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1. ÊDz»ÊÇÖ§³Å²ÄÁÏ£¨Supporting Information£©ºÜÖØÒª, ÏÖÔÚµÄͶ¸åºÃÏñ¶¼ÒªÓÐ 2. Éó¸åÈËÒªÇó¡°Transforming from P21/n to P21/c is prefered generally¡± ÊÇÖØÐ¾«ÐÞ, »¹ÊÇÖ±½Ó¸ÄCIF Îļþ¡£½«CIF ÎļþµÄ×åȺ¸ÄΪ P21/cºó£¬AÀà´íÎó¾Í³öÁË. 3. Éó¸åÈË˵¡°_publ_section_exptl_refinement section is not appropiate¡±, Õâ¸öÒ»°ãÓ¦¸ÃÔõôд.ÎÒµÄÖ±½ÓÓõľ§ÌåÊý¾ÝÀïµÄCIFÎļþÀïµÄ_refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. 4. _refine_ls_abs_structure_Flack ´ÓÄĸöÎļþ¿ÉÒÔÕÒµ½??? [ Last edited by zhchem on 2008-4-11 at 10:46 ] |
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zhchem
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