24小时热门版块排行榜    

查看: 1400  |  回复: 12

icyiceberg

铜虫 (正式写手)

[求助] 请教A、B类错误怎么解决????

请教下面的A、B类错误怎么解决????
DENSX01_ALERT_1_A The ratio of the calculated to measured crystal density
lies outside the range 0.80 <> 1.20
Calculated density = 1.362
Measured density = 0.000

PLAT093_ALERT_1_B No su’s on H-atoms, but refinement reported as . mixed
Alert level C
ABSTY03_ALERT_1_C The _exptl_absorpt_correction_type has been given as none.
However values have been given for Tmin and Tmax. Remove
these if an absorption correction has not been applied.
From the
回复此楼

» 猜你喜欢

» 本主题相关价值贴推荐,对您同样有帮助:

已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖
回帖置顶 ( 共有1个 )

lijunjie84

版主 (职业作家)

隐者

优秀版主


drg1984: 回帖置顶 2011-12-25 18:22:34
drg1984(金币+1): 欢迎来发帖交流问题! 2011-12-25 18:22:37
引用回帖:
3楼: Originally posted by icyiceberg at 2011-12-25 15:32:57:
第一个怎么改成一样的??

在cif 里将_exptl_crystal_density_meas 0
改为:_exptl_crystal_density_meas ?
5楼2011-12-25 15:37:01
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖
普通回帖

lijunjie84

版主 (职业作家)

隐者

优秀版主

【答案】应助回帖


感谢参与,应助指数 +1
icyiceberg(金币+10): ★★★很有帮助 2011-12-25 15:32:24
drg1984(金币+1): 欢迎来发帖交流问题! 2011-12-25 18:22:19
第一个改成一样的就行,第二个你在cif中把mixed 改成none就好了!
2楼2011-12-25 14:42:09
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

icyiceberg

铜虫 (正式写手)

引用回帖:
: Originally posted by lijunjie84 at 2011-12-25 14:42:09:
第一个改成一样的就行,第二个你在cif中把mixed 改成none就好了!

第一个怎么改成一样的??
3楼2011-12-25 15:32:57
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

icyiceberg

铜虫 (正式写手)

引用回帖:
: Originally posted by lijunjie84 at 2011-12-25 14:42:09:
第一个改成一样的就行,第二个你在cif中把mixed 改成none就好了!

_exptl_crystal_density_meas       0
_exptl_crystal_density_diffrn     1.362

是把上面的那两行改成
_exptl_crystal_density_meas       0.8
_exptl_crystal_density_diffrn     1.2

这样吗??
4楼2011-12-25 15:35:44
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

icyiceberg

铜虫 (正式写手)

引用回帖:
2楼: Originally posted by lijunjie84 at 2011-12-25 14:42:09:
第一个改成一样的就行,第二个你在cif中把mixed 改成none就好了!

还是把cif里最后的的
_refine_diff_density_max    0.168
_refine_diff_density_min   -0.281
_refine_diff_density_rms    0.041
改掉??
我是新手,请多指教
6楼2011-12-25 15:41:20
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

icyiceberg

铜虫 (正式写手)

引用回帖:
5楼: Originally posted by lijunjie84 at 2011-12-25 15:37:01:
在cif 里将_exptl_crystal_density_meas 0
改为:_exptl_crystal_density_meas ?

还是存在问题啊
Alert level A
DENSD01_ALERT_1_A The ratio of the submitted crystal density and that
calculated from the formula is outside the range 0.90 <> 1.10
Crystal density given = 1.200
Calculated crystal density = 1.362
DENSX01_ALERT_1_A The ratio of the calculated to measured crystal density
lies outside the range 0.80 <> 1.20
Calculated density = 1.200
Measured density = 0.800
PLAT044_ALERT_1_A Calculated and Reported Dx Differ .............. ?
PLAT046_ALERT_1_A Reported Z, MW and D(calc) are Inconsistent .... 1.362
7楼2011-12-25 15:44:14
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

lijunjie84

版主 (职业作家)

隐者

优秀版主


drg1984(金币+1): 欢迎来发帖交流问题! 2011-12-25 18:22:52
引用回帖:
7楼: Originally posted by icyiceberg at 2011-12-25 15:44:14:
还是存在问题啊
Alert level A
DENSD01_ALERT_1_A The ratio of the submitted crystal density and that
calculated from the formula is outside the range 0.90 <> 1.10
Crystal density given = 1 ...

