Znn3bq.jpeg
²é¿´: 1105  |  »Ø¸´: 11
µ±Ç°Ö÷ÌâÒѾ­´æµµ¡£
µ±Ç°Ö»ÏÔʾÂú×ãÖ¸¶¨Ìõ¼þµÄ»ØÌû£¬µã»÷ÕâÀï²é¿´±¾»°ÌâµÄËùÓлØÌû

gaofenzi895

гæ (СÓÐÃûÆø)

[½»Á÷] CIFÉó¸åÒâ¼ûÇóÖú?

ͶÁËһƪSCIÎÄÕÂ,ÆäÖÐ ¹ØÓÚCIF²¿·ÖÓÐÈçÏÂÉó¸åÒâ¼û:
In particular, the Friedel pairs should be merged and the refinement repeated thereafter. The short H-H contacts are probably due to some sort of tert-butyl disorder which unfortuantely has not been sddressed in the Exp.Part. Is it reasonable to include such hydrogen with split occupancies in the refinement? Probably also the necessity for restraints orininates from the disorder? Please explain.

ÕâʲôÒâ˼°¡?ÎÊÌâ´óô?Ôõô¸Ä°¡?лл.
»Ø¸´´ËÂ¥
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

xi2004

ÖÁ×ðľ³æ (Ö°Òµ×÷¼Ò)

¸ÃÔÓÖ¾ÓÐûÓÐÒªÇóÏûÃðAlert C°¡?
ûÓеϰ,
¼Ómerg 4
CIFÖмӶÔÎÞÐò, restrainµÈµÄ˵Ã÷,
ÔÙɾ³ýһЩÎÞÐòÔì³ÉµÄ²»ºÏÀí¼ü,
Ó¦¸ÃÄÜͨ¹ýÁË.
xi2004-emuch@163.com
9Â¥2008-09-21 00:38:12
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
²é¿´È«²¿ 12 ¸ö»Ø´ð

xi2004

ÖÁ×ðľ³æ (Ö°Òµ×÷¼Ò)

ÓÖ¼ûÎÞÐò, Í·´ó.

ÄãµÄ tert-butyl ÊDz»ÊÇÎÞÐò? ÇâÔõô¼ÓµÄ. ÏÈ×Ô¼ºÓÃCIFcheck checkÒ»ÏÂ, ¿´¿´ÎªºÎH-HÌ«½ü.
»¹ÓжàÓàµÄµãÒªMergedÒ»ÏÂ.

½â¾öÊÇ¿ÉÒÔ½â¾öµÄ, ¹À¼Æ, µ«ÉÔÂé·³.
xi2004-emuch@163.com
2Â¥2008-09-20 17:37:50
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

xi2004

ÖÁ×ðľ³æ (Ö°Òµ×÷¼Ò)

Õ⼸ÌìÍøÂçÂý, ÖØ·¢ÁË, ²»ºÃÒâ˼.
xi2004-emuch@163.com
3Â¥2008-09-20 17:38:08
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

gaofenzi895

гæ (СÓÐÃûÆø)

