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Firstly, the data quality appears to be very good indeed: I/sigma is 24, Rint is 2.4 % -- and yet, the resulting structure has an Rfactor of 7.3%, which is not too high by any means, but is still higher than one could expect. The modelled disorder is curious, and this model reports the use of 1078 restraints. There is no detail about these restraints, and still: the geometry of some of the phenyl rings is somewhat distorted. ×îºóÒ»¾ä²»Ì«Ã÷°×£¬ÊÇÒªÔõô»Ø´ðÕâЩÏÞÖÆµÄϸ½Ú£¬ÇëÖ¸½Ì |
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