改成?号!
8楼2011-12-25 15:48:45
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

lijunjie84

版主 (职业作家)

隐者

优秀版主


lichun1210(金币+1): 感谢交流~ 2011-12-26 00:03:54
引用回帖:
8楼: Originally posted by lijunjie84 at 2011-12-25 15:48:45:
改成?号!

或者你都写成1试一试!0.8-1.2是范围!
9楼2011-12-25 15:50:05
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

lijunjie84

版主 (职业作家)

隐者

优秀版主

引用回帖:
7楼: Originally posted by icyiceberg at 2011-12-25 15:44:14:
还是存在问题啊
Alert level A
DENSD01_ALERT_1_A The ratio of the submitted crystal density and that
calculated from the formula is outside the range 0.90 <> 1.10
Crystal density given = 1 ...

论坛很多帖子,我发了个涉及到很多AB类错误的PDF!自己下下来看看!
10楼2011-12-25 15:51:18
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖
相关版块跳转 我要订阅楼主 icyiceberg 的主题更新
最具人气热帖推荐 [查看全部] 作者 回/看 最后发表
[考研] 0857调剂 +3 一ll半 2026-02-28 3/150 2026-03-01 18:32 by 热情沙漠
[考研] 材料学调剂 +9 提神豆沙包 2026-02-28 11/550 2026-03-01 18:15 by ms629
[考博] 26申博 +4 想申博! 2026-02-26 6/300 2026-03-01 17:32 by 想申博!
[考研] 化工专硕348,一志愿985求调剂 +5 弗格个 2026-02-28 8/400 2026-03-01 17:25 by sunny81
[考研] 0856求调剂285 +8 吕仔龙 2026-02-28 8/400 2026-03-01 17:25 by 刘兵
[考研] 0856材料求调剂 +4 麻辣鱿鱼 2026-02-28 4/200 2026-03-01 16:51 by caszguilin
[考研] 材料学硕318求调剂 +8 February_Feb 2026-03-01 10/500 2026-03-01 16:48 by sunny81
[考研] 285求调剂 +8 满头大汗的学生 2026-02-28 8/400 2026-03-01 16:47 by caszguilin
[基金申请] 刚录用,没有期刊号,但是在线可看的论文可以放为代表作吗 10+3 arang1 2026-03-01 3/150 2026-03-01 16:43 by babero
[考研] 材料化工调剂 +9 今夏不夏 2026-03-01 10/500 2026-03-01 16:01 by hmn_wj
[考研] 295求调剂 +6 19171856320 2026-02-28 6/300 2026-03-01 15:52 by jxstnuZYX
[考研] 0856调剂 +4 刘梦微 2026-02-28 4/200 2026-03-01 15:35 by 吸一口猫气
[考研] 材料工程274求调剂 +3 Lilithan 2026-03-01 3/150 2026-03-01 14:58 by ms629
[考研] 一志愿中南大学理学化学 +3 15779376950 2026-03-01 4/200 2026-03-01 14:27 by 15779376950
[论文投稿] 求助coordination chemistry reviews 的写作模板 10+3 ljplijiapeng 2026-02-27 4/200 2026-03-01 09:07 by babero
[考研] 304求调剂 +3 52hz~~ 2026-02-28 5/250 2026-03-01 00:00 by 52hz~~
[考研] 292求调剂 +3 yhk_819 2026-02-28 3/150 2026-02-28 21:57 by gaoxiaoniuma
[考研] 264求调剂 +3 巴拉巴拉根556 2026-02-28 3/150 2026-02-28 21:31 by gaoxiaoniuma
[考研] 085600材料工程一志愿中科大总分312求调剂 +8 吃宵夜1 2026-02-28 10/500 2026-02-28 20:27 by L135790
[考研] 276求调剂 +3 路lyh123 2026-02-28 4/200 2026-02-28 19:45 by 路lyh123
信息提示
请填处理意见