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summiler_XU

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[求助] 投稿Talanta,审稿人意见如下,感觉遇到了统计学专家,求大神帮忙梳理一下,非常感谢 已有2人参与

Reviewer #3:
The ms is well written and organized. Especially Introduction and Experimental sections. The synthesis of the composite is well described and documented, though elemental analysis of the magnetic core (Fe3O4) was not provided. I am not convinced that it does not contain some residual water.
In analytical part, it would far much better if authors could perform statistical analysis of the designed extraction experiment so that the optimal experimental conditions could by uniquely determined. Was it possible to compare obtained extraction yields with a standard method which produces known yields?
Validation procedure should be performed more comprehensively. Linear parameters should be given with proper statistical ANOVA analysis and regression coefficients must be given with appropriate errors. LOD should be determined from the regression data and for S/N method data should be provided together with the significance test.
A chromatogram of the synthetic mixture should be given together with the chromatogram of the extracted material from the real sample.
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学术巨星

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哦 貌似你的实验是铁氧体萃取 然后色谱检测吧

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4楼2015-11-22 14:39:15
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雨梦无声

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2楼2015-11-22 13:49:31
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summiler_XU

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引用回帖:
2楼: Originally posted by 雨梦无声 at 2015-11-22 13:49:31
看起来不难回答

回答起来也觉得并不简单呢
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3楼2015-11-22 14:07:52
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【答案】应助回帖

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感谢参与,应助指数 +1
summiler_XU: 金币+20, ★★★很有帮助 2015-11-22 18:42:35
1. 补充Fe3O4元素分析结果,确定是否含有结晶水
2. 运用化学计量学对萃取实验进行析因设计试验
3. 与现有的已知萃取率的方法进行对比,考察所建方法的萃取率
4. 补充方法确认参数,线性、回归系数、回归结果的误差、检出限、信噪比等
5. 补充合成的混合液(估计是模拟样品)的色谱图
5楼2015-11-22 14:58:44
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