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脑袋空空木虫 (小有名气)
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[求助]
微谱求助，万分感谢~已有1人参与
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最近分到一个东西，含C，H都比较少，自己解谱认为是苯乙酸甲酯，但是外观性质不同，具体未确定，麻烦诸位帮忙搜下先~~~ 质谱，标品尽快搞定，我就纳闷儿了~~~ 13C NMR (126 MHz, MeOD) δ 174.55,134.27,129.23,128.43, 126.92,49.49,41.15 |
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seuseasoar
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2楼2014-09-09 22:08:29
seuseasoar
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3楼2014-09-09 22:11:09
seuseasoar
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【答案】应助回帖
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1 . (S)-3-amino-2-phenylpropionic acid 相似度:85.7% European Journal of Organic Chemistry 2010 6464-6470 Synthesis and Conformational Properties of Nonsymmetric Pillar[5]arenes and Their Acetonitrile Inclusion Compounds Yuhui Kou, Hongqi Tao, Derong Cao, Zhiyong Fu, Dieter Schollmeyer and Herbert Meier Structure 13C NMR 碳谱模拟图 2 . 1,4-dimethylbicyclo[2.2.2]oct-7-ene-2,3,5,6-tetracarboxylic acid bis(phenylimide) C26H22N2O4 相似度:77.7% Heterocycles 2004 64 199-206 Diels-Alder Reaction and Double Phenylation in Reaction of Thiophenes with Diphenyliodonium Triflate Bian-Xiang Zhang, Takato Nuka, Yuzo Fujiwara, Teizo Yamaji, Zhaomin Hou, and Tsugio Kitamura* Structure 13C NMR 碳谱模拟图 3 . phenylacetic acid 相似度:71.4% Journal of Natural Products 2005 68 568-571 Biscopyran, a Phytotoxic Hexasubstituted Pyranopyran Produced by Biscogniauxia mediterranea,a Fungus Pathogen of Cork Oak Antonio Evidente, Anna Andolfi, Lucia Maddau, Antonio Franceschini, and Francesco Marras Structure 13C NMR 碳谱模拟图 4 . Phenylacetic acid C8H8O2 相似度:71.4% Journal of Natural Products 2010 73 553-556 Jacaranone-Derived Glucosidic Esters from Jacaranda glabra and Their Activity against Plasmodium falciparum M. Salomé Gachet, Olaf Kunert, Marcel Kaiser, Reto Brun, Ricardo A. Muñoz, Rudolf Bauer and Wolfgang Schühly Structure 13C NMR 碳谱模拟图 5 . N,N'-甲基-苯基脲 相似度:71.4% Chinese Journal of Marine Drugs 2000 19(5) 1-3 STUDIES ON THE CHEMICAL CONSTITUTIONS OF THE SPONGE SUBERITES TYLOBTUSA LEVI Li Wenlin, Mao Shilong, Yi Yanghua Structure 13C NMR 碳谱模拟图 6 . 苯乙酸 相似度:71.4% Chinese Journal of Marine Drugs 1998 3 31-32 CHEMICAL CONSTITUENTS OF MARINE SPONGE GELLIODES SPINOSELLA IN THE SOUTH CHINA SEA Deng Songzhi, Li Fengying, Peng Shengshi Structure 13C NMR 碳谱模拟图 7 . L-Phenylalanine C9H11NO2 相似度:71.4% Organic Letters 2009 Vol.11,No.16 3714-3717 Brevianamide J, A New Indole Alkaloid Dimer from Fungus Aspergillus versicolor Guo-You Li, Tao Yang, Ying-Gang Luo, Xiao-Zhen Chen, Dong-Mei Fang, and Guo-Lin Zhang Structure 13C NMR 碳谱模拟图 8 . Benzyl isothiocyanate 相似度:71.4% Phytochemistry Letters 2012 5 351-357 Antimicrobial volatile glucosinolate autolysis products from Hornungia petraea (L.) Rchb. (Brassicaceae) Niko S. Radulović, Milan S. Dekić, Zorica Z. Stojanović-Radic Structure 13C NMR 碳谱模拟图 9 . L-phenylalanine 相似度:71.4% China Journal of Chinese Materia Medica 2010 35 2412-2415 Chemical constituents of Gekko swinhonis LI Wen; WANG Guocai; ZHANG Xiaoqi; WANG Ying; YE Wencai; Structure 13C NMR 碳谱模拟图 10 . [18O]Phenylessigs¨aure 相似度:71.4% Zeitschrift für Naturforschung B 2003 58 595-605 Partial Oxygen Migration in the Photochemical Wolff Rearrangement - a-Oxocarben-Oxiren-Isomerization or Intermolecular Mechanism? (In German) P. Haiss and K.-P. Zeller Structure 13C NMR 碳谱模拟图 11 . Methyl 2-phenylacetate 相似度:71.4% Tetrahedron 2012 68 2113-2120 Pd-catalyzed decarboxylative cross-couplings of potassium malonate monoesters with aryl halides Yi-Si Feng, Wei Wu, Zhong-Qiu Xu, Yan Li, Ming Li, Hua-Jian Xu Structure 13C NMR 碳谱模拟图 12 . S-Methyl 2-phenylethanethioate 相似度:71.4% Organic & Biomolecular Chemistry 2010 8 234-246 Identification and biosynthesis of tropone derivatives and sulfur volatiles produced by bacteria of the marine Roseobacter clade Verena Thiel, Thorsten Brinkhoff, Jeroen S. Dickschat, Susanne Wickel, Jörg Grunenberg, Irene Wagner-Döbler, Meinhard Simon and Stefan Schulz Structure 13C NMR 碳谱模拟图 13 . 4-(2-Phenylaziridin-1-yl)-4H-1,2,4-triazole C10H10N4 相似度:71.4% European Journal of Organic Chemistry 2012 1554-1562 Sulfur–Nitrogen and Carbon–Nitrogen Bond Formation by Intermolecular Imination and Amidation without Catalyst Wen Bo Ma, Sheng Nan Li, Zhong Hua Zhou, Heng Shui Shen, Xue Li, Qiu Sun, Ling He and Ying Xue Structure 13C NMR 碳谱模拟图 14 . 1,1-dimethoxy-1-phenyl-2,2-dichloroethane C10H12Cl2O2 相似度:71.4% Russian Journal of Organic Chemistry 2002 38 902-904 Iodosobenzene Dichloride, a Convenient Reagent for Chloro- and Iodomethoxylation of Double and Triple Bonds M. S. Yusubov, R. Ya. Yusubova, V. D. Filimonov and Chi Ki-Whan Structure 13C NMR 碳谱模拟图 15 . bis(1,3,4-oxadiazol-2-yl-phenylmethyl) disulfide C18H14N4O2S2 相似度:71.4% Tetrahedron 2012 68 3616-3625 Reactions of α-mercaptocarboxylic acid hydrazides with triethyl orthoesters: synthesis of 1,3,4-thiadiazin-5(6H)-ones and 1,3,4-oxadiazoles Agnieszka Kudelko Structure 13C NMR 碳谱模拟图 16 . (S)-2-chloro-3-phenylpropanoic acid 相似度:71.4% European Journal of Organic Chemistry 2011 1015-1022 Biocatalyzed Enantioselective Reduction of Activated C=C Bonds: Synthesis of Enantiomerically Enriched -Halo-β-arylpropionic Acids Elisabetta Brenna, Francesco G. Gatti, Alessia Manfredi, Daniela Monti and Fabio Parmeggiani Structure 13C NMR 碳谱模拟图 17 . (S)-2-bromo-3-phenylpropanoic acid 相似度:71.4% European Journal of Organic Chemistry 2011 1015-1022 Biocatalyzed Enantioselective Reduction of Activated C=C Bonds: Synthesis of Enantiomerically Enriched -Halo-β-arylpropionic Acids Elisabetta Brenna, Francesco G. Gatti, Alessia Manfredi, Daniela Monti and Fabio Parmeggiani Structure 13C NMR 碳谱模拟图 |
4楼2014-09-09 22:11:18
脑袋空空
木虫 (小有名气)
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5楼2014-09-10 15:33:51
脑袋空空
木虫 (小有名气)
- 应助: 2 (幼儿园)
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6楼2014-09-26 21:12:37