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title: Thermodynamic properties and solid−liquid phase equilibrium of bisphenolA-bis (5,5-dimethyl-1,3-dioxaphosphorinanyl-2-oxyphosphate ester) in selected solvents source: Journal of Chemical and Pharmaceutical Research, 2014, 6(2):47-59 лл |
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baiyuefei
版主 (文学泰斗)
风雪
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【答案】应助回帖
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感谢参与，应助指数 +1
rosarain(oven1986代发): 金币+10, 代扣结帖。 2014-06-13 10:39:25
oven1986: 检索EPI+1, 感谢应助！ 2014-06-13 10:39:32
感谢参与，应助指数 +1
rosarain(oven1986代发): 金币+10, 代扣结帖。 2014-06-13 10:39:25
oven1986: 检索EPI+1, 感谢应助！ 2014-06-13 10:39:32
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Accession number: 20141117465484 Title: Thermodynamic properties and solid-liquid phase equilibrium of bisphenol A-bis (5, 5-dimethyl-1,3-dioxaphosphorinanyl-2-oxyphosphate ester) in selected solvents Authors: Jiang, Lin-Kun1, 2; Wang, Li-Sheng1 Author affiliation: 1School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing, China 2Wuhai College, Inner Mongol University of Technology, Wuhai, China Corresponding author: Wang, L.-S. Source title: Journal of Chemical and Pharmaceutical Research Abbreviated source title: J. Chem. Pharm. Res. Volume: 6 Issue: 2 Issue date: 2014 Publication year: 2014 Pages: 47-59 Language: English E-ISSN: 09757384 Document type: Journal article (JA) Publisher: Journal of Chemical and Pharmaceutical Research Abstract: In this work, we investigated the thermodynamic properties of flame retardant bisphenol A-bis (5,5-dimethyl-1, 3-dioxaphosphorinanyl-2-oxy phosphate ester) (BADOPE), including the melting point and the enthalpy of fusion of BADOPE by differential scanning calorimeter (DSC) and the thermal stability of BADOPE by thermogravimetric analysis (TGA). BADOPE was synthesized and characterized by EA, FT-IR and 1HNMR. Using a static analytic method, solid-liquid phase equilibrium data (the solubility) of BADOPE in acetonitrile, acetone, methanol, tetrahydrofuran, ethanol, ethyl acetate, methylethylketone and 1,4-dioxane were obtained at temperatures ranging from 293 to 338 K. Several thermodynamic models, including the ideal, modified Apelblat, Wilson, NRTL, UNIQUAC and Scatchard-Hildebrand models, were applied to correlate the experimental solubility data. Number of references: 28 Main heading: Phase equilibria Controlled terms: Acetone - Differential scanning calorimetry - Esterification - Esters - Flame retardants - Oils and fats - Solubility - Synthesis (chemical) - Thermodynamic properties - Thermogravimetric analysis Uncontrolled terms: Differential scanning calorimeters - Enthalpy of fusion - Experimental solubility datum - Phosphate esters - Phosphorus-containing - Solid-liquid phase equilibria - Tetra-hydrofuran - Thermodynamic model Classification code: 641.1 Thermodynamics - 801 Chemistry - 801.4 Physical Chemistry - 802.2 Chemical Reactions - 803 Chemical Agents and Basic Industrial Chemicals - 804.1 Organic Compounds Database: Compendex Compilation and indexing terms, © 2013 Elsevier Inc. |
2楼2014-06-12 16:22:30
baiyuefei
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- 注册: 2008-12-18
- 性别: GG
- 专业: 合成药物化学
- 管辖: 有机交流
3楼2014-06-12 16:22:44
4楼2014-06-12 16:28:42