[求助] 有做五氯酚还原脱氯的虫友么，交流一下

10楼: Originally posted by xuyh_326 at 2015-05-20 14:07:32
Quantitative analysis of the dehalogenated products was
performed using a Waters HPLC system with a symmetry
column (250 mm length  4.6 mm i.d., 5 mm particle size) and
a Waters 2996 Photodiode  ...

2楼: Originally posted by xuyh_326 at 2015-05-12 09:17:14
这个我做过，有什么具体问题尽管问！

3楼: Originally posted by pesistence at 2015-05-12 10:46:24
五氯酚水溶性很差，就加了些氢氧化钠，电解质加的是硫酸钠。在脱氯过程中发现阴极的电解池中有固体析出，查资料说PH小于6.6，五氯酚就析出了。所以想知道您之前做的时候用的电解质，阴极电解池的PH情况，五氯酚中加 ...