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huangchangliang

金虫 (小有名气)

[求助] 求助:Au/CeO2制备中出现的问题

使用沉淀法制备Au/CeO2,沉淀剂是(NH4)2CO3, PH值调控在8-9,但是在400度煅烧之后的Au/CeO2催化剂颜色显绿色,方法是按照文献的方法做的。不知道是什么原因,而用NaBH4制备的Au/CeO2是显紫色的。请问什么原因啊,求助。
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huangchangliang

金虫 (小有名气)

方法如下:CeO2 powder (3 g) was slurried in DI water (150 mL) whilst
stirring and aqueous (NH4)2CO3 solution (75 mL; 1m) was then
added. HAuCl4•3H2O (99.99%, Alfa; 0.174 mmol) was dissolved in
DI water (75 mL) and added to the above solution dropwise. The
pH value was kept at 8–9 during the whole process. The resulting
precipitate was aged at room temperature for 1 h, then filtered and
washed three times with DI water at 60–70C. The product was dried
in vacuo at 70–80C overnight and then calcined in air at 400C for
4 h.不知道你使用沉淀法制备的Au /CeO2是什么颜色。
3楼2011-10-19 11:06:20
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mgyawm

银虫 (正式写手)

【答案】应助回帖

能不能把具体点的方法发出来,这样有点笼统
2楼2011-10-19 08:51:08
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