372
1.9217 3.8 5.9 4 0 0      47.259 23.630 0.2602 3.2695
1.9217 3.8 5.9 2 0 3      47.259 23.630 0.2602 3.2695
1.9010 0.4 0.6 -4 0 1      47.808 23.904 0.2630 3.3052
1.8947 1.4 2.2 3 -2 2      47.976 23.988 0.2639 3.3162
1.8947 1.4 2.2 -1 -2 3      47.976 23.988 0.2639 3.3162
1.8917 1.5 2.4 2 2 2      48.058 24.029 0.2643 3.3215
1.8848 3.4 5.4 3 -3 1      48.244 24.122 0.2653 3.3336
1.8848 3.4 5.4 -4 2 0      48.244 24.122 0.2653 3.3336
1.8817 3.8 6.0 3 2 0      48.330 24.165 0.2657 3.3392
1.8776 2.4 3.8 2 -3 2      48.442 24.221 0.2663 3.3465
1.8566 4.8 7.7 -3 -2 1      49.024 24.512 0.2693 3.3842
1.8566 4.8 7.7 4 -1 1      49.024 24.512 0.2693 3.3842
1.8300 20.9 34.0 -1 4 0      49.785 24.893 0.2732 3.4334
1.8300 20.9 34.0 -3 1 3      49.785 24.893 0.2732 3.4334
1.8101 2.0 3.3 4 0 1      50.371 25.186 0.2762 3.4712
1.8053 2.5 4.1 -2 -3 1      50.513 25.256 0.2770 3.4803
1.7957 4.8 8.0 1 2 3      50.804 25.402 0.2784 3.4991
1.7957 4.8 8.0 2 -2 3      50.804 25.402 0.2784 3.4991
1.7843 1.1 1.8 4 -2 1      51.151 25.576 0.2802 3.5214
1.7843 1.1 1.8 1 3 2      51.151 25.576 0.2802 3.5214
1.7813 1.3 2.2 3 2 1      51.243 25.621 0.2807 3.5273
1.7813 1.3 2.2 0 4 0      51.243 25.621 0.2807 3.5273
1.7730 2.0 3.4 1 -4 1      51.499 25.750 0.2820 3.5437
1.7730 2.0 3.4 -3 3 2      51.499 25.750 0.2820 3.5437
1.7593 8.3 14.1 0 0 4      51.932 25.966 0.2842 3.5715
1.7593 8.3 14.1 -4 0 2      51.932 25.966 0.2842 3.5715
1.7551 5.1 8.7 4 1 0      52.064 26.032 0.2849 3.5799
1.7520 3.6 6.1 -1 0 4      52.163 26.081 0.2854 3.5862
1.7270 11.7 20.2 -2 -2 3      52.977 26.488 0.2895 3.6382
1.7270 11.7 20.2 -3 2 3      52.977 26.488 0.2895 3.6382
1.7215 10.6 18.4 -4 2 2      53.161 26.580 0.2904 3.6499
1.7158 5.1 8.9 0 -1 4      53.349 26.675 0.2914 3.6619
1.7158 5.1 8.9 0 4 1      53.349 26.675 0.2914 3.6619
1.6988 1.5 2.6 0 1 4      53.927 26.964 0.2943 3.6986
1.6988 1.5 2.6 -4 3 0      53.927 26.964 0.2943 3.6986
1.6945 1.0 1.8 -1 3 3      54.077 27.038 0.2951 3.7081
1.6894 0.3 0.5 -1 -1 4      54.251 27.125 0.2960 3.7191
1.6894 0.3 0.5 3 -3 2      54.251 27.125 0.2960 3.7191
1.6828 0.8 1.4 1 -3 3      54.483 27.242 0.2971 3.7338
1.6789 1.2 2.1 -4 3 1      54.619 27.309 0.2978 3.7424
1.6789 1.2 2.1 1 0 4      54.619 27.309 0.2978 3.7424
1.6724 1.1 2.0 -2 -3 2      54.848 27.424 0.2990 3.7569
1.6724 1.1 2.0 3 -1 3      54.848 27.424 0.2990 3.7569
1.6667 0.6 1.1 4 1 1      55.053 27.527 0.3000 3.7699
1.6625 1.5 2.7 1 -1 4      55.204 27.602 0.3008 3.7794
1.6625 1.5 2.7 -2 0 4      55.204 27.602 0.3008 3.7794
1.6579 0.9 1.6 4 -1 2      55.372 27.686 0.3016 3.7899
1.6527 0.5 0.9 3 0 3      55.559 27.780 0.3025 3.8018
1.6527 0.5 0.9 -3 4 0      55.559 27.780 0.3025 3.8018
1.6493 0.7 1.3 0 3 3      55.685 27.843 0.3032 3.8097
1.6328 0.4 0.7 -4 -1 2      56.295 28.147 0.3062 3.8480
1.6240 2.6 4.8 1 -4 2      56.629 28.314 0.3079 3.8689
1.6240 2.6 4.8 -1 4 2      56.629 28.314 0.3079 3.8689
1.6160 0.6 1.1 -1 -3 3      56.936 28.468 0.3094 3.8882
1.6073 5.0 9.3 4 -2 2      57.272 28.636 0.3111 3.9092
1.6031 9.9 18.4 0 -4 2      57.437 28.718 0.3119 3.9195
1.6031 9.9 18.4 -2 4 2      57.437 28.718 0.3119 3.9195
1.5903 0.3 0.6 -1 2 4      57.942 28.971 0.3144 3.9510
1.5903 0.3 0.6 -2 -1 4      57.942 28.971 0.3144 3.9510
1.5870 0.3 0.6 2 3 2      58.072 29.036 0.3151 3.9591
1.5754 1.4 2.6 -5 1 1      58.544 29.272 0.3174 3.9884
1.5754 1.4 2.6 2 -4 2      58.544 29.272 0.3174 3.9884
1.5735 1.5 2.8 -4 3 2      58.621 29.311 0.3178 3.9932
1.5735 1.5 2.8 0 4 2      58.621 29.311 0.3178 3.9932
1.5680 1.0 1.9 3 3 0      58.844 29.422 0.3189 4.0070
1.5640 1.5 2.9 0 2 4      59.011 29.505 0.3197 4.0174
1.5640 1.5 2.9 1 -2 4      59.011 29.505 0.3197 4.0174
1.5596 0.7 1.3 -3 3 3      59.194 29.597 0.3206 4.0287
1.5534 1.9 3.6 -2 2 4      59.456 29.728 0.3219 4.0449
1.5534 1.9 3.6 -1 -2 4      59.456 29.728 0.3219 4.0449
1.5490 1.5 2.9 -5 2 0      59.638 29.819 0.3228 4.0562
1.5468 0.9 1.7 2 -1 4      59.733 29.867 0.3232 4.0621
1.5468 0.9 1.7 4 2 0      59.733 29.867 0.3232 4.0621
1.5413 1.7 3.3 -5 2 1      59.970 29.985 0.3244 4.0767
1.5413 1.7 3.3 1 3 3      59.970 29.985 0.3244 4.0767
1.5374 3.3 6.4 5 0 0      60.136 30.068 0.3252 4.0869
1.5321 2.1 4.1 -5 0 1      60.364 30.182 0.3263 4.1009
1.5321 2.1 4.1 -4 2 3      60.364 30.182 0.3263 4.1009
1.5203 2.9 5.7 -1 -4 2      60.884 30.442 0.3289 4.1329
1.5203 2.9 5.7 -3 0 4      60.884 30.442 0.3289 4.1329
1.5070 0.2 0.4 3 3 1      61.480 30.740 0.3318 4.1694
1.4905 1.1 2.2 -4 4 0      62.234 31.117 0.3355 4.2154
1.4905 1.1 2.2 4 -3 2      62.234 31.117 0.3355 4.2154
1.4879 1.4 2.8 2 4 0      62.358 31.179 0.3361 4.2230
1.4837 1.2 2.4 4 2 1      62.550 31.275 0.3370 4.2347
1.4796 4.8 9.7 2 -2 4      62.745 31.372 0.3379 4.2465
1.4783 4.8 9.7 1 2 4      62.809 31.404 0.3382 4.2504
1.4765 3.0 6.1 3 -3 3      62.894 31.447 0.3386 4.2556
1.4735 3.2 6.5 3 -4 2      63.034 31.517 0.3393 4.2641
1.4735 3.2 6.5 -3 -3 2      63.034 31.517 0.3393 4.2641
1.4656 1.7 3.5 -5 2 2      63.415 31.708 0.3412 4.2872
1.4640 1.9 3.9 -4 -2 2      63.491 31.745 0.3415 4.2918
1.4614 5.6 11.4 -5 0 2      63.618 31.809 0.3421 4.2995
1.4614 5.6 11.4 -2 -2 4      63.618 31.809 0.3421 4.2995
1.4497 0.2 0.4 -2 5 0      64.193 32.097 0.3449 4.3342
1.4465 0.3 0.6 -5 3 1      64.351 32.175 0.3457 4.3437
1.4465 0.3 0.6 4 -1 3      64.351 32.175 0.3457 4.3437
1.4433 0.8 1.7 -1 4 3      64.509 32.254 0.3464 4.3532
1.4433 0.8 1.7 1 -4 3      64.509 32.254 0.3464 4.3532
1.4393 0.5 1.0 2 4 1      64.711 32.356 0.3474 4.3654
1.4337 3.0 6.2 0 -4 3      64.998 32.499 0.3488 4.3826
1.4337 3.0 6.2 -2 4 3      64.998 32.499 0.3488 4.3826
1.4303 2.5 5.2 0 -3 4      65.171 32.585 0.3496 4.3930
1.4303 2.5 5.2 -1 3 4      65.171 32.585 0.3496 4.3930
1.4238 0.4 0.8 -2 5 1      65.506 32.753 0.3512 4.4131
1.4238 0.4 0.8 -4 3 3      65.506 32.753 0.3512 4.4131
1.4210 0.6 1.3 4 0 3      65.651 32.826 0.3519 4.4218
1.4210 0.6 1.3 1 -3 4      65.651 32.826 0.3519 4.4218
1.4162 0.3 0.6 2 -5 1      65.898 32.949 0.3530 4.4365
1.4145 0.3 0.6 4 -2 3      65.987 32.994 0.3535 4.4419
1.4145 0.3 0.6 -2 3 4      65.987 32.994 0.3535 4.4419
1.4118 0.2 0.4 3 2 3      66.134 33.067 0.3542 4.4506

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