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The esds on the unit cell lengths are higher than one might expect (by a factor of 10) from data collected on a modern diffractometer. This begs the question: why? The answer to this question must also be added to the manuscript text. My concern here is that perhaps the diffraction peak positions may be subject to twinning which hasnt been resolved. ¾§ÌåÖÊÁ¿ºÜ²î£¬Öظ´¶à´Î¶¼²»ºÃ£¬ÉÔÓзֻ¯£¬Í¬Ê±ÓÎÀëµÄ¼×´¼·Ö×ÓÎÞÐò£¬clo4-Ò²ÊÇÎÞÐò£¬ ±¾È˸սӴ¥¾§Ì壬ʵÔÚÊDzËÄñ£¬²»ÖªÔõô»Ø´ðÉÏÃæµÄÎÊÌ⣬ϣÍû¸ßÈËÖ¸µã¡£ÓÃÓ¢ÎĽâ´ð¸üºÃ£¬·Ç³£¸Ðл£¡ |
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