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rosarain

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[求助] 求一篇文章的EI文献检索号，多谢

title: Thermodynamic properties and solid−liquid phase equilibrium of bisphenolA-bis (5,5-dimethyl-1,3-dioxaphosphorinanyl-2-oxyphosphate ester) in selected solvents

source: Journal of Chemical and Pharmaceutical Research, 2014, 6(2):47-59 лл

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感谢参与，应助指数 +1
rosarain(oven1986代发): 金币+10, 代扣结帖。 2014-06-13 10:39:25
oven1986: 检索EPI+1, 感谢应助！ 2014-06-13 10:39:32

Accession number:

20141117465484

Title:

Thermodynamic properties and solid-liquid phase equilibrium of bisphenol A-bis (5, 5-dimethyl-1,3-dioxaphosphorinanyl-2-oxyphosphate ester) in selected solvents

Authors:

Jiang, Lin-Kun1, 2; Wang, Li-Sheng1

Author affiliation:

1School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing, China

2Wuhai College, Inner Mongol University of Technology, Wuhai, China

Corresponding author:

Wang, L.-S.

Source title:

Journal of Chemical and Pharmaceutical Research

Abbreviated source title:

J. Chem. Pharm. Res.

Volume:

6

Issue:

2

Issue date:

2014

Publication year:

2014

Pages:

47-59

Language:

English

E-ISSN:

09757384

Document type:

Journal article (JA)

Publisher:

Journal of Chemical and Pharmaceutical Research

Abstract:

In this work, we investigated the thermodynamic properties of flame retardant bisphenol A-bis (5,5-dimethyl-1, 3-dioxaphosphorinanyl-2-oxy phosphate ester) (BADOPE), including the melting point and the enthalpy of fusion of BADOPE by differential scanning calorimeter (DSC) and the thermal stability of BADOPE by thermogravimetric analysis (TGA). BADOPE was synthesized and characterized by EA, FT-IR and 1HNMR. Using a static analytic method, solid-liquid phase equilibrium data (the solubility) of BADOPE in acetonitrile, acetone, methanol, tetrahydrofuran, ethanol, ethyl acetate, methylethylketone and 1,4-dioxane were obtained at temperatures ranging from 293 to 338 K. Several thermodynamic models, including the ideal, modified Apelblat, Wilson, NRTL, UNIQUAC and Scatchard-Hildebrand models, were applied to correlate the experimental solubility data.

Number of references:

28

Main heading:

Phase equilibria

Controlled terms:

Acetone  -  Differential scanning calorimetry  -  Esterification  -  Esters  -  Flame retardants  -  Oils and fats  -  Solubility  -  Synthesis (chemical)  -  Thermodynamic properties  -  Thermogravimetric analysis

Uncontrolled terms:

Differential scanning calorimeters  -  Enthalpy of fusion  -  Experimental solubility datum  -  Phosphate esters  -  Phosphorus-containing  -  Solid-liquid phase equilibria  -  Tetra-hydrofuran  -  Thermodynamic model

Classification code:

641.1 Thermodynamics -  801 Chemistry -  801.4 Physical Chemistry -  802.2 Chemical Reactions -  803 Chemical Agents and Basic Industrial Chemicals -  804.1 Organic Compounds

Database:

Compendex

Compilation and indexing terms, © 2013 Elsevier Inc.