Âé·³ÎÊÏÂ,
PLAT220_ALERT_2_A Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       5.75 Ratio
--------------------------------------------------------------------------------Alert level B
PLAT230_ALERT_2_B Hirshfeld Test Diff for    C11    --  C12_a   ..      10.61 su   
PLAT230_ALERT_2_B Hirshfeld Test Diff for    C11    --  C13_a   ..      10.62 su   
PLAT230_ALERT_2_B Hirshfeld Test Diff for    C12    --  C11_a   ..      10.59 su   
PLAT230_ALERT_2_B Hirshfeld Test Diff for    C13    --  C11_a   ..      10.62 su   
PLAT024_ALERT_4_B Merging of Friedel Pairs is STRONGLY Indicated .          !
ÕâЩ¶¼Ê²Ã´´íÎó°¡?
4Â¥2008-09-20 18:48:54
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
×î¾ßÈËÆøÈÈÌûÍÆ¼ö [²é¿´È«²¿] ×÷Õß »Ø/¿´ ×îºó·¢±í
[¿¼ÑÐ] 283Çóµ÷¼Á +20 ÄǸöàà×Ó 2026-04-09 20/1000 2026-04-10 09:50 by liuhuiying09
[¿¼ÑÐ] 0854µ÷¼Á +7 950824he@ 2026-04-09 7/350 2026-04-10 09:10 by Delta2012
[¿¼ÑÐ] ²ÄÁÏÓ뻯¹¤300Çóµ÷¼Á +27 Ф¿ªÎÄ 2026-04-09 29/1450 2026-04-10 08:26 by Sammy2
[¿¼ÑÐ] 087100³õÊÔ311Çóµ÷¼Á +3 ÈÎÑÅÇÙ 2026-04-09 3/150 2026-04-09 22:42 by lbsjt
[¿¼ÑÐ] ±¾¿Æ211 ¹¤¿Æ085400 280·ÖÇóµ÷¼Á ¿É¿çרҵ +3 LZH£¨µÈ´ýµ÷¼ÁÖÐ 2026-04-09 3/150 2026-04-09 21:29 by wutongshun
[¿¼ÑÐ] 284Çóµ÷¼Á +7 ÈÃÎÒÉϰ¶°É°¢Î÷ 2026-04-09 7/350 2026-04-09 18:59 by haironglove
[¿¼ÑÐ] 085501»úеר˶ 302·Ö ²»ÌôרҵÇóµ÷¼Á +5 Íôij. 2026-04-09 5/250 2026-04-09 15:38 by ½¯ð©Óí
[¿¼ÑÐ] 368»¯Ñ§Çóµ÷¼Á +13 wwwwabcde 2026-04-07 14/700 2026-04-09 14:47 by heaven_jay
[¿¼ÑÐ] ¶þ´Îµ÷¼ÁÇóÀÏʦÊÕÁô +3 ЦЦԬ 2026-04-08 3/150 2026-04-08 23:50 by ×íÔÚ·çÀï
[¿¼ÑÐ] ÉúÎïѧ328·ÖÇóµ÷¼Á +9 ÉÁµçkkl 2026-04-08 10/500 2026-04-08 21:42 by liuhuiying09
[¿¼ÑÐ] 0703µ÷¼Á£¬Ò»Ö¾Ô¸Ìì½ò´óѧ319·Ö +23 haaaabcd 2026-04-05 26/1300 2026-04-08 16:19 by luoyongfeng
[¿¼ÑÐ] Çóµ÷¼Á +9 ÔÂ@163.com 2026-04-07 11/550 2026-04-08 14:48 by qlm5820
[¿¼ÑÐ] 285Çóµ÷¼Á +7 ¶ñ·¨´ó¶þµÄÆøÎ¶ß 2026-04-05 10/500 2026-04-08 14:34 by zhq0425
[¿¼ÑÐ] 259Çóµ÷¼Á +5 ¾Í°®³ÔÍÁ¶¹Ñ½Ñ½ 2026-04-07 5/250 2026-04-07 22:40 by JourneyLucky
[¿¼ÑÐ] ¿¼Ñе÷¼Á +3 WwwwwwwÍÛ 2026-04-06 3/150 2026-04-06 20:55 by lbsjt
[¿¼ÑÐ] Ò»Ö¾Ô¸ºÓ±±¹¤Òµ´óѧ²ÄÁϹ¤³Ì£¬³õÊÔ344Çóר˶µ÷¼Á +6 15933906766 2026-04-05 6/300 2026-04-06 13:21 by Î޼ʵIJÝÔ­
[¿¼ÑÐ] 0855Çóµ÷¼Á²ÄÁÏ +11 ºìÌÒׯׯ 2026-04-04 12/600 2026-04-06 10:26 by À¶ÔÆË¼Óê
[¿¼ÑÐ] Ò»Ö¾Ô¸¹þ¶û±õ¹¤Òµ´óѧ085600Ó¢Ò»Êý¶þ337·ÖÇóµ÷¼Á +12 lyz0427 2026-04-03 12/600 2026-04-06 06:37 by houyaoxu
[¿¼ÑÐ] 272Çóµ÷¼Á +4 µçÆøÀî 2026-04-05 4/200 2026-04-05 10:41 by lbsjt
[¿¼ÑÐ] 085602µ÷¼Á ³õÊÔ×Ü·Ö335 +12 19123253302 2026-04-04 12/600 2026-04-05 08:08 by 544594351
ÐÅÏ¢Ìáʾ
ÇëÌî´¦ÀíÒâ¼û