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江城武汉

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[求助] 壳聚糖的纯化方法

各位对于壳聚糖的纯化方法有没有高见呀,求指导!
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shaojing690

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1,10 g CS溶于1 L1%醋酸溶液中,在40℃。状态下搅拌过夜,后在10000转/分钟,室温状态下离心1 h;
2,悬浮液用0.5 M NaOH溶液在搅拌状态下滴定,当pH=6.0时出现絮凝物,直至pH达到8.0;
3,在2中加入10 ml 10% w/v SDS溶液,加热到90-95℃,在其状态下搅拌5 min,冷却至室温,另滴数滴0.5 M NaOH溶液,使pH接近10,后在6000转/分钟,室温状态下离心30 min,接着用去离子水反复清洗(至少3遍),每清洗一遍离心一次,提取沉淀物,直到再次清洗沉淀物(搅匀)时悬浮液中完全去除SDS,最后将离心后的沉淀物冻干(先在70℃低温冰箱冻1 h,后放于冻干机中)。
2楼2014-10-20 14:27:46
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