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dyy981

木虫 (著名写手)

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The esds on the unit cell lengths are higher than one might expect (by a factor of 10) from data collected on a modern diffractometer. This begs the question: why? The answer to this question must also be added to the manuscript text. My concern here is that perhaps the diffraction peak positions may be subject to twinning which hasnt been resolved.

晶体质量很差,重复多次都不好,稍有分化,同时游离的甲醇分子无序,clo4-也是无序,  本人刚接触晶体,实在是菜鸟,不知怎么回答上面的问题,希望高人指点。用英文解答更好,非常感谢!
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alusia

金虫 (正式写手)

编辑认为你这个警惕的衍射峰可能有孪晶现象。
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2楼2008-07-02 13:26:31